• Title/Summary/Keyword: piezoelectric ceramic material

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Electrical Properties of $Bi_4Ti_3O_{12}$ Thin Films dependant on Oxygen Partial Pressure during Annealing (열처리 산소 분압에 따른 $Bi_4Ti_3O_{12}$ 박막의 전기적 특성 변화)

  • Cha, Yu-Jeong;Nahm, Sahn;Jeong, Young-Hun;Lee, Young-Jin;Paik, Jong-Hoo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.191-191
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    • 2009
  • $Bi_4Ti_3O_{12}$ (BiT) thin films were well developed on the Pt/Ti/$SiO_2/Si$ substrate by a metal organic decomposition (MOD) method. Oxygen was effective on the crystallization of the BiT thin films during a rapid thermal annealing process. The electrical properties of the BiT films dependant on the oxygen partial pressure were investigated. No crystalline phase was observed for the BiT film annealed at $700^{\circ}C$ under oxygen free atmosphere. However, its crystallinity was significantly evolutionned with increasing oxygen partial pressure. In addition, its dielectric and piezoelectric properties were enhanced with increasing oxygen partial pressure to 10 torr. Especially, the BiT film, annealed at $700^{\circ}C$ and 10 torr oxygen pressure, showed good dielectric properties: dielectric constant of 51 and dielectric loss of 0.2 % at 100 kHz. Its leakage current and piezoelectric constant ($d_{33}$) was also considerably improved, being as 0.62 nA/$cm^2$ at 1 V and approximately 51 pm/V, respectively.

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Effects of Pre-synthesized $BaTiO_3$ Addition on the Microstructure and Dielectric/ Piezoelectric Properties of $(Bi_{0.5}Na_{0.5})_{0.94}Ba_{0.06}TiO_3$ Piezoelectric Ceramics

  • Khansur, Neamul Hayet;Yoon, Man-Soon;Kweon, Soon-Yong;Lee, Young-Geun;Ur, Soon-Chul
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.189-189
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    • 2008
  • Due to the environmental issue vast research is going on to replace the widely used lead contented piezoelectric materials. Bismuth sodium titanate (abbreviated as BNT) based bismuth sodium titanate-barium titanate (abbreviated as BNBT) ceramic was prepared by using modified method rather than conventional mixed oxide method. This modification was made to improve the properties of BNT based ceramic. In this procedure $BaTiO_3$ (abbreviated as BT) was prepared using conventional mixed oxide method. Analytical grade raw materials of $BaCO_3$ and $TiO_2$ were weighted and ball milled using ethanol medium. The mixed slurry was dried and sieved under 80 mesh. Then the powder was calcined at $1100^{\circ}C$ for 2 hours. This calcined BT powder was used in the preparation of BNBT. Stoichiometric amount of $Bi_2O_3$, $Na_2CO_3$, $TiO_2$ and BT were weighted and mixed by using ball mill. The used calcination temperature was $850^{\circ}C$ for 2 hours. Calcined powder was taken for another milling step. BNBT disks were pressed to 15 mm of diameter and then cold isostatical press (CIP) was used. Pressed samples were sintered at $1150^{\circ}C$ for 2 hours. The SEM microstructure analysis revealed that the grain shape of the sintered ceramic was polyhedral and grain boundary was well matched where as the sample prepared by conventional method showed irregular arrangement and grain boundary not well matched. And sintered density was better (5.78 g/cc) for the modified method. It was strongly observed that the properties of BNBT ceramic near MPB composition was found to be improved by the modified method compare to the conventional mixed oxide method. The piezoelectric constant dB of 177.33 pC/N, electromechanical coupling factor $k_p$ of 33.4%, dielectric constant $K_{33}^T$ of 688.237 and mechanical quality factor $Q_m$ of 109.37 was found.

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Evolution of Remnant State Variables and Linear Material Moduli in a PZT Cube under Compressive Stress at Room and High Temperatures (상온과 고온에서 압축하중을 받는 PZT에서의 잔류상태변수와 선형재료상수의 변화)

  • Ji, Dae Won;Kim, Sang-Joo
    • Journal of the Korean Ceramic Society
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    • v.50 no.1
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    • pp.82-86
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    • 2013
  • A poled lead zirconate titanate (PZT) cube specimen is subjected to impulse-type compressive stress with increasing magnitude in parallel to the poling direction at four room and high temperatures. During the ferroelastic domain switching induced by the compressive stress, electric displacement in the poling direction and longitudinal and transverse strains are measured. Using the measured responses, linear material properties, namely, the piezoelectric and elastic compliance coefficients, are evaluated by a graphical method, and the effects of stress and temperature are analyzed. Finally, the dependency of the evaluated linear material properties on relative remnant polarization is analyzed and discussed.

Preparation and Characterization of Small Sized PZT Powders: A Sol-Gel Modified Approach

  • Choi, Kyu-Man;Lee, Hae-Chun
    • The Journal of Korea Institute of Information, Electronics, and Communication Technology
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    • v.1 no.2
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    • pp.27-32
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    • 2008
  • A current research basically diverted towards an increase in the operational output with the minimization of the materials used, which ultimately scaled down the dimensions of ceramic electronic components. In this direction the nano-technology pave the revolutionary changes in particular the electronic industries. The applications of nano-sized particles or nano-sized materials are hence, playing a significant role for various purposes. The PZT(lead, zirconium, titanium) based ceramics which, are reported to be ferroelectric materials have their important applications in the areas of surface acoustic waves (SAW), filters, infrared detectors, actuators, ferroelectric random access memory, speakers, electronic switches etc. Moreover, these PZT materials possess the large electro mechanical coupling factor, large spontaneous polarization, low dielectric loss and low internal stress etc. Hence, keeping in view the unique properties of PZT piezoelectric ceramics we also tried to synthesize indigenously the small sized PZT ceramic powder in the laboratory by using the modified sol-gel approach. In this paper, propyl alcohol based sol-gel method was used for preparation of PZT piezoelectric ceramic. The powder obtained by this sol-gel process was calcined and sintering to reach a pyrochlore-free crystal phase. The characterization of synthesized material was carried out by the XRD analysis and the surface morphology was determined by high resolution scanning electron microscopy.

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Development of the Ultrasonic Transducers for the Degradation of TCE in Aqueous Solution (수중 TCE 분해용 압전 초음파 트랜스듀서 개발)

  • Lee, Youngjin
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.27 no.11
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    • pp.753-759
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    • 2014
  • This paper describes the development of a piezoelectric flextensional transducer, which aims to effectively degrade the TCE contained in aqueous solution. In order to adjust the 1st flextensional resonant frequency and output displacement of the flextensional transducer, the effect of the geometrical variations on performance was analyzed using the finite element analysis (FEM). The results indicated that the effect of external shell's thickness and curvature were most significant, and experimental fabrication and characterization of a transducer was performed to confirm the results. To prove the capacity to degrade the TCE contained in aqueous solution, 50 and 100 ppm of TCE were prepared in sealed chamber, and investigated the removal rate of TCE through the time and initial concentration.

The FEA of the Travelling-wave Ultrasonic Motor (진행파형 초음파 모터의 유한요소해석)

  • Kim, Sung-Hyun;Park, Tae-Gone
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07b
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    • pp.681-684
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    • 2003
  • Piezoelectric motors have been successfully developed for various applications like autofocus drives in camera lenses and handling equipment for high-accuracy positioning. In this paper, the travelling-wave motor which used in the camera lense, using bending vibration of a ring was studied. The basic structure of the motor is same but we suggested a few parameters for considering their design. The parameter is different from sine and cosine region of the voltage of the ceramic surface, displacement according to the wave number difference, and the phase difference. Same size of ceramics and aluminium ring were used for the stator. As a result, the displacement is dependent on the wave number.

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Design and Analysis of a L shape two touch point ultrasonic rotary motor (L형 2타점 회전모터의 설계와 해석)

  • Kim, Sung-Hyun;Park, Tae-Gone
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.11a
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    • pp.85-88
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    • 2004
  • The piezoelectric ceramic is attached between 'L' type guide and 'L' type stator, This motor has rotary motion which is operated by longitudinal and bending mode. The basic structure of the two kinds of type motor that called one stator motor, two stator motor is same but we suggested a few parameters for considering their stator design and characteristics. As a result, the two stator type motor is much more useful than one stator type motor for hi-direction rotation.

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The fabrication and strain properties of piezoeletric ceramic actuator using PMN - PT -PZ system (PMN - PT - PZ 계 세라믹스를 이용한 압전 엑츄에이터의 제작 및 변위 특성)

  • Ji, Seung-Han;Lee, Neung-Heon;Lee, Deok-Chool;Kim, Ho-Gi
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1993.05a
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    • pp.15-18
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    • 1993
  • Piezoelectric Actuator and electrostrictive Actuator samples were fabricated using PMN-PT-PZ system ceramics with Barium substitution, and the strain properties of them investigated. The largest Piezoelectric coefficient and electromechanical coupling coefficient were observed at sintering temperature $1250^{\circ}C$, Barium 0.05 mol %. The strain of poled samples is observed twice highly then unpoled ones, and the former showed larger hysteresis in strain then the latter, too. Poled multilayered actuator samples showed considerable strain.

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The effect of PCN substitution on dielectric and piezoelectric properties of PMN-PZT Ceramics (PCN 치환이 PMN-PZT 세라믹스에 유전 및 압전특성에 미치는 영향)

  • Nam, Seung-Hyon;Yoo, Ju-Hyun;Lee, Su-Ho;Jeong, Yeong-Ho;Park, Chang-Yub
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.04b
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    • pp.161-164
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    • 2004
  • In this study, to develop the composition ceramics for the Ultrasonic vibrator, $Pb(Mn_{1/3}Nb_{2/3})O_3Pb(Zr.Ti)O_3$ system ceramics were manufactured as a function of PCN substitution. Its dielectric and piezoelectric characteristics were investigated. With increasing the amount of PCN substitution, electromechanical coupling factor(kp) were increased until 3mol% PCN and that after decreased. mechanical quality factor(Qm) showed the maxinum value at 2mol% PCN. Eletromechanical coupling factor, mechanical quality factor and dielectric constant were showed optimum value at PCN 2mol% as 0.58, 1630 and 1407, respectively for ultrasonic vibrator applications.

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The Characteristics of an Ultrasonic Sprayer by using Piezoelectric Ceramic Resonator (압전 세라믹 진동자를 이용한 초음파 분무기의 분무 특성)

  • Bae, Sang-Tae;Lee, Su-Ho;Sug, Jeong-Young;Kim, Cheol-Hwan;SaGong, Geon
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.22 no.5
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    • pp.405-410
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    • 2009
  • The conventional ultrasonic nozzle produces a mist by applying an ultrasonic vibration into a non-flowering liquid. In this paper, we first present a novel designed nozzle type sprayer that is able to apply an ultrasonic vibration directly to the moving liquid and generate a mist instantly. For the novel nozzle, a ring-type actuator of the novel nozzle was designed and built using the PZW-PMN-PZT ceramics. This paper will describe a variety of physical, mechanical, and electrical characteristics of the ultrasonic nozzle. The characteristics of the mist particles was also measured as the amount of the outflow liquid was varied.