• Title/Summary/Keyword: pore scale

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Evaluation of homogenized thermal conductivities of imperfect carbon-carbon textile composites using the Mori-Tanaka method

  • Vorel, Jan;Sejnoha, Michal
    • Structural Engineering and Mechanics
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    • v.33 no.4
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    • pp.429-446
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    • 2009
  • Three-scale homogenization procedure is proposed in this paper to provide estimates of the effective thermal conductivities of porous carbon-carbon textile composites. On each scale - the level of fiber tow (micro-scale), the level of yarns (meso-scale) and the level of laminate (macro-scale) - a two step homogenization procedure based on the Mori-Tanaka averaging scheme is adopted. This involves evaluation of the effective properties first in the absence of pores. In the next step, an ellipsoidal pore is introduced into a new, generally orthotropic, matrix to make provision for the presence of crimp voids and transverse and delamination cracks resulting from the thermal transformation of a polymeric precursor into the carbon matrix. Other sources of imperfections also attributed to the manufacturing processes, including non-uniform texture of the reinforcements, are taken into consideration through the histograms of inclination angles measured along the fiber tow path together with a particular shape of the equivalent ellipsoidal inclusion proposed already in Sko ek (1998). The analysis shows that a reasonable agreement of the numerical predictions with experimental measurements can be achieved.

Resolution and Image processing Methods of Tomogram and There impact of Computational Velocity Estimation (토모그램의 해상도와 영상처리 기법이 속도예측에 미치는 영향)

  • Lee, Min-Hui;Song, Da-Hee;Keehm, Young-Seuk
    • 한국지구물리탐사학회:학술대회논문집
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    • 2009.10a
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    • pp.147-154
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    • 2009
  • Physical properties of rocks, such as velocity, are strongly dependant on detailed pore structures, and recently, pore micro-structures by X-ray tomography techniques have been used to simulate and understand the physical properties. However, the smoothing effect during the tomographic reconstruction procedure often causes an artifact - overestimating the contact areas between grains. The pore nodes near a grain contact are affected by neighboring grain nodes, and are classified into grain nodes. By this artifact, the pore structure has higher contact areas between grains and thus higher velocity estimation than the true one. To reduce this artifact, we tried two image processing techniques - sharpening filter and neural network classification. Both methods gave noticeable improvement on contact areas between grains visually; however, the estimated velocities showed only incremental improvement. We then tried to change the resolutions of tomogram and quantify its impact on velocity estimation. The estimated velocity from the tomogram with higher spatial resolution was improved significantly, and with around 2 micron spatial resolution, the calculated velocity was very close to the lab measurement. In conclusion, the resolution of pore micro-structure is the most important parameter for accurate estimation of velocity using pore-scale simulation techniques. Also the estimation can be incrementally improved if combined with image processing techniques during the pore-grain classification.

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The Study of Pore Structure in Shale Gas Reservoir Using Large-area Particle Measurement Method (대면적 입자 측정 분석법을 이용한 셰일 가스 저류층 내공극 구조 연구)

  • Park, Sun Young;Ko, Yong-kyu;Choi, Jiyoung;Lee, Junhee
    • Korean Journal of Mineralogy and Petrology
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    • v.34 no.4
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    • pp.209-218
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    • 2021
  • Studies of pore structure in shale gas reservoirs are essential to increase recovery rates, which is in the spotlight concerning unconventional resources. In this study, the distribution of pores in shale gas reservoir sample were observed using Scanning Electron Microscope Particle Analysis (SELPA), which is appropriate to analyze the distribution of particle or shape for sample in large area. A sample from the A-068 borehole drilled in the Liard Basin was analyzed; calcite is the main mineral. The pore size ranges from tens of nanometers to hundreds of micrometers and the contribution of each pore size to overall sample porosity was determined using SELPA. The distribution of pores was determined by observing the surface in the same area at magnifications of ×1000, ×3000 and ×5000. Pores less than 100 nm were observed at high magnifications and confirm that small-scale pore distribution can be analyzed and identified rapidly using SELPA. The method introduced in this study will be useful to understand pore structures in unconventional reservoirs.

Fabrication of Wafer-Scale Anodized Aluminum oxide(AAO)-Based capacitive biosensor

  • Kim, Bongjun;Oh, Jeseung;Yoo, Kyunghwa
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.372.2-372.2
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    • 2016
  • Various nanobiosensors have been developed and extensively investigated. For their practical applications, however, the reproducibility and uniformity should be good enough and the mass-production should be possible. To fabricate anodized aluminium oxide (AAO)-based nanobiosesnor on wafer scale, we have designed and constructed a wafer-scale anodizing system. $1{\mu}m$-thick-aluminum is deposited on 4 inch SiO2/Si substrate and then anodized, resulting in uniform nanopores with an average pore diameter of about 65 nm. Furthermore, most AAO sensors constructed on this wafer provide capacitance values of 30 nF ~ 60 nF in PBS, demonstrating their uniformity.

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UNIFICATION OF THERMO-PHYSICS OF MATERIALS AND MECHANICS OF STRUCTURES - TOWARD A LIFE SPAN SIMULATOR OF STRUCTURAL CONCRETE -

  • Maekawa, K.;Ishida, T.
    • Proceedings of the Korea Concrete Institute Conference
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    • 1999.10a
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    • pp.29-46
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    • 1999
  • The performance based design obligates quantitative assessment of required performances by means of transparent and objective science. In this design scheme, simulation of both macro and micro-scale structural behaviors is thought to be a powerful tool. This paper proposes a way how to unify the structural safety and serviceability check method and durability assessment of RC structures. Though component chemical-physical processes are crudely assumed, system dynamics of micro-scale pore structure formation and macro-scale defects and deformation of structures was shown as possible and promising approach in future. The authors understand that the unification of structural and durability design has just started. For further progress and development, predictive tool of structural behaviors from birth to death of concrete under any specified environment and load serves as an essential technicality.

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Development and Basic Performance Characterization of Neutralized Fabric Filter (제전사여과포의 개발 및 기초성능 규명)

  • 박영옥;구철오;임정환;김홍룡;손재익;이영우
    • Journal of Energy Engineering
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    • v.7 no.1
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    • pp.57-64
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    • 1998
  • A neutralized fabric filter of which major raw materials were polyester and stainless steel fibers was developed and its physiochemical properties and basic filter characteristics were investigated. Four finds of dusts generated in the typical domestic industry were used, which were coke dust from a steel manufacturing process, cement dust from a cement manufacturing process, flu ash from a fluidized-bed combustor, and incinerator ash from a waste plastics incinerator. The physicochemical properties of the neutralized fabric filter were analyzed in terms of changes in tensile strength and initial elastic modulus under $SO_2$ and $NO_2$ atmospheres, mean flow pore pressure, bubble point pore diameter, mean flow pore diameter, and pore size distribution. In addition, the pressure drop, dust penetration, and figure of merit for the fabric filter were investigated in a bench-scale filter testing unit. The pressure drop increased as the filtration velocity and dust loading increased, and its increasing shape depended on the type of dust. The dust penetration rapidly decreased as the dust loading increased irrespective of the type of dust. The figures of merit for the fabric filters increased in the early stage of filtration and then showed rapid decreases followed maintaining a constant level.

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Development and Characterization of High Temperature Filter (내열성여과포의 개발 및 기초성능 규명)

  • 박영옥;구철오;임정환;김홍룡;손재익;이영우
    • Journal of Energy Engineering
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    • v.7 no.1
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    • pp.103-112
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    • 1998
  • A high temperature fabric filter was developed and characterized in order to solve the various problems encountered in the operation of industrial fabric filters. Four kinds of dusts generated in the typical domestic industry were used for its characterization, coke dust from a steel manufacturing process, cement dust from a cement manufacturing process, fly ash from a fluidized-bed combustor, and incinerator ash from a waste plastics incinerator. The physical and chemical properties of the high temperature fabric filter were analyzed in terms of mean flow pore pressure, bubble point pore diameter, mean flow pore diameter, pore size distribution, and the changes in tensile strength and initial elastic modulus under $SO_2$ and $NO_2$ atmospheres. Pressure drop, dust penetration, and figure of merit for the fabric filter were also investigated in a bench-scale filter testing unit. The fabric filter developed in this study had good physical and chemical filter properties and showed a very applicability to typical industrial dusts treatments.

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Microstructural, Mechanical, and Durability Related Similarities in Concretes Based on OPC and Alkali-Activated Slag Binders

  • Vance, Kirk;Aguayo, Matthew;Dakhane, Akash;Ravikumar, Deepak;Jain, Jitendra;Neithalath, Narayanan
    • International Journal of Concrete Structures and Materials
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    • v.8 no.4
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    • pp.289-299
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    • 2014
  • Alkali-activated slag concretes are being extensively researched because of its potential sustainability-related benefits. For such concretes to be implemented in large scale concrete applications such as infrastructural and building elements, it is essential to understand its early and long-term performance characteristics vis-a'-vis conventional ordinary portland cement (OPC) based concretes. This paper presents a comprehensive study of the property and performance features including early-age isothermal calorimetric response, compressive strength development with time, microstructural features such as the pore volume and representative pore size, and accelerated chloride transport resistance of OPC and alkali-activated binder systems. Slag mixtures activated using sodium silicate solution ($SiO_2$-to-$Na_2O$ ratio or $M_s$ of 1-2) to provide a total alkalinity of 0.05 ($Na_2O$-to-binder ratio) are compared with OPC mixtures with and without partial cement replacement with Class F fly ash (20 % by mass) or silica fume (6 % by mass). Major similarities are noted between these binder systems for: (1) calorimetric response with respect to the presence of features even though the locations and peaks vary based on $M_s$, (2) compressive strength and its development, (3) total porosity and pore size, and (4) rapid chloride permeability and non-steady state migration coefficients. Moreover, electrical impedance based circuit models are used to bring out the microstructural features (resistance of the connected pores, and capacitances of the solid phase and pore-solid interface) that are similar in conventional OPC and alkali-activated slag concretes. This study thus demonstrates that performance-equivalent alkali-activated slag systems that are more sustainable from energy and environmental standpoints can be proportioned.

A Study on Interaction Behaviors of Soil-PET Mat installed on Dredged Soils (연약한 준설점토상 매립시 포설된 PET 매트와 지반거동에 관한 연구)

  • Lee Man-Soo;Jee Sung-Hyun;Yang Tae-Seon
    • Journal of the Korean Geotechnical Society
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    • v.22 no.3
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    • pp.13-21
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    • 2006
  • Geosynthetic damage has attracted a major attention since the introduction of geotextiles for civil engineering applications. In this study 3 pilot trial embankments were carried out to investigate the behaviours of reinforced embankments over soft cohesive soils and to find the optimum methodology of embankments over soft soils. As the seamed part of polyester mat (PET, tensile strength 15 ton) used in the first full-scale field test was ruptured under progressing rotational slope failure because of unexpectedly rapid construction of embankments, the excessive pore water pressures were measured. On the soil behavior where tension explosion of mat was continued, pore pressure larger than the one caused by embankment height was measured. Especially, at the depth of 5.0 m under the ground pore pressure increased over long term. It was discussed with respect to the height of embankment and heaving behavior of soft soils.

Multi-scale simulation of drying process for porous materials using molecular dynamics (part 2: material properties) (분자동역학을 이용한 다공성 물질 건조공정 멀티스케일 시뮬레이션(2부: 미시 물성))

  • Baik S.M.;Keum Y.T.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.15 no.4
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    • pp.162-167
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    • 2005
  • As the properties of porous materials during the drying process relate to the atomistic defects of heterogeneous materials such as dislocation, grain, grain boundary, pore, etc., the knowledge of nano-scale analysis is needed in order to accurately analyze the drying process for porous materials. In this study, the atomic behavior of porous materials Is statically predicted by using the molecular dynamics simulation and the nano-scale material properties are computed. The elastic modulus, thermal expansion coefficient, and volumetric heat capacity numerically found from the molecular dynamics simulation are compared with those of experiment and theory and proved the accuracy.