• Title/Summary/Keyword: pore analysis

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Metal/$Al_2O_3-SiO_2$ System Interface Investigations

  • Korobova, N.;Soh, Deawha
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2004.05a
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    • pp.70-73
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    • 2004
  • The packaging of the integrated circuits requires knowledge of ceramics and metals to accommodate the fabrication of modules that are used to construct subsystems and entire systems from extremely small components. Composite ceramics (Al$_2$O$_3$-SiO$_2$) were tested for substrates. A stress analysis was conducted for a linear work-hardening metal cylinder embedded in an infinite ceramic matrix. The bond between the metal and ceramic was established at high temperature and stresses developed during cooling to room temperature. The calculations showed that the stresses depend on the mismatch in thermal expansion, the elastic properties, and the yield strength and work hardening rate of the metal. Experimental measurements of the surface stresses have also been made on a Cu/Al$_2$O$_3$-SiO$_2$ceramic system, using an indentation technique. A comparison revealed that the calculated stresses were appreciably larger than the measured surface stresses, indicating an important difference between the bulk and surface residual stresses. However, it was also shown that porosity in the metal could plastically expand and permit substantial dilatational relaxation of the residual stresses. Conversely it was noted that pore clusters were capable of initiating ductile rupture, by means of a plastic instability, in the presence of appreciable tri-axiality. The role of ceramics for packaging of microelectronics will continue to be extremely challenging.

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Fracture and Residual Stresses in $Metal/Al_2O_3-SiO_2$ System

  • Soh, D.;Korobova, N.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.11a
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    • pp.308-312
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    • 2003
  • The packaging of the integrated circuits requires knowledge of ceramics and metals to accommodate the fabrication of modules that are used to construct subsystems and entire systems from extremely small components. Composite ceramics ($Al_2O_3-SiO_2$) were tested for substrates. A stress analysis was conducted for a linear work-hardening metal cylinder embedded in an infinite ceramic matrix. The bond between the metal and ceramic was established at high temperature and stresses developed during cooling to room temperature. The calculations showed that the stresses depend on the mismatch in thermal expansion, the elastic properties, and the yield strength and work hardening rate of the metal. Experimental measurements of the surface stresses have also been made on a $Cu/Al_2O_3-SiO_2$ ceramic system, using an indentation technique. A comparison revealed that the calculated stresses were appreciably larger than the measured surface stresses, indicating an important difference between the bulk and surface residual stresses. However, it was also shown that porosity in the metal could plastically expand and permit substantial dilatational relaxation of the residual stresses. Conversely it was noted that pore clusters were capable of initiating ductile rupture, by means of a plastic instability, in the presence of appreciable tri-axiality. The role of ceramics for packaging of microelectronics will continue to be extremely challenging.

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A Relationship between Hydraulic Conductivity and Electrical Properties of Silty Sand on the Riverside of the Nakdong River (낙동강변 실트질 모래의 수리전도도와 전기적 물성과의 관계)

  • Kim, Soo-Dong;Park, Samgyu;Hamm, Se-Yeong;Oh, Yun-Yeong
    • Journal of Soil and Groundwater Environment
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    • v.19 no.3
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    • pp.39-46
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    • 2014
  • Hydraulic conductivity is an important parameter, representing permeable property of the groundwater in aquifers, in the issues of groundwater development, groundwater contamination, and groundwater flow, etc. We estimated a relationship between hydraulic conductivity and electrical properties (formation factor, chargeability, and time constant) of silty sand in the laboratory. For this study, we conducted grain size analysis, constant head permeameter test, and measured electrical resistivity and spectral induced polarization of silty sand samples collected from the riverside alluvium of the Nakdong River in Nogok-ri area, Dasan-myeon, Goryeong-gun in Gyeongbook Province, Korea. In the laboratory test, we used soil samples of approximately uniform porosity with 0.5% error range, and kept the electrical resistivity of pore water with 100 ohm-m. As a result, the relationship between effective particle size and hydraulic conductivity agrees fairly well with the existing empirical formulas. Hydraulic conductivity was correlated with formation factor, chargeability, and time constant: hydraulic conductivity increased with increasing formation factor and time constant as well as with decreasing chargeability.

Analysis of Disc Degeneration in a Poroelastic Spinal Motion Segment FE Model (다공탄성체 척추운동분절 유한요소 모델을 이용한 추간판의 퇴화과정 분석)

  • Woo D.G.;Kim Y.E.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.10a
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    • pp.248-251
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    • 2005
  • To investigate the degeneration process in the intervertebral disc, a three dimensional (3D) poroelastic finite-element (FE) model was developed. Disc was modeled as two different regions, such as annulus modeled with fiber reinforced 20 node poroelastic ground matrix and nucleus having large porosity. Excess Von Mises stress in the disc element assumed to be a possible source of degeneration under compressive loading condition. Recursive calculation was continued until the desired convergence was attained by changing the permeability and porosity of those elements, which could be predicted from the previous iteration. The degenerated disc model showed that relatively small compressive stresses were generated in the nucleus elements compared to normal disc. Its distribution along the sagittal plane was matched well with a previously reported experimental result. Contrasts to this result, pore pressures in the nucleus were higher than those in the normal disc. Total stress indicated similar values for two different models. This new approach using poroelastic modeling could provide the explanation of the interaction between fluid and solid matrix in the disc during the degeneration process.

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Effects of Current Density and Phosphoric Acid Concentration on Anodic Oxide Film of Titanium (전류밀도와 전해액의 인산농도가 Ti 양극 산화 피막에 미치는 영향)

  • Kim, Kye-Sung;Chung, Won-Sub;Shin, Heon-Cheol;Choe, Young-Son;Cho, Young-Rae
    • Korean Journal of Metals and Materials
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    • v.46 no.6
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    • pp.370-376
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    • 2008
  • The formation of anodic oxide film of titanium (Ti) was studied at a variety of electrolyte concentrations and current density to clarify their effects on morphology, microstructure and composition of Ti oxide layer. For the analysis of the Ti oxide films, a scanning electron microscopy (SEM), X-ray diffractometer (XRD), and X-ray photoelectron spectroscopy (XPS) were used. The results showed that the concentration of phosphoric acid played a crucial role in the crystalline structure of the Ti oxide layer while the current density gave a critical effect on the thickness and diameter of its pore. In particular, the crystalline anatase phase with a thickness larger than $2{\mu}m$, which is quite desirable for a dental implant application, could be readily prepared at the phosphoric acid concentration of 0.5 M and current density higher than $2.0A/dm^2$.

Shallow landslide susceptibility mapping using TRIGRS

  • Viet, Tran The;Lee, Giha;An, Hyun Uk
    • Proceedings of the Korea Water Resources Association Conference
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    • 2015.05a
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    • pp.214-214
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    • 2015
  • Rainfall induced landslides is one of the most devastating natural disasters acting on mountainous areas. In Korea, landslide damage areas increase significantly from 1990s to 2000s due to the increase of both rainfall intensity and rainy days in addition with haphazard land development. This study was carried out based on the application of TRIGRS unsaturated (Transient Rainfall Infiltration and Grid-based Regional Slope stability analysis), a Fortran coded, physically based, and numerical model that can predict landslides for areas where are prone to shallow precipitation. Using TRIGRS combining with the geographic information system (GIS) framework, the landslide incident happened on 27th, July 2011 in Mt. Umyeon in Seoul was modeled. The predicted results which were raster maps showed values of the factors of safety on every pixel at different time steps show a strong agreement with to the observed actual landslide scars in both time and locations. Although some limitations of the program are still needed to be further improved, some soil data as well as landslide information are lack; TRIGRS is proved to be a powerful tool for shallow landslide susceptibility zonation especially in great areas where the input geotechnical and hydraulic data for simulation is not fully available.

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Experimental assessment of the effect of frozen fringe thickness on frost heave

  • Jin, Hyun Woo;Lee, Jangguen;Ryu, Byun Hyun;Shin, Yunsup;Jang, Young-Eun
    • Geomechanics and Engineering
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    • v.19 no.2
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    • pp.193-199
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    • 2019
  • A frozen fringe plays a key role in frost heave development in soils. Previous studies have focused on the physical and mechanical properties of the frozen fringe, such as overall hydraulic conductivity, water content and pore pressure. It has been proposed that the thickness of the frozen fringe controls frost heave behavior, but this effect has not been thoroughly evaluated. This study used a temperature-controllable cell to investigate the impact of frozen fringe thickness on the characteristics of frost heave. A series of laboratory tests was performed with various temperature boundary conditions and specimen heights, revealing that: (1) the amount and rate of development of frost heave are dependent on the frozen fringe thickness; (2) the thicker the frozen fringe, the thinner the resulting ice lens; and (3) care must be taken when using the frost heave ratio to characterize frost heave and evaluate frost susceptibility because the frost heave ratio is not a normalized factor but a specimen height-dependent factor.

Techniques to Estimate Permeability Based on Spectral Induced Polarization Survey (광대역유도분극 탐사에 기초한 유체투과도 예측기법들)

  • Kim, Bitnarae;Cho, AHyun;Weller, Andreas;Nam, Myung Jin
    • Journal of Soil and Groundwater Environment
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    • v.25 no.2_spc
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    • pp.55-69
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    • 2020
  • Permeability-analyzing methods commonly involve small-scale drilling, such as pumping or slug test, but it is difficult to identify overall distribution of permeability of the entire target sites due to high cost and time requirement. Spectral induced polarization (SIP) method is known to be capable of providing distributions of both the porosity and the pore size, the two major parameters determining permeability of the porous medium. The relationship between SIP variables and permeability has been studied to identify the hydrological characteristics of target sites. Kozeny-Carman formula has been improved through many experiments to better predict fluid permeability with electrical properties. In this work, the permeability prediction techniques based on SIP data were presented in accordance with the hydrogeological and electrical characteristics of a porous medium. Following the summary of the techniques, various models and related laboratory experiments were analyzed and examined. In addition, the field applicability of the prediction model was evaluated by field case analysis.

A Study on the Corrosion Behavior of Magnesium Alloy Sealed with Chemical Conversion Coating and Sol-gel Coating

  • Lee, Dong Uk;Chaudhari, Shivshankar;Choi, Seung Yong;Moon, Myung Jun;Shon, Min Young
    • Corrosion Science and Technology
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    • v.20 no.4
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    • pp.175-182
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    • 2021
  • Magnesium alloy is limited in the industrial field because its standard electrode potential is -2.363 V vs. NHE (Normal Hydrogen Electrode) at 25 ℃. This high electrochemical activity causes magnesium to quickly corrode with oxygen in air; chemical conversion coating prevents corrosion but causes surface defects like cracks and pores. We have examined the anti-corrosion effect of sol-gel coating sealed on the defected conversion coating layer. Sol-gel coatings produced higher voltage current and smaller pore than the chemical conversion coating layer. The conversion coating on magnesium alloy AZ31 was prepared using phosphate-permanganate solution. The sol-gel coating was designed using trimethoxymethylsilane (MTMS) and (3-Glycidyloxypropyl) trimethoxysilane (GPTMS) as precursors, and aluminum acetylacetonate as a ring-opening agent. The thermal shock resistance was tested by exposing specimens at 140 ℃ in a convection oven; the results showed changes in the magnesium alloy AZ31 surface, such as oxidization and cracking. Scanning electron microscope (FE-SEM) analysis confirmed a sealed sol-gel coating layer on magnesium alloy AZ31. Electrochemical impedance spectroscopy (EIS) measured the differences in corrosion protection properties by sol-gel and conversion coatings in 0.35 wt% NaCl solution, and the potentiodynamic polarization test and confirmed conversion coating with the sol-gel coating show significantly improved resistance by crack sealing.

Experimental study on treatment of waste slurry by vacuum preloading with different conditioning agents

  • Wu, Yajun;Jiang, Haibo;Lu, Yitian;Sun, Dean
    • Geomechanics and Engineering
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    • v.17 no.6
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    • pp.543-551
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    • 2019
  • In China, serious environmental problems are induced by the extremely soft construction waste slurries in many urban areas, and there is no appropriate method to treat it presently. In this paper, four model tests were conducted to investigate the efficiency of waste slurry treatment by combining three conditioning agents which can change characteristics of the slurries with a traditional vacuum preloading method. The tests of size analysis of particle aggregate were conducted to investigate the influence of different conditioning agents on the size distributions of particle aggregate. During the model test, the discharged water volumes were monitored. The pore-size distribution and void ratio of the waste slurries after the vacuum preloading were measured by mercury intrusion porosimetry (MIP). It is found that 1) During the natural precipitation, volume of water out of the organic agent is higher than that of the mixed agent, but it is smaller than that of the mixed agent in the vacuum preloading stage; 2) the mixed agent has a higher total volume of water out than the organic agent and the inorganic agent after test, while the organic agent and the inorganic agent have little difference with respect to the drainage effect. The results demonstrate that the combination of mixed conditioning agent and vacuum preloading for the solid-liquid separation in waste slurry has a satisfactory effect and can be applied in engineering practice.