• Title/Summary/Keyword: performance characterization

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Fabrication of Micro Solid Oxide Fuel Cell by Thin Film Processing Hybridization: I. Multilayer Structure of Sputtered YSZ Thin Film Electrolyte and Ni-Based Anodes deposited by Spray Pyrolysis (박막공정의 융합화를 통한 초소형 고체산화물 연료전지의 제작: I. Spray Pyrolysis법으로 증착된 Ni 기반 음극과 스퍼터링으로 증착된 YSZ 전해질의 다층구조)

  • Son, Ji-Won;Kim, Hyoung-Chul;Kim, Hae-Ryoung;Lee, Jong-Ho;Lee, Hae-Weon;Bieberle-Hutter, A.;Rupp, J.L.M.;Muecke, U.P.;Beckel, D.;Gauckler, L.J.
    • Journal of the Korean Ceramic Society
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    • v.44 no.10
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    • pp.589-595
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    • 2007
  • Physical properties of sputtered YSZ thin film electrolytes on anode thin film by spray pyrolisis has been investigated to realize the porous electrode and dense electrolyte multilayer structure for micro solid oxide fuel cells. It is shown that for better crystallinity and density, YSZ need to be deposited at an elevated temperature. However, if pure NiO anode was used for high temperature deposition, massive defects such as spalling and delamination were induced due to high thermal expansion mismatch. By changing anode to NiOCGO composite, defects were significantly reduced even at high deposition temperature. Further research on realization of full cells by processing hybridization and cell performance characterization will be performed in near future.

The novel encapsulation method for organic thin-film transistor (새로운 방식의 유기박막트랜지스터 패시베이션 기술)

  • Lee, Jung-Hun;Kim, Seong-Hyun;Kim, Ki-Hyun;Lim, Sang-Chul;Cho, Eu-Na-Ri;Jang, Jin;Zyung, Tae-Hyung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.05a
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    • pp.177-180
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    • 2004
  • In this study, we report a novel encapsulation method for longevity of an organic thin-film transistor (OTFT) using pentaceneby means of an adhesive multiplayerincluded Al film. For encapsulation of OTFTs, the Al film adhered onto the OTFT in a dry nitrogen atmosphere using a proper adhesive. A lifetime, which was defined as the time necessary to reduce mobility to 2% of initial mobility value, was observed from the typical $I_{D-VD}$ characteristics of the field-effect transistor (FET). The initial field effect mobility ${\mu}$ was measured to be $2.0{\times}10^{-1}\;cm^2/Vs$. The characterization was maintained for long times in air. No substantial degeneration occurred. The performance and the stability are probably due to the encapsulation effect.

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Property change of organic light-emitting diodes due to a SAM treatment of the ITO surface (ITO 표면의 SAM형 습식 개질에 의한 유기 발광 소자의 특성 변화)

  • Na, Su-Hwan;Joo, Hyun-Woo;An, Hui-Chul;Kim, Tae-Wan;Song, Min-Jong;Lee, Ho-Sik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.314-315
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    • 2008
  • We have studied a property change of organic light-emitting diodes (OLED)s due to a surface reformation of indium-tin-oxide(ITO) substrate. An ITO is widely used as a transparent electrode in light-emitting diodes, and the OLEDs device performance is sensitive to the surface properties of the ITO. The ITO surface reformation could reduce the Schottky barrier at the ITO/organic interface and increase the adhesion of the organic layer onto the electrode. We have studied the characteristics of OLEDs with a treatment by a wet processing of the ITO substrate. The self-assembled monolayer(SAM) was used for wet processing. The characteristics of OLEDs were improved by SAM treatment of an ITO in this work. The OLEDs with a structure of ITO/TPD(50nm)/$Alq_3$(70nm)/LiF(0.5nm)/Al(100nm) were fabricated, and the surface properties of ITO were investigated by using seneral characterization techniques. Self-assembled monolayer introduced at the anode/organic interface gave an improvement in turn-on voltage, luminance and external quantum efficiency compared to the device without the SAM layer. SAM-treatment time of the ITO substrate was made to be 0/10/15/20/25min. The current efficiency of the device with 15min. treated SAM layer was increased by 3 times and the external quantum efficiency by 2.6 times.

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Characterization of A Catalystic Gas Sensor for Measuring Heat Content of Natural Gas (천연가스의 열용량을 측정하기 위한 촉매가스센서의 특징)

  • Lee K. Y.;Maclay G. J.;Stetter J. R.
    • Journal of the Korean Institute of Gas
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    • v.2 no.1
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    • pp.1-6
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    • 1998
  • A low power (below than 300 mW) catalytic bead combusible gas sensor is developed and utilized with a computer controlled sampling system for measuring heat content of natural gas. The heat content of gas is proportional to the change in the energy required to exposure to the sample of combustible gas. The heat content of natural gas samples ranging 36.30 - 39.88 $MJ/m^3$ is measured in the range of approximately $1\%$ error, which is comparable to its nominal heat content. Each gas represents a slightly different curve of sensitivity to sensor temperature. Thus all of the sensitivities are not equal to every temperature. In calibration process the choice of a optimum operating temperature is an important factor that influences the overall performance of the measurement system.

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Evaluation of the Performance of Multi-binders (lime, DAP and ladle slag) in Treating Metal(loid)s-contaminated Soils (중금속류 오염 토양 처리를 위한 복합 고화제(lime, DAP, 래들 슬래그) 성능 평가)

  • Choi, Jiyeon;Shin, Won Sik
    • Journal of Environmental Science International
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    • v.26 no.8
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    • pp.955-966
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    • 2017
  • Amendment of multi-binders was employed for the immobilization of metal(loid)s in field-contaminated soils to reduce the leaching potential. The effect of different types of multi-binders (lime/diammonium phosphate, diammonium phosphate/ladle slag and lime/ladle slag) on the solidification/stabilization of metal(loid)s (Pb, Zn, Cu and As) from the smelter soil and mine tailing soil were investigated. The amended soils were evaluated by measuring Toxicity Characterization Leaching Procedure (TCLP) leaching concentration of metal(loid)s. The results show that the leaching concentration of metal(loid)s decreased with the immobilization using multi-binders. In terms of TCLP extraction, the mixed binder was effective in the order of lime/ladle slag > diammonium phosphate/ladle slag > lime/diammonium phosphate. When the mixed binder amendment (0.15 g lime+0.15 g ladle slag for 1g smelter soil and 0.05 g lime+0.1 g ladle slag for 1 g mine tailing soil, respectively) was used, the leaching concentration of metal(loid)s decreased by 90%. However, As leaching concentration increased with diammonium phosphate/lime and diammonium phosphate/ladle slag amendment competitive anion exchange between arsenic ion and phosphate ion from diammonium phosphate. The Standard, Measurements and Testing programme (SM&T) analysis indicated that fraction 1 (F1, exchangeable fraction) decreased, while fraction 4 (F4, residual fraction) increased. The increased immobilization efficiency was attributed to the increase in the F4 of the SM&T extraction. From this work, it was possible to suggest that both arsenic and heavy metals can be simultaneously immobilized by the amendment of multi-binder such as lime/ladle slag.

A Study on Fabrication and Characterization of Inorganic Insulation Material by Hydrothermal Synthesis Method (1) (수열합성법을 이용한 무기계 단열소재 제조방법 및 특성에 관한 연구 (1))

  • Seo, Sung-Kwan;Chu, Yong-Sik;Lee, Jong-Kyu;Song, Hun;Park, Jae-Wan
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.1 no.3
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    • pp.219-224
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    • 2013
  • In this study, the inorganic insulating material was fabricated with quartzite, ordinary portland cement(OPC), lime and anhydrous gypsum. After characteristic analysis of slurry, the optimum mixing ratio was derived with different $CaO/SiO_2$ mole ratio. Based on derived mixing ratio, the inorganic insulating material was fabricated at different water content and hydrothermal synthesis conditions. Specific gravity was $0.26g/cm^3$, compressive strength was 0.4 MPa, and thermal conductivity was 0.064 W/mK. This properties were enhanced performance of conventional ALC (Autoclaved Lightweight Concrete). And it can replace organic insulation with harmless inorganic insulation through continues research and development.

A Study on the Performance of Deep learning-based Automatic Classification of Forest Plants: A Comparison of Data Collection Methods (데이터 수집방법에 따른 딥러닝 기반 산림수종 자동분류 정확도 변화에 관한 연구)

  • Kim, Bomi;Woo, Heesung;Park, Joowon
    • Journal of Korean Society of Forest Science
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    • v.109 no.1
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    • pp.23-30
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    • 2020
  • The use of increased computing power, machine learning, and deep learning techniques have dramatically increased in various sectors. In particular, image detection algorithms are broadly used in forestry and remote sensing areas to identify forest types and tree species. However, in South Korea, machine learning has rarely, if ever, been applied in forestry image detection, especially to classify tree species. This study integrates the application of machine learning and forest image detection; specifically, we compared the ability of two machine learning data collection methods, namely image data captured by forest experts (D1) and web-crawling (D2), to automate the classification of five trees species. In addition, two methods of characterization to train/test the system were investigated. The results indicated a significant difference in classification accuracy between D1 and D2: the classification accuracy of D1 was higher than that of D2. In order to increase the classification accuracy of D2, additional data filtering techniques were required to reduce the noise of uncensored image data.

Characterization of the high mannose asparagine-linked oligosaccharides synthesized by microfilariae of Dirofilaria immitis (심장사상충 자충이 합성한 high mannose asparagine-linked oligosaccharides의 분자화학적 분석)

  • 강승원
    • Parasites, Hosts and Diseases
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    • v.32 no.2
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    • pp.101-110
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    • 1994
  • This report describes the structures of high-mannose-type N-linked oligosaccharides in glycoproteins synthesized by the microfilariae of Diroflcrio immitis. Microfilariae of D. immitis were incubated in vitro in media containing 2-(3H) mannose to allow metabolic radiolabeling of the oligosaccharide moieties of newly synthesized glycoproteins. Glycopeptides were prepared from the radiolabeled glycoproteins by digestion with pronase and fractionation by chromatography on concanavalin A Sepharose. Thirty eight percent of 2- (3H) mannose incorporated into the microalariae of D. immitis glycopeptides was recovered in high mannose-type asparagine-linked oligosaccharides which were bound to the immobilized lectin. Upon treatment of 2-(3H) mannose labeled glycopeptides with endo - β- N- acetylglu co saminidase H , the high mannose type chains were released and their structures were determined by high performance liquid chromatography and exoglycosidase digestion. The major species of high mannose-type chains synthesized by microfilariae of D. immitis have the composition Man5GlcNAc2, Man6ClcNAc2, Man7GlcNAc2, and Man8GlcNAc2. Structural analyses indicate that these oligosaccharides are similar to high mannose-type chains synthesized by vertebrates.

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Identification and Characterization of a Novel Antioxidant Peptide from Bovine Skim Milk Fermented by Lactococcus lactis SL6

  • Kim, Sang Hoon;Lee, Ji Yoon;Balolong, Marilen P.;Kim, Jin-Eung;Paik, Hyun-Dong;Kang, Dae-Kyung
    • Food Science of Animal Resources
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    • v.37 no.3
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    • pp.402-409
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    • 2017
  • A novel peptide having free radical scavenging activity was separated, using an on-line high-performance liquid chromatography (HPLC) - ABTS screening method, from bovine skim milk fermented by Lactococcus lactis SL6 (KCTC 11865BP). It was further purified using reverse phase-HPLC (RP-HPLC) and sequenced by RP-HPLC-tandem mass spectrometry. The amino acid sequence of the identified peptide was determined to be Phe-Ser-Asp-Ile-Pro-Asn-Pro-Ile-Gly-Ser-Glu-Asn-Ser-Glu-Lys-Thr-Thr-Met-Pro-Leu-Trp (2,362 Da), which is corresponding to the C-terminal fragment of bovine ${\alpha}_{s1}$-casein (f179-199). The hydroxyl radicals scavenging activity ($IC_{50}$ $28.25{\pm}0.96{\mu}M$) of the peptide chemically synthesized based on the MS/MS data showed a slightly lower than that of the natural antioxidant Trolox ($IC_{50}$ $15.37{\pm}0.52{\mu}M$). Furthermore, derivatives of the antioxidant peptide were synthesized. The antioxidative activity of the derivatives whose all three proline residues replaced by alanine significantly decreased, whereas replacement of two proline residues in N-terminal region did not affect its antioxidative activity, indicating that $3^{rd}$ proline in C-terminal region is critical for the antioxidative activity of the peptide identified in this study. In addition, N-terminal region of the antioxidant peptide did not show its activity, whereas C-terminal region maintained antioxidative activity, suggesting that C-terminal region of the peptide is important for antioxidative activity.

Seismic characterization of cold formed steel pallet racks

  • Saravanan, M.;Marimuthu, V.;Prabha, P.;Surendran, M.;Palani, G.S.
    • Earthquakes and Structures
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    • v.7 no.6
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    • pp.955-967
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    • 2014
  • Storage racks are used worldwide in industries and commercial outlets due to the advantage of lighter, faster erection and easy alteration of pallet level as required. The studies to understand the behaviour of cold formed steel pallet racks, under seismic action is one of the emerging area of research. The rack consists of perforated uprights and beams with hook-in end connector, which enables the floor height adjustments. The dynamic characteristics of these racks are not well established. This paper presents the dynamic characteristics of 3-D single bay two storey pallet rack system with hook-in end connectors, which is tested on shake table. The sweep sine test and El Centro earthquake acceleration is used to evaluate the seismic performance of the cold formed steel pallet racks. Also an attempt is made to evaluate the realistic dynamic characteristics by using STAAD Pro software. Modal analysis is performed by incorporating the effective moment of inertia of the upright, which considers the effect of presence of perforations and rotational stiffness of the beam-to-upright connection to determine the realistic fundamental frequency of pallet racks, which is required for carrying out the seismic design. Finite element model of the perforated upright section has been developed as a cantilever beam through which effective moment of inertia is evaluated. The stiffness of the hook-in connector is taken from the previous study by Prabha et al. (2010). The results from modal analysis are in good agreement with the respective experimental results.