• Title/Summary/Keyword: particle variance

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Influence of inorganic composition and filler particle morphology on the mechanical properties of self-adhesive resin cements

  • Marina Rodrigues Santi ;Rodrigo Barros Esteves Lins;Beatriz Ometto Sahadi;Giovanna Correa Denucci;Gabriela Soffner ;Luis Roberto Marcondes Martins
    • Restorative Dentistry and Endodontics
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    • v.47 no.3
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    • pp.32.1-32.11
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    • 2022
  • Objectives: This study aimed to evaluate the influence of inorganic composition and filler particle morphology on the mechanical properties of different self-adhesive resin cements (SARCs). Materials and Methods: Three SARCs including RelyX Unicem-2 (RUN), Maxcem Elite (MAX), and Calibra Universal (CAL) were tested. Rectangular bar-shaped specimens were prepared for flexural strength (FS) and flexural modulus (FM) and determined by a 3-point bending test. The Knoop microhardness (KHN) and top/bottom microhardness ratio (%KHN) were conducted on the top and bottom faces of disc-shaped samples. Sorption (Wsp) and solubility (Wsl) were evaluated after 24 hours of water immersion. Filler morphology was analyzed by scanning electron microscopy and X-ray energy dispersive spectroscopy (EDS). FS, FM, %KHN, Wsp, Wsl, and EDS results were submitted to 1-way analysis of variance and Tukey's post-hoc test, and KHN also to paired t-test (α = 0.05). Results: SARC-CAL presented the highest FS value, and SARC-RUN presented the highest FM. SARC-MAX and RUN showed the lowest Wsp and Wsl values. KHN values decreased from top to bottom and the SARCs did not differ statistically. Also, all resin cements presented carbon, aluminum, and silica in their composition. SARC-MAX and RUN showed irregular and splintered particles while CAL presented small and regular size particles. Conclusions: A higher mechanical strength can be achieved by a reduced spread in grit size and the filler morphology can influence the KHN, as well as photoinitiators in the composition. Wsp and Wsl can be correlated with ions diffusion of inorganic particles.

Producing synthetic lightweight aggregates by treating waste TFT-LCD glass powder and reservoir sediments

  • Tang, Chao-Wei
    • Computers and Concrete
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    • v.13 no.3
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    • pp.325-342
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    • 2014
  • The use of lightweight aggregate (LWA) instead of ordinary aggregate may make lightweight aggregate concrete, which possesses many advantages such as lightweight, lower thermal conductivity, and better fire and seismic resistance. Recently the developments of LWA have been focused on using industrial wastes as raw materials to reduce the use of limited natural resources. In view of this, the intent of this study was to apply Taguchi optimization technique in determining process condition for producing synthetic LWA by incorporating waste thin film transition liquid crystal displays (TFT-LCD) glass powder with reservoir sediments. In the study the waste TFT-LCD glass cullet was used as an additive. It was incorporated with reservoir sediments to produce LWA. Taguchi method with an orthogonal array L16(45) and five controllable 4-level factors (i.e., cullet content, preheat temperature, preheat time, sintering temperature, and sintering time) was adopted. Then, in order to optimize the selected parameters, the analysis of variance method was used to explore the effects of the experimental factors on the performances (particle density, water absorption, bloating ratio, and loss of ignition) of the produced LWA. The results showed that it is possible to produce high performance LWA by incorporating waste TFT-LCD glass cullet with reservoir sediments. Moreover, Taguchi method is a promising approach for optimizing process condition of synthetic LWA using recycled glass cullet and reservoir sediments and it significantly reduces the number of tests.

Computation of Transmissivity and Signal Loss in Inhomogeneous Complex Media (불균일 복합매질의 투과도 및 신호감쇄량 계산)

  • 김채영;정종철
    • Journal of the Korea Institute of Military Science and Technology
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    • v.2 no.1
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    • pp.30-37
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    • 1999
  • Transmissivity and the signal loss in soil are computed. An electric field expression for the inhomogeneous complex media modelled by two layers is shown as an integral form. Volume scattering occurs in inhomogeneous media, and iterative Born approximation is used to analyze this scattering effect. The degree of randomness is controlled by specifying the variance and correlation length. Expression for the transmissivity and the signal loss is presented as the parameter of soil moisture contents, soil particle radius, temperature and frequency. The analysis shows that big deviation in signal loss depends on the temperature variation remarkably and the physical reason of unusual level is explained.

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Analysis of Material Removal Rate of Glass in MR Polishing Using Multiple Regression Design (다중회귀분석을 이용한 BK7 글래스 MR Polishing 공정의 재료 제거 조건 분석)

  • Kim, Dong-Woo;Lee, Jung-Won;Cho, Myeong-Woo;Shin, Young-Jae
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.19 no.2
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    • pp.184-190
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    • 2010
  • Recently, the polishing process using magnetorheological fluids(MR fluids) has been focused as a new ultra-precision polishing technology for micro and optical parts such as aspheric lenses, etc. This method uses MR fluid as a polishing media which contains required micro abrasives. In the MR polishing process, the surface roughness and material removal rate of a workpiece are affected by the process parameters, such as the properties of used nonmagnetic abrasives(particle material, size, aspect ratio and density, etc.), rotating wheel speed, imposed magnetic flux density and feed rate, etc. The objective of this research is to predict MRR according to the polishing conditions based on the multiple regression analysis. Three polishing parameters such as wheel speed, feed rates and current value were optimized. For experimental works, an orthogonal array L27(313) was used based on DOE(Design of Experiments), and ANOVA(Analysis of Variance) was carried out. Finally, it was possible to recognize that the sequence of the factors affecting MRR correspond to feed rate, current and wheel speed, and to determine a combination of optimal polishing conditions.

Sensory Characteristics of Rice Confections by Descriptive Analysis (묘사분석을 이용한 쌀 과자의 관능적 특성 연구)

  • Jung, Daeun;Yang, Jeong Eun;Chung, Lana
    • Journal of the Korean Society of Food Culture
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    • v.31 no.1
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    • pp.105-110
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    • 2016
  • The objective of this study was to determine sensory profiles of rice confections. The samples used in this study obtained from Korea (traditional Korea rice snack and local specialty rice snack) and three countries (USA, Japan, and China) were evaluated and compared. The sensory characteristics of five kinds of rice confections were evaluated using a sensory test and were analyzed via quantitative description analysis (QDA), principal component analysis (PCA), and hierarchical cluster analysis (HCA). In the descriptive analysis, 10 trained panelists evaluated sensory characteristics consisting of 19 attributes, and there were significant differences (p<0.05) among the 16 characteristics. For the descriptive data, multivariate analysis of variance was carried out and identified differences among the samples. The PCA of rice confections for the first two principal components could explain 85.66% of the variations. The Korean, Japanese, and Chinese rice confections were savory, gritty, and particle-sized, the other Korean local specialty rice confections were fruity, sweet, honey-flavored, compact, and crispy, and those from the USA were glossy, grainy, bright, adhesive, cohesive, crispy, and sweet.

A Study on Filtration Performance Test with Electrostatically Enhanced Fabric Filter (정전형여과집진방식에서 여과특성에 관한 연구)

  • 천중국;박출재;최금찬
    • Journal of Korean Society for Atmospheric Environment
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    • v.11 no.4
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    • pp.361-367
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    • 1995
  • This study has been carried out to investigate the filteration performance of Electrostatically Stimulated Fabric Filter(ESFF) at high temperature condition. The electric field was maintained parallel to the fabric surface. The benefits of ESFF are lower residual pressure drop, improvement of fine particle removal efficiency and increasing reduced rate of pressure drop during a filteration cycle, stable operation at higher filtering velocities. According to the variance of filtering velocities and dust loadings, the results are summarized as follows; By imposing an electric field on the filter, the reduced rate of pressure drop was 7.sim.18% at room temperature, and when filtering velocity was 1.8m/min and dust loading was 1g/m$^{3}$, the value of reduced rate of pressure drop was shown the highest. Under the electric field around the filter, the reduced rate of pressure drop was 10.sim.35% at high temperature, and when filtering velocity was 1.8m/min and dust loading was 1g/m$^{3}$, the value of reduced rate of pressure drop was shown the highest. Most of all, at high temperature, the value of reduced rate of pressure drop was resulted to 25%. Also the collecting efficiency was shown clearly improved. By the SEM photo analysis, the number of penetrated particles at the Conventional Fabric Filter was approximately two times that of Electrostatically Stimulated Fabric Filter.

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Spalling Properties of High Performance Concrete Designed with the Various Blaine of Cement, Mineral Admixture Types and Fiber Contents (시멘트 입도, 혼화재 종류 및 PP섬유 혼입률 변화에 따른 고성능 콘크리트의 폭렬특성)

  • Song, Yong-Won;Shin, Jae-Kyung;Lee, Jae-Sam;Hann, Chang-Pyung;Yang, Seong-Hwan;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2006.11a
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    • pp.103-106
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    • 2006
  • This study investigates spalling properties of 60MPa class, high performance concrete, made with the various influential parameters, such as, blaine of cement, mineral admixture and polypropylene(PP) fiber contents. Totally 21 parameters of ${\phi}100{\times}200mm$ in size was fabricated; three specimens for variance in blaine of cement, 4 specimens for combination of mineral admixture type, along with 0.05, 0.1, 0.15% of fiber adding ratio. After that, one hour unloading fire test was conducted, and then spalling appearance and spalling degree of specimens was examined. Test showed that a specimen made with high blaine of cement(H) improved early strength but exhibited similar value to a specimen made with low blaine(L) at the age of 28 days, thus indicating comparable spalling appearance. In conclusion, spalling easily occur in higher strength and smaller particle shape of cement and mineral admixture.

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Comparison of Physicochemical Properties of Hard and Floury Type Rice Flour by Dry Heat Treatment (건열처리에 따른 경질미와 분질미 쌀가루의 이화학적 특성 비교)

  • Jung, Hee Nam
    • Journal of the Korean Society of Food Culture
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    • v.36 no.5
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    • pp.484-491
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    • 2021
  • This study investigated the effect of dry heat treatment (DHT) on the physicochemical properties of hard type (HR) and floury type (FR) rice to improve the processing aptitude of rice flour. The rice flour was heated at 130℃ for 0, 2 and 4 hours, and the color value, water absorption index (WAI), water soluble index (WSI), swelling power, solubility, pasting properties, particle shape and the X-ray diffraction were measured. After DHT, the L value of rice flour decreased, and the b value increased. The WAI, WSI, swelling power and solubility of HR and FR increased with the increase of treatment time. The cold viscosity and setback increased, while breakdown decreased. Cracks and lumps formed with fine particles were observed. The X-ray diffraction pattern was A-type, while the diffraction intensity decreased. According to the results of the two-way analysis of variance (ANOVA) test, the hydration and pasting properties were significantly different between HR and FR and were affected by DHT time. The results suggest that the properties of modified rice flour by DHT can be used in the food industry.

Cultivation of Sparassis crispa on Several kinds of Medium Density and Particle Size of Sawdust-based Medium Made of Larix kaempferi (낙엽송 톱밥배지 밀도 및 입자크기에 따른 꽃송이버섯의 재배특성)

  • Park, Hyun;Ryu, Sung-Ryul;Ka, Kang-Hyeon
    • Journal of the Korean Wood Science and Technology
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    • v.39 no.1
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    • pp.68-74
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    • 2011
  • Cauliflower mushroom ($Sparassis$ $crispa$) is being cultivated as a functional mushroom since the mushroom contains larger amount of ${\beta}$-glucan than other edible or medicinal mushrooms. In this study, as a fundamental study for the cultivation process of cauliflower mushroom, we assayed the mycelial growth and the productivity of the mushroom cultivated on the sawdust-based medium made of larch ($Larix$ $kaempferi$) by 4 kinds of medium densities and 6 kinds of particle sizes. Low densities of sawdust-based media (0.68~0.72 g/$cm^3$) showed high variations in mycelial growth at early stage on sawdust-based medium. The coefficient of variance for the mycelial growth decreased from higher than 40% at the 3rd week to lower than 10% at the 7th week. High density of sawdust-based medium (0.80 g/$cm^3$) showed relatively lower variation in the mycelial growth at early stage with less than 30% of coefficient of variance, the high density of sawdust-based medium was thought to be quite stable compared to the lower densities of sawdust-based medium. From the viewpoint of mushroom productivity especially for the goods (excluding bottom of fruiting body), 0.76 g/$cm^3$ was better than any other densities; the return rates of fruiting body from each medium were 12.2, 13.6, 13.1, and 12.0% for 0.80, 0.76, 0.72, and 0.68 g/$cm^3$, respectively. By the way, it took about 40 days for harvesting from primordium formation with the sawdust-based medium excluded the particles less than 1 mm, while it took about 70 days with the medium including the particles less than 1 mm. The yield from the sawdust-based medium with the particles less than 1 mm was also quite less than any other sawdust-based medium especially for the goods. Therefore, we recommend that the sawdust-based medium with larch for the cultivation of cauliflower mushroom be prepared as 0.76 g/$cm^3$ in medium density with excluding the particles less than 1 mm.

Density Estimation Technique for Effective Representation of Light In-scattering (빛의 내부산란의 효과적인 표현을 위한 밀도 추정기법)

  • Min, Seung-Ki;Ihm, In-Sung
    • Journal of the Korea Computer Graphics Society
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    • v.16 no.1
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    • pp.9-20
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    • 2010
  • In order to visualize participating media in 3D space, they usually calculate the incoming radiance by subdividing the ray path into small subintervals, and accumulating their respective light energy due to direct illumination, scattering, absorption, and emission. Among these light phenomena, scattering behaves in very complicated manner in 3D space, often requiring a great deal of simulation efforts. To effectively simulate the light scattering effect, several approximation techniques have been proposed. Volume photon mapping takes a simple approach where the light scattering phenomenon is represented in volume photon map through a stochastic simulation, and the stored information is explored in the rendering stage. While effective, this method has a problem that the number of necessary photons increases very fast when a higher variance reduction is needed. In an attempt to resolve such problem, we propose a different approach for rendering particle-based volume data where kernel smoothing, one of several density estimation methods, is explored to represent and reconstruct the light in-scattering effect. The effectiveness of the presented technique is demonstrated with several examples of volume data.