• 제목/요약/키워드: plasma measurement

검색결과 780건 처리시간 0.034초

구리 시료의 정량분석을 위한 LIBS의 최적조건 연구 (Investigation of the optimum condition for the quantitative analysis of Cu sample by Laser induced breakdown spectroscopy)

  • 김승현;신희성;주준식;김호동
    • 분석과학
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    • 제22권2호
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    • pp.141-147
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    • 2009
  • Laser induced breakdown spectroscopy (LIBS)의 정량분석에 대한 측정의 정확도를 향상시키고자, 플라즈마의 특성을 분석하여, 상대적으로 안정적인 Outer sphere에 해당하는 영역을 측정하는 방법으로 Cu alloy sample을 측정하여 분석하였다. 신호의 높은 재현성을 고려한 측정 조건에서 측정이 수행되었으며, 600 mtorr 진공상태에서 20 mm정도의 크기로 플라즈마를 성장시켜, Outer sphere 영역인 플라즈마 성장방향으로 6.0 mm 지점을 측정하였다. 그 결과 Cu의 선형 분석 $R^2$ 값은 0.9886로, Ni의 $R^2$ 값은 0.9988로 획득하였으며, 측정오차는 Ni의 경우 기존보다는 향상된 0.78%의 측정오차를 획득하였다.

여성 견비통 환자의 생혈액 형태에 대한 임상적인 연구 (A Clinical Study of the Live Blood Condition of Women′s Shoulder Measurement)

  • 김경철
    • 대한한의학회지
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    • 제25권3호
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    • pp.99-104
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    • 2004
  • Objectives : To study the Live Blood Condition of chronic shoulder measurement. Methods : Twenty-one patients were studied. The observation items of the Live Blood Condition are the form's abnormality and cohesion of red blood cells, the abnormality of hemoglobin and the toxicity in plasma. Results : 1. The form's abnormality and cohesion of red blood cells observed were erythrocyte aggregation (8 persons), Rouleau (3 persons), target cells (7 persons), ovalocytes (3 persons), poikilocytes (2 persons). Double conditions observed were erythrocyte aggregation & target cells (3 persons), erythrocyte aggregation & poikilocytes (1 person), target cells & ovalocytes (l person). 2. The abnormality of hemoglobin and the toxicity in plasma observed were cholesterol crystals (5 persons), atherosclerotic plaque (3 persons), chylous (6 persons). 3. The form normality of red blood was generally observed in one woman. The normality of hemoglobin and the non-toxicity in plasma were generally observed in seven women. Conclusions : According to this study of the Live Blood Condition of women's shoulder measurement, these results suggest that the twenty-one patients evidence the conditions of extravasated blood and phlegm.

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Measurement of ion-induced secondary electron emission coefficient for MgO thin film with $O_{2}$ plasma treatment

  • Jeong, H.S.;Oh, J.S.;Lim, J.Y.;Cho, J.W.;Choi, E.H.
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2003년도 International Meeting on Information Display
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    • pp.802-805
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    • 2003
  • The ion-induced secondary electron emission coefficient ${\gamma}$ for MgO thin film with $O_{2}$ plasma treatment has been investigated by ${\gamma}$-FIB (focused ion beam) system. The MgO thin film deposited from sintered material with $O_2$ plasma treatment is found to have higher ${\gamma}$ than that without $O_{2}$ plasma treatment. The energy of $Ne^{+}$ ions used has been ranged from 100eV to 200eV throughout this experiment. It is found that the highest secondary electron emission coefficient ${\gamma}$ has been achieved for 10 minutes of $O_{2}$ plasma treatment.

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Effects of Ar-Plasma Treatment in Alkali-Decomposition of Poly(ethylene terephthalate)

  • Seo, Eun-Deock
    • Macromolecular Research
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    • 제11권5호
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    • pp.387-392
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    • 2003
  • The ablation effects of Ar-plasma treatment and alkali-decomposition behavior in NaOH solution of polyethylene terephthalate (PET) film were investigated. The modifications were evaluated by analysis of atomic force microscopy topographical changes, and by the measurement of decomposition yield in conjunction with heats of formation and electron densities of acyl carbon calculated by Parameterization Method 3 method. It has shown that the alkali-decomposition is hampered by plasma treatment and its decomposition yield is closely related with plasma treatment conditions such as exposure time to plasma. Plasma-treated PET films exhibited lower decomposition yield, compared to that of virgin PET. Increasing plasma exposure time contributes positively to decrease the decomposition yield. It has also shown that the topography of PET surface was affected by the base-promoted hydrolysis as well as Ar-plasma treatments. These behaviors are attributed to the decreased nucleophilicity of acyl carbon damaged by the ablation of Ar-plasma.

Amine functionalized plasma polymerized PEG film: Elimination of non-specific binding for biosensing

  • Park, Jisoo;Kim, Youngmi;Jung, Donggeun;Kim, Young-Pil;Lee, Tae Geol
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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    • pp.378.2-378.2
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    • 2016
  • Biosensors currently suffer from severe non-specific adsorption of proteins, which causes false positive errors in detection through overestimation of the affinity value. Overcoming this technical issue motivates our research. Polyethylene glycol (PEG) is well known for its ability to reduce the adsorption of biomolecules; hence, it is widely used in various areas of medicine and other biological fields. Likewise, amine functionalized surfaces are widely used for biochemical analysis, drug delivery, medical diagnostics and high throughput screening such as biochips. As a result, many coating techniques have been introduced, one of which is plasma polymerization - a powerful coating method due to its uniformity, homogeneity, mechanical and chemical stability, and excellent adhesion to any substrate. In our previous works, we successfully fabricated plasmapolymerized PEG (PP-PEG) films [1] and amine functionalized films [2] using the plasma enhanced chemical vapor deposition (PECVD) technique. In this research, an amine functionalized PP-PEG film was fabricated by using the plasma co-polymerization technique with PEG 200 and ethylenediamine (EDA) as co-precursors. A biocompatible amine functionalized film was surface characterized by X-ray photoelectron spectroscopy (XPS) and Fourier-transform infrared spectroscopy (FT-IR). The density of the surface amine functional groups was carried out by quantitative analysis using UV-visible spectroscopy. We found through surface plasmon resonance (SPR) analysis that non-specific protein adsorption was drastically reduced on amine functionalized PP-PEG films. Our functionalized PP-PEG films show considerable potential for biotechnological applications such as biosensors.

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유전체 장벽 방전 플라즈마의 전자파 산란 특성 분석 (Analysis of Electromagnetic Wave Scattering Characteristics of Dielectric Barrier Discharge Plasma)

  • 이수민;오일영;홍용준;육종관
    • 한국전자파학회논문지
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    • 제24권3호
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    • pp.324-330
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    • 2013
  • 본 논문은 대기압 환경에서 발생하는 유전체 장벽 방전(dielectric barrier discharge: DBD) 플라즈마의 전자파 산란 특성을 측정하였다. 본 논문에서는 기본적인 DBD 플라즈마 발생기 구조를 병렬로 연결하여 넓은 면적의 플라즈마 발생기를 제작하였고, 14 kV, 4 kHz의 고전압 발생장치를 이용해 플라즈마가 발생하는 것을 확인하였다. 두 개의 혼 안테나와 벡터 네트워크 분석기를 이용해 S-parameter의 비교를 통해 전자파 산란 특성을 측정하였다. 전방 산란의 경우 제작된 플라즈마 발생기의 구조적 특성으로 인해 안테나의 편파에 따라 다른 결과 값을 얻었다. 편파가 수평일 때 최대 2 dB의 산란파 감쇠 특성을 확인할 수 있었다. 또한, 편파가 수평일 경우, 플라즈마 발생기 뒤에 PEC를 설치한 후 후방 산란 특성을 측정하였다. 그 결과, 5 GHz에서 안테나 관찰 각도가 $40^{\circ}C$, $60^{\circ}C$일 때 최대 2 dB 산란파 감쇠 특성을 얻었다.

Determination of Isotopic Ratios for Ca in Inductively Coupled Plasma Mass Spectrometry (ICPMS) by Removing Water Related Molecules

  • 박용남;S. R. Koirtyohann
    • Bulletin of the Korean Chemical Society
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    • 제18권11호
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    • pp.1172-1175
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    • 1997
  • Calcium isotopic ratios are precisely measured by removing isobaric interferences originated from water in the plasma. Liquid Ar cryogenic trap combined with membrane desolvator could eliminate backgrounds at m/z 42 and 44. Slow drift of ICP-MS is corrected by the frequent running of the standards. It is found necessary to separate Ca from the sample matrix using Ca oxalate precipitation technique. Currently, the RSD is 0.5-1.0% for 2 minutes of measurement but is expected to be improved if the measurement time is increased. The technique was applied to 42Ca enriched baby fecal samples and successfully determined 42Ca/44Ca ratio changes.

Organic Thin Film Transistors with Gate Dielectrics of Plasma Polymerized Styrene and Vinyl Acetate Thin Films

  • Lim, Jae-Sung;Shin, Paik-Kyun;Lee, Boong-Joo
    • Transactions on Electrical and Electronic Materials
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    • 제16권2호
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    • pp.95-98
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    • 2015
  • Organic polymer dielectric thin films of styrene and vinyl acetate were prepared by the plasma polymerization deposition technique and applied for the fabrication of an organic thin film transistor device. The structural properties of the plasma polymerized thin films were characterized by Fourier-transform infrared spectroscopy, X-ray diffraction, atomic force microscopy, and contact angle measurement. Investigation of the electrical properties of the plasma polymerized thin films was carried out by capacitance-voltage and current-voltage measurements. The organic thin film transistor device with gate dielectric of the plasma polymerized thin film revealed a low operation voltage of −10V and a low threshold voltage of −3V. It was confirmed that plasma polymerized thin films of styrene and vinyl acetate could be applied to functional organic thin film transistor devices as the gate dielectric.

Measurement of Electron Temperature and Plasma Density in Coplanar AC Plasma Display Panels.

  • Cho, Il-Ryong;Moon, Min-Yook;Ryu, Chung-Gon;Choi, Myung-Chul;Choi, Eun-Ha
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2003년도 International Meeting on Information Display
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    • pp.748-751
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    • 2003
  • The electron temperature and plasma density in coplanar alternating-current plasma display panels (AC-PDPs) have been experimentally investigated by a micro Langmuir probe and the high speed discharge images in this experiment.

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An Indirect Method to Monitor Plasma Status in a Transformer Coupled Plasma

  • 유대호;안승규;김지훈;장홍영
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2011년도 제40회 동계학술대회 초록집
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    • pp.216-216
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    • 2011
  • There have been various direct or indirect methods to measure the characteristics of plasma. Comparing to direct method like Langmuir probe method, indirect measurements which give information as some external parameters like current, voltage, or phase are easier to obtain. In this research, an indirect method to measure averaged plasma density in a transformer coupled plasma(TCP) has been proposed and evaluated. With a simple analytic model connecting electrical characteristics to plasma impedance, direct measurement via double Langmuir probe has been performed. This result may play a meaningful role to diagnose TCP or similar plasma sources

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