• Title/Summary/Keyword: paste materials

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A Study on the Evaluation Methods of Residual Flux Cleaning Ability by Alternative Semi-Aqueous Cleaners Using Metal Test Tools After Soldering with Solder Paste (솔더페이스트로 솔더링 후 잔류 플럭스 오염물에 대한 준수계 세정제의 금속치구를 이용한 세정성능 평가방법 연구)

  • Lee, Dong-Kee
    • Clean Technology
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    • v.14 no.2
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    • pp.103-109
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    • 2008
  • In this study, in order to develop evaluation method of the cleaning efficiency of residual flux which remains on the surface after soldering with solder paste, a specially designed metal tool is used to reduce spread uncertainty of flux while soldering. Using this tool, the measurement of cleaning efficiency of flux after soldering for some typical alternative semi-aqueous cleaners and 1,1,1-TCE by weighing method was conducted. As the test result of cleaning efficiency for each cleaner at several different cleaning times, the precision of the data is confirmed to within about 4% relative standard deviation (RSD) range. So, it is considered that this would be a good evaluation method for evaluating the cleaning efficiency of the residual flux which remains after solder paste soldering in the alternative cleaning. The results of this test method shows that the cleaning efficiency of ST 100SX and Neozal 750H in the cleaning of residual flux was better than other semi-aqueous cleaners, but its cleaning efficiency was clearly inferior to 1,1,1-TCE.

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Separation of Radionuclide from Dismantled Concrete Waste (해체 콘크리트 폐기물로부터 방사성핵종 분리)

  • Min, Byung-Youn;Park, Jung-Woo;Choi, Wang-Kyu;Lee, Kune-Woo
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.7 no.2
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    • pp.79-86
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    • 2009
  • Concrete materials in nuclear facilities may become contaminated or activated by various radionuclides through different mechanism. Decommissioning and dismantling of these facilities produce considerable quantities such as concrete structure, rubble. In this paper, the characteristics distribution of the radionuclide have been investigated for the effects of the heating and grinding test for aggregate size such as gravel, sand and paste from decommissioning of the TRIGA MARK II research reactor and uranium conversion plant. The experimental results showed that most of the radionuclide could be removed from the gravel, sand aggregate and concentrated into a paste. Especially, we found that the heating temperature played an important role in separating the radionuclide from the concrete waste. Contamination of concrete is mainly concentrated in the porous paste and not in the dense aggregate such as the gravel and sand. The volume reduction rate could be achieved about 80% of activated concrete waste and about 75% of dismantled concrete waste generated from UCP.

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Discoloration of teeth due to different intracanal medicaments

  • Afkhami, Farzaneh;Elahy, Sadaf;Nahavandi, Alireza Mahmoudi;Kharazifard, Mohamad Javad;Sooratgar, Aidin
    • Restorative Dentistry and Endodontics
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    • v.44 no.1
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    • pp.10.1-10.11
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    • 2019
  • Objectives: The objective of this study was to assess coronal discoloration induced by the following intracanal medicaments: calcium hydroxide (CH), a mixture of CH paste and chlorhexidine gel (CH/CHX), and triple antibiotic paste (3Mix). Materials and Methods: Seventy extracted single-canal teeth were selected. Access cavities were prepared and each canal was instrumented with a rotary ProTaper system. The specimens were randomly assigned to CH, CH/CHX, and 3Mix paste experimental groups (n = 20 each) or a control group (n = 10). Each experimental group was randomly divided into 2 subgroups (A and B). In subgroup A, medicaments were only applied to the root canals, while in subgroup B, the root canals were completely filled with medicaments and a cotton pellet dipped in medicament was also placed in the pulp chamber. Spectrophotometric readings were obtained from the mid-buccal surface of the tooth crowns immediately after placing the medicaments (T1) and at 1 week (T2), 1 month (T3), and 3 months (T4) after filling. The ${\Delta}E$ was then calculated. Data were analyzed using 2-way analysis of variance (ANOVA), 3-way ANOVA, and the $Scheff{\acute{e}}$ post hoc test. Results: The greatest color change (${\Delta}E$) was observed at 3 months (p < 0.0001) and in 3Mix subgroup B (p = 0.0057). No significant color change occurred in the CH (p = 0.7865) or CH/CHX (p = 0.1367) groups over time, but the 3Mix group showed a significant ${\Delta}E$ (p = 0.0164). Conclusion: Intracanal medicaments may induce tooth discoloration. Use of 3Mix must be short and it must be carefully applied only to the root canals; the access cavity should be thoroughly cleaned afterwards.

Choice of resin cement shades for a high-translucency zirconia product to mask dark, discolored or metal substrates

  • Dai, Shiqi;Chen, Chen;Tang, Mo;Chen, Ying;Yang, Lu;He, Feng;Chen, Bingzhuo;Xie, Haifeng
    • The Journal of Advanced Prosthodontics
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    • v.11 no.5
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    • pp.286-296
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    • 2019
  • PURPOSE. The aim was to study the masking ability of high-translucency monolithic zirconia and provide guidance in selecting resin luting cements in order to mask discolored substrates. MATERIALS AND METHODS. 160 high-translucency zirconia specimens were divided into 32 groups depending on their thickness and shades. Using five shades of try-in paste, the specimens were luted onto the substrates (Co-Cr, precious-metal, opaque porcelain-sintered Co-Cr, opaque porcelain-sintered precious-metal, and 5M3-shade zirconia). All CIELAB color parameters were measured and statistically analyzed. RESULTS. Zirconia shade and thickness and try-in paste shade affected CIELAB color parameters (P=.000) in different substrates groups, and there were interactions among these factors (P=.000). All five try-in paste shades can be chosen to achieve ${\Delta}E$ values of zirconia with 1.2 - 1.5 mm for masking dark-tooth-like 5M3-shade and zirconia with 1.5 mm for masking precious-metal groups < 2.6. Only suitable try-in paste shades were used, can ${\Delta}E$ values that less than 2.6 be achieved when applied translucent monolithic zirconia with 0.7-1.0 mm for masking dark-tooth-like 5M3-shade and zirconia with 0.7 - 1.2 mm for masking precious-metal groups. CONCLUSION. Choosing suitable resin cement shades is necessary for high-translucency monolithic zirconia to achieve ideal masking ability (${\Delta}E$ < 2.6) on the dark-tooth.

Evaluation on the Mechanical Performance and Microstructure of Cement Pastes Using Carbon Nanotube (탄소나노튜브 적용 시멘트 페이스트의 역학적 성능 및 미세구조 평가)

  • Chae-Ik, Lim;Se-Ho, Park;Won-Woo, Kim;Jae-Heum, Moon;Seung-Tae, Lee
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.10 no.4
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    • pp.489-497
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    • 2022
  • In this study, the fluidity, mechanical properties and microstructure of cement pastes with carbon nanotube (CNT) were experimentally investigated. The 6 types of cement paste mixes with different PCE:CNT and w/b had been manufactured, and several tests including flow, compressive strength, absorption and water porosity were performed on cement pastes with or without CNT.Additionally, microstructural observations such as x-ray diffraction (XRD) and scanning electron microscopy (SEM) were carried out to examine hydrates formed in cement paste with CNT. As a result, it was found that the performance of cement pastes with CNT was better compared to that of control cement paste (OPC) due to both of hydration acceleration effect and filling effect. Furthermore, the SEM images clearly showed that CNT can bridge cracks formed in cement matrix. Conclusively, it is believed that the CNT, if mixed appropriately, could be an option as nono-materials to improve performance of concrete structures.

A Study on the Properties of the Confined water ratio for Binder type and Replacement ratio (결합재의 종류 및 치환율에 따른 구속수비의 특성에 관한 연구)

  • Kwon Yeong-Ho;Lee Hyun-Ho;Lee Hwa-Jin;Ha Jae-Dam
    • Proceedings of the Korea Concrete Institute Conference
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    • 2004.05a
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    • pp.584-587
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    • 2004
  • This research investigates the rheological behavior and the confined water ratio of the cement paste and binder condition in order to predict mix design proportion of the high flowing concrete. The purpose of this study is to determine the optimum replacement ratio of binders including fly ash, and lime stone powder by the cement weight. For this purpose, belite cement, blast furnace slag cement and ordinary portland cement are selected. As test results, the confined water ratio shows the following range ; OPC>blast furnace slag cement>belite cement. Therefore, belite cement is proved very excellent cementitious materials in a view point of the flowability. The optimum replacement ratio of lime stone powder is shown over $30\%$ in case of belite cement and about $10\%$ in case of slag cement type. Also, the optimum replacement ratio of fly ash is shown $30\%$ by the cement weight considering the confined water ratio and deformable coefficient of the paste condition.

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Viscoelastic Properties of Fresh Cement Paste to Study the Flow Behavior

  • Choi, Myoungsung;Park, Kyoungsoo;Oh, Taekeun
    • International Journal of Concrete Structures and Materials
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    • v.10 no.sup3
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    • pp.65-74
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    • 2016
  • During concrete pumping, the migration and redistribution of particles occur in a pipe and the lubrication layer that forms between the bulk concrete and the pipe wall is the governing factor determining the flow behavior. In order to identify flow behavior of pumping, in this study, the viscoelastic properties related to the microstructural behavior of a flocculated suspension were examined by using dynamic oscillatory measurements. Cement paste is assumed to be a constituent material of the lubrication layer and ten cases of mixing design are employed by changing the proportions of mineral admixtures. The relationship between the yield stress obtained from the steady shear test and the dynamic modulus resulted from the oscillatory shear measurement was derived and the implications of the correlation are discussed. Moreover, based on the investigation of the viscoelastic properties with oscillatory measurements, the initial behavior of pumped concrete was analyzed systematically.

The effect of fly ash/slag on the property of reactive powder mortar designed by using Fuller's ideal curve and error function

  • Hwang, C.L.;Hsieh, S.L.
    • Computers and Concrete
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    • v.4 no.6
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    • pp.425-436
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    • 2007
  • This study is mainly focused on applying Fuller's ideal gradation curve to theoretically design blended ratio of all solid materials of a reactive powder mortar (RPM), also known as reactive powder concrete (RPC), with the aid of error function, and then to study the effect of fly ash/slag on the performance of RPM. The solid particle is assumed to be spherical particles. Then, the void volume of paste ($V_{\nu}$) and the paste content with specific quality can be obtained. As conclusion, under Fuller's ideal grading curve, the amount of fly ash/slag mixture is higher than that with silica fume along due to it better filled the void within solid particle and obtains higher packing density.

A study on plating conditions and characteristics of Sn layers as inserted metals for electronic component (전자부품의 접합재료로서의 Sn도금막 형성 조건 및 도금막의 특성에 관한 연구)

  • ;;;Shuji Nakata
    • Electrical & Electronic Materials
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    • v.6 no.6
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    • pp.505-513
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    • 1993
  • 본 논문은 전자 부품의 Soldring기에 사용되는 접합제를 Flux를 포함한 Solder paste 대신에 도금막을 이용하기 위한 Sn 도금막 형성 프로세스를 검토한 것이다. 반도체 Device를 Packaging한 외부단자(lead frame)과 HIC상의 후막전극(Ag/Pd)과의 접합 및 PCB상의 Cu land와의 접합시에는 스크린 프린트에 의한 Solder Paste가 일반적으로 사용되고 있다. 본 논문은 Fluxless Soldering의 한수단으로 도금막을 lead상에 형성시켜 접합 재료로서의 형성 프로세스 및 도금막의 특성과 도금형성 Paramete와의 관련성을 실험적으로 검토한 것으로 전류밀도 200 A/m$^{2}$의 조건으로 형성한 Sn 도금막이 접합용으로 최적조건임을 밝혔다.

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Photolithographic Method of Patterning Barrier Ribs for PDP by Green Sheet

  • Park, Lee-Soon;Jang, Dong-Gyu;Hur, Young-June;Lee, Sung-Ho;Kim, Duck-Gon;Kwon, Young-Hwan
    • 한국정보디스플레이학회:학술대회논문집
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    • 2005.07b
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    • pp.1225-1228
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    • 2005
  • Barrier ribs in the plasma display panel(PDP) function to maintain the discharge space between the glass plates as well as to prevent optical crosstalk. Patterning of barrier ribs is one of unique processes for making PDP. In this work photosensitive barrier rib pastes were prepared by incorporating binder polymer, solvent, functional monomers photoinitiator, and barrier rib powder of which surface was treated with fumed silica particles. Study on the function of materials for the barrier rib paste were undertaken. After optimization of paste formulation and photolithographic process, it was found that photolithographic patterning of barrier ribs with photosensitive barrier rib green sheet could be used in the fabrication of high resolution PDP.

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