• Title/Summary/Keyword: optimum condition of preparation

Search Result 215, Processing Time 0.032 seconds

Preparation of BaTiO3 Powder in $BaO2-TiO2-Reduction Agent-PSCA (Particle Size Control Agent) System by SHS and Its Dielectric Properties (B3O2-TiO2-환원제-입자제어제계에서 자전연소합성법에 의한 BaTiO3분말의 제조 및 유전특성)

  • Yun, Ki-Seok;Lim, Sung-Jae;Nersisyan, Hayk;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
    • /
    • v.41 no.11
    • /
    • pp.842-850
    • /
    • 2004
  • We have investigated on the preparation of BaTiO$_3$ powder at the system of BaO$_2$-TiO$_2$-Reduction ag.-PSCA by SHS. C and Mg were used as reduction agent, and NaCl was used as PSCA (Particle Size Control Agent). The effects of the various reduction agent and its concentration, particle size control agent, reaction mixture mass on the product in the preparation of BaTiO$_3$ powder at the optimum system by SHS were investigated. The optimum conditions for reaction system and composition were BaO$_2$+TiO$_2$+0.11 Mg +0.2C+0.75NaCl in the As atmosphere. NaCl as PSCA showed the effect of controlling the particle size of product as well as the combustion temperature. The particle size of BaTiO$_3$ synthesized at the optimum condition was about 0.5 ${\mu}{\textrm}{m}$. And as the mixture mass for the reaction was increased, the more stable combustion wave appeared. We have conducted the sintering experiment at the temperature of 130$0^{\circ}C$, the time of 2 h and the atmosphere of air to measure the dielectric properties of BaTiO$_3$ synthesised in this work, and the sample sintered in this condition showed 2,290 of dielectric constant at 10$0^{\circ}C$ and 13,890 at curie point (129$^{\circ}C$).

A Study on Bending Fatigue Strength of One Side Fillet Welded T-Joint by SM 490A steel (Sm 490A강으로 제작된 T형 편면용접이음재의 굽힘피로강동에 관한 연구)

  • 엄동석;강성원;이태훈;이해우;조수형
    • Journal of Welding and Joining
    • /
    • v.16 no.5
    • /
    • pp.134-141
    • /
    • 1998
  • In this study, a fillet size for bending fatigue strength of one side fillet welded T-joint, used in box type girder and other welding structure, was investigated by bending fatigue test with or without edge preparation and burn through, with variation of joint shape. As a result, the following conclusions were obtained. (1) In one side fillet welded T-joint, the larger the leg length, the greater the bending fatigue strength. The increase in bending fatigue strength. (2) One side filet welded T-joint with edge preparation showed higher bending fatigue strength than that with twofold-large leg length and without edge preparation. (3) In one side fillet welded T-joint without edge preparation, both manual welding and automatic welding were carried out with same condition. In this case, automatic welding shoed deeper penetration and more increased horizontal leg length than manual welding, so that automatic welding offers grater bending fatigue strength. (4) For one side fillet welded T-joint without edge preparation, the ratio(h/t) of the leg length (h) and the main plate thickness (t) in which toe crack can occur was 1.2 over. (5) In one side fillet welded T-joint with edge preparation, the burn through led to reduced bending fatigue strength. However, this bending fatigue strength was higher than that of one side fillet welded T-joint without edge preparation and with a larger leg length.

  • PDF

Optimum Soaking Condition of Raw Soybean for Meju Preparation (메주 제조를 위한 원료 대두의 최적 침지 조건)

  • Im, Moo-Hyeog;Choi, Jong-Dong;Chung, Hyun-Chae;Choi, Choeng;Choi, Kwang-Soo
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.27 no.4
    • /
    • pp.664-667
    • /
    • 1998
  • In order to establish scientific foundations for the production of meju, optimum soaking conditions of raw soybean were investigated. 100% hydration of raw soybean by soaking conditions were observed in 17 hrs at 5$^{\circ}C$, 15 hrs at 1$0^{\circ}C$, 11 hrs at 15$^{\circ}C$, 9 hrs at 2$0^{\circ}C$, 7 hrs $25^{\circ}C$, 5 hrs 3$0^{\circ}C$, 4 hrs at 4$0^{\circ}C$ and 3 hrs at 5$0^{\circ}C$. Exudation amounts of total free amino acids and free sugars were the least when soybean was soaked for 2$0^{\circ}C$ for 9 hours.

  • PDF

Cu2ZnSnSe4 Thin Films Preparation by Pulsed Laser Deposition Using Powder Compacted Target

  • Kim, Kyoo-Ho;Wibowo, Rachmat Adhi;Alfaruqi, M.Hilmy;Ahn, Jong-Heon
    • Journal of the Korean institute of surface engineering
    • /
    • v.44 no.5
    • /
    • pp.185-189
    • /
    • 2011
  • $Cu_2ZnSnSe_4$ thin films for solar absorber application were prepared by pulsed laser deposition of a synthesized $Cu_2ZnSnSe_4$ compound target. The film's composition revealed that the deposited films possess an identical composition with the target material. Further film compositional control toward a stoichiometric composition was performed by optimizing substrate temperature, deposition time and target rotational speed. At the optimum condition, X-ray diffraction patterns of films showed that the films demonstrated polycrystalline stannite single phase with a high degree of (112) preferred orientation. The absorption coefficient of $Cu_2ZnSnSe_4$ thin films were above 104 cm.1 with a band gap of 1.45 eV. At an optimum condition, films were identified as a p type semiconductor characteristic with a resistivity as low as $10^{-1}{\Omega}cm$ and a carrier concentration in the order of $10^{17}cm^{-3}$.

Effects of Setting on the Gelation Characteristics of Frozen Mackerel Surimi Prepared by Alkaline Washing under Reduced Pressure (Setting조건이 감압 알칼리수세하여 제조한 고등어 냉동 Surimi의 Gel화 특성에 미치는 영향)

  • Park, Hyung-Sun;Park, Sang-Woo;Yang, Seung-Taek
    • Korean Journal of Food Science and Technology
    • /
    • v.30 no.5
    • /
    • pp.1152-1157
    • /
    • 1998
  • In this study, an attempt was made to obtain the optimum setting condition of frozen mackerel surimi prepared from alkaline washing under atmospheric, 660 and 560 mmHg pressure. Mackerel surimi were incubated at 15, 25, 35 and $45^{\circ}C$ for 2, 4, 6, 8 and 10 hr, respectively, followed by heating at $90^{\circ}C$ for 25 min to be cooked gel. The qualities of surimi gels were examined by analyzing the transglutaminase (TGase) activity, gel strength and scanning electron microscopy (SEM). For the preparation of mackerel surimi gel, optimum condition of setting was incubation at $35^{\circ}C$ for 6 hr.

  • PDF

A Study for Preparation of Nano Ethosome Loaded with Resveratrol (레스베라트롤을 함유한 나노 에토좀 제조에 관한 연구)

  • Seo, Dong Hoan;Yoon, Jong Hyuk;Kim, Youn Joon;Byun, Sang Yo
    • Journal of the Society of Cosmetic Scientists of Korea
    • /
    • v.41 no.2
    • /
    • pp.105-112
    • /
    • 2015
  • Resveratrol is a natural polyphenol. It protects skin from skin injury, ultraviolet radiation and pathogenic attack. This study is to find the optimum condition for the preparation of ethosome loading amount of resveratrol in ethosome. Ethosomes were prepared by modified hydrated liquid crystal method. Investigation of factors affecting the entrapment efficiency and particle size of ethosomes was carried out. The particle size of ethosome were measured by particle analyzer. The loading efficiency of resveratrol in ethosome was measured by HPLC. The particle sizes were 111.2 ~ 112.8 nm and the loading efficiency of resveratrol was 81.25 ~ 88.75%. The optimum conditions for the preparation of ethosome was obtained from of lecithin : resveratrol : cholesterol : ethanol at a weight ratio of 2.0 : 0.08 : 0.05 : 20.0.

Optimum Design of Rubber Injection Molding Process for the Preparation of Anti-vibration Rubber (방진고무사출성형의 적정설계)

  • Lim, Kwang-Hee
    • Korean Chemical Engineering Research
    • /
    • v.48 no.4
    • /
    • pp.490-498
    • /
    • 2010
  • The optimum mold design and the optimum process condition were constructed upon executing process simulation of rubber injection molding with the commercial CAE program of MOLDFLOW(Ver. 5.2) in order to solve the process-problems of K company relating to air-traps and short-shots. The former occurs at the cavity edge of torque-rod-bush and the latter takes place for the injection molding of dynamic dampers. As a result the process problem relating to air traps was solved by optimizing edge-angle and the number of gates to prevent the flow congestion of flow-front and to make the flow-front movement unaffected by congestion. For dynamic dampers of K company the unmolded flaw caused by their unfilled cavity was corrected by installing the air-vent at the confronting locations of both upstream and downstream of flow-front where air traps frequently occur. Besides the unmolded flaws were rectified by altering the position of gate from the upper to the middle or by increasing the number of gates. Thus the process problems of K company relating to air-traps and short-shots of torque-rod-bush and dynamic dampers, respectively, were solved by proper altering of mold design with process simulation of rubber injection molding.

The Investigation of Reaction Parameters on the Reactivity in the Preparation of SiC by SHS (자전연소합성법에 의한 SiC 분말 제조시 반응변수의 영향)

  • Shin, Chang-Yun;Won, Hyung-Il;Nersisyan, Hayk;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
    • /
    • v.43 no.7 s.290
    • /
    • pp.427-432
    • /
    • 2006
  • The preparation of SiC powder by SHS in the system of $SiO_2-Mg-C$ was investigated in this study. The effects of various processing parameters such as the initial pressure of inert gas in reactor, the content of Mg and C in mixture and the size of $SiO_2$ particles on the synthesis of SiC by SHS methode were investigated. The minimum initial pressure of inert gas in reactor for SHS reaction in this system was 5 atm, and as the pressure increased, and the concentration of unreacted Mg decreased. At 50 atm of the initial inert gas pressure in reactor, the optimum composition for the preparation of pure SiC was $SiO_2+2.5Mg+1.2C$. SiC powder synthesized in this condition had a mixture of ${\alpha}-SiC\;and\;{\beta}-SiC$ with an irregular shape and the particle size of $0.5{\sim}0.8{\mu}m$.

Optimization of Fermentation Condition for Onion Vinegar Using Acetobacter orientalis MAK88 (Acetobacter orientalis MAK88 균주를 이용한 양파 식초의 발효 최적화)

  • Lee, Jin-A;Lee, Sulhee;Park, Young-Seo
    • Food Engineering Progress
    • /
    • v.21 no.4
    • /
    • pp.403-408
    • /
    • 2017
  • Acetic acid bacteria strains were isolated from a variety of fermented foods and fallen fruits. Among them, the strain MAK88, whose acetic acid fermentation ability, acid-tolerance, and alcohol-tolerance were high, was selected and identified as Acetobacter orientalis. A seed culture of A. orientalis MAK88 was inoculated into onion juice, and the optimum conditions of acetic acid fermentation was investigated. The optimum initial concentration of ethanol in onion juice was 5% (v/v) and in that condition, acidity was 4.31% at 144 h of fermentation. The optimum initial concentration of acetic acid was 1% and the final acidity was 5.32%. The optimum fermentation temperature was determined to be $28^{\circ}C$. The most appropriate preparation method of onion juice was to heat the onion at $121^{\circ}C$ for 15 min and produce juice with pressure followed by filtering, and then sterilization at $121^{\circ}C$ for 15 min. Prepared onion juice was used for fermentation without dilution.

A Study on Stree Analysis and Bending Fatigue Strength of One Side Fillet Welded T-joint (T형 평면용접이음재의 응력해석과 굽힘피로강도에 관한 연구)

  • Gang, Seong-Won;Lee, Tae-Hun;Jeon, Jae-Mok;Kim, Chung-Hui
    • Journal of Ocean Engineering and Technology
    • /
    • v.13 no.2 s.32
    • /
    • pp.51-57
    • /
    • 1999
  • In this study, one side fillet welded T-joint, used in box type girder and other welding structure, was investigated by stress analysis and bending fatigue test without edge preparation, with variation of joint shape. The purpose of this study is to give the welding condiltion and design standard on manufacturing one side fillet welded T-joint. As a result, the following conclusions were obtained. 1) In one side fillet welded T-joint, the larger the leg length and the penetration depth, the greater the bending fatigue strength because reduction of stress and strain on toe and root. The increase of the longitudinal leg length rather than vertical leg length contributed to the increase in bending fatigue strength. 2) In one side fillet welded T-joint without edge preparation, both general manual welding and general automatic welding were carried out with same condition. In this case, automatic welding showed deeper penetration and more increased longitudinal leg length than manual welding, so that automatic welding offers greater bending fatigue strength. 3) For one side fillet welded T-joint without edge preparation with automatic welding, the ratio(h/t) of the leg length(h) and the main plate thickness(t) in which toe crake can occur was 1.0 over.

  • PDF