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EFFECT OF PH AND STORAGE TIME ON THE ELUTION OF RESIDUAL MONOMERS FROM POLYMERIZED COMPOSITE RESINS (산도변화와 침지시간이 광중합 복합레진의 잔류단량체 유출에 미치는 영향)

  • Jeon, Cheol-Min;Yoo, Hyun-Mi;Kwon, Hyuk-Choon
    • Restorative Dentistry and Endodontics
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    • v.29 no.3
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    • pp.249-266
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    • 2004
  • The purpose of this study was to determine whether pH and time has any influence on the degradation behavior of composite restoration by analyzing the leached monomers of dental composites qualitatively and quantitatively after storage in acetate buffer solution as a function of time using high performance liquid chromatography (HPLC) / mass spectrometer. Materials and Methods:Three commercial composite restorative resin materials (Z-250, Heliomolar and Aeliteflo) with different matrix structure and filler composition were studied. Thirty specimens (7mm $diameter{\times}2mm$ thick) of each material were prepared. The cured materials were stored in acetate buffer solution at different pH (4, 7) for 1, 7 and 45days. As a reference, samples of unpolymerized composite materials of each product were treated with methanol (10mg/ml). Identification of the various compounds was achieved by comparison of their mass spectra with those of reference compound, with literature data. and by their fragmentation patterns. Data were analysed statistically using ANOVA and Duncan's test. Results:1. Amounts of leached TEGDMA in Aeliteflo were significantly larger than those of UDMA in Z-250 and Heliomolar at experimental conditions of different storage time and pH variation (p<0.001). 2. As to comparison of the amounts of leached monomers per sorage time, amounts of leached TEGDMA in Aeliteflo and UDMA in Z-250 and Heliomolar were increased in the pH 4 solution more significantly than in the pH 7 solution after 1day, 7days and 45days, respectively (p<0.001). 3. In total amounts of all the leached monomers with storage times, the overall amounts of pH 4 extracts were larger than those of pH 7 extracts for all resin groups, but there was no significant difference (p>0.05).

Image Analysis Using Grid Suppression Software to Remove Moire Artifact from Micro Lesions of Sprague Dawley Rat (Sprague Dawley Rat의 미세병변에서 Moire Artifact를 제거하기 위한 Grid suppression software 사용 후 영상분석)

  • Lee, Sang-Ho
    • Journal of radiological science and technology
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    • v.40 no.4
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    • pp.575-580
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    • 2017
  • Because moire artifacts overlap with fine lesions and frequency bands, image processing software that removes moire artifacts can lead to loss of micro lesions. In this study, microscopic lesions such as microcalcification and microfracture were randomly formed on SD (Sprague Dawley) rats and image and optimized grid images were compared and analyzed using reference image and grid suppression software. The images were read by two consecutive radiologists using a McNemar's test. Among the 73 microcalcifications, in the 13 cases after grid suppression, the image of the optimized grid shows the loss of image in 3 cases, and the image after grid suppression shows statistically significant image loss (p=0.021). In all 53 fracture lines, there were 19 cases of image loss after the grid suppression, and only one case of the optimized grid showed no image loss. Therefore, the use of grid suppression software to remove moire artifacts should be carefully considered in the diagnosis of micro lesions.

Asbestos and Non-Asbestos Fiber Content in Lungs of Autopsied Subjects in Pohang with no Known History of Occupational Asbestos Exposure (포항지역 부검 폐조직에서 석면과 비석면 섬유농도에 관한 연구)

  • Lim, Hyun-Sul;Kim, Dong-Hoon;Sakai, Kiyoshi;Hisanaga, Naomi;Kim, Ji-Yong
    • Journal of Preventive Medicine and Public Health
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    • v.33 no.4
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    • pp.477-483
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    • 2000
  • Objectives : To obtain reference values for the pulmonary asbestos and non-asbestos fiber contents of residents in Korea and to compare them with similar results from Japan. Methods : The autopsied lung specimens from 22 deceased people (20 males and 2 females) in Pohang, without any known occupational history of asbestos exposure, were analyzed for incidence of asbestos and non-asbestos fibers by transmission electron microscopy with energy dispersive X-ray analysis after using low temperature ashing procedures. Results : Chrysotite fiber (46.2%) was the major fiber type found in the lungs of the subjects. The asbestos fiber concentrations found in males and females were $0.09\times10^6$ fiberss(g of dry lungs) and $0.30\times10^6$ fibers/(g of dry lungs), respectively, showing a geometric mean concentration $0.09\times10^6$ fibers/(g of dry lung tissue), due to the predominance of males in the sample. The non-asbestos fiber contents in males and females were $4.61\times10^6$ fibers/(g of dry lungs) and $17.79\times10^6$ fibers/(g of dry lungs), respectively, with a geometric mean concentration $5.21\times10^6$ fibers/(g of dry lung tissue). Conclusions : Residents in Pohang had significantly lower levels of both asbestos and non-asbestos fibers than urban residents in Korea. Furthermore, Koreans had significantly lower levels of both asbestos and non-asbestos fibers than Japanese.

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Analysis of Kinematic Parameters of Gait in Normal Subject (정상 성인의 운동 형상학적 보행 분석)

  • Jung, Hwa-Su
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.5
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    • pp.2989-2995
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    • 2014
  • This study was to performed to get the reference data of the kinematic parameters for normal subjects according to the arm movement type. Forty-five normal subjects participated in this study and preformed four sequence according to the arm movement type : normal arm movement, one arm movement, no arm movement, fitness arm movement. The study data was collected from June to August 2010. The kinematic data were measured using Vicon motion system 6MX3 cameras while each subjects walked through a 10m walkway. There were significant differences according arm movement type in the kinematic parameters such as range of motion (ROM) of the right pelvic, hip in sagittal plane, and ROM of the pelvic, hip, lumbar in coronal plane and ROM of the pelvic, thoracic, lumbar in transverse plane. This study can be utilized as the basic reference data in gait analysis for patients with pathologic gaits.

The Reference Model based on Web Services for USN Application Service (USN 응용 서비스를 위한 웹 서비스 기반의 참조 모델)

  • Bang, Jin-Suk;Kim, Yong-Woon;Yoo, Sang-Keun;Jung, Hoe-Kyung
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.12 no.5
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    • pp.948-955
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    • 2008
  • Recently, as the dissemination of the Internet and development of computer network technology, Research is actively underway for realization of the next-generation computing paradigm called Ubiquitous Computing. For realization of Ubiquitous computing, The data recognized from each sensors must be collected on real-time and transferred to applied service so that they may be used as data for providing service to users. However, there are several problem for realization. First, there is no standardization of sensor metadata, interface and event definition. Second, applied service has weak point that difficult of approaching to the data. Third, none interoperability with each platform and protocol. In this paper, we designed Sensor Service Description Language based on XML to resolve problem above. This Language expresses the measurement of the sensor and Service Metadata in the form to be standardized. In addition, we have proposed and development a reference model for USN application service.

Evaluation of Homogeneity and Stability of Korean Mussel (Mytilus coruscus) Standards for Cadmium Analysis (카드뮴 분석용 홍합(Mytilus coruscus) 표준물질의 균질성 및 안정성 시험평가)

  • Lee, Ha-Eun;Lee, Jangho;Chung, David;Lee, Soo Yong;Park, Ki-Wan;Shim, Kyu-Young
    • Journal of Environmental Science International
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    • v.28 no.11
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    • pp.1041-1045
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    • 2019
  • In this study, the KS A ISO Guide 35 was applied to develop analytical standards for heavy metal cadmium using the Korean mussel (Mytilus coruscus) and to evaluate the homogeneity and stability of the sample. Some of the crucial characteristics that reference materials must consist include homogeneity and stability of both intra- and inter-bottles. We tested homogeneity using ANOVA analysis and short-term stability using regression analysis. The variations of cadmium concentrations did not significantly differ between intra- and inter-bottles (F=0.41, p=0.90). For short-term stability verification, cadmium analysis results were not statistically significant as a result of the regression analysis (significance F=0.51, p=0.53). This suggests that we can not dismiss the null hypothesis that there is no significant variation in concentrations of cadmium over time. These results indicated that the cryogenic-milling process has statistically proven the short-term stability for materials from mussels in the chemical analysis of cadmium. Therefore, we propose that the Korean mussel's reference material developed for the proficiency test could be used as a tool to evaluate reliability and consistency in laboratories.

A Meta-Analysis of the Effect of Face (Chemyon) on Leisure Consumers' Consumption Behavior

  • KIM, Young-Doo
    • The Journal of Industrial Distribution & Business
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    • v.12 no.11
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    • pp.17-31
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    • 2021
  • Purpose: Despite the fact that face (i.e. Chemyon) is deeply-rooted in Korean culture and significantly affects the behavior of Korean people, the effect of face on leisure consumers' consumption behavior has only reported mixed findings, that is, significant and/or insignificant face effects have been reported. It is necessary to integrate prior research findings, and comprehensively examine the effect of face on leisure consumers' consumption behavior. The purpose of this study was to investigate the effect (i.e. effect size, and moderating variables) of face on leisure consumers' consumption behavior through meta-analysis. Research design, data and methodology: Among 1,019 face-related academic studies, retrieved from the academic research information services (RISS), 34 studies and 300 cases examining the effect of face on leisure consumers' consumption behavior were finally included for meta-analysis. Face measured as face sensitivity and/or a face sensitivity sub-component (shame-consciousness, formality-consciousness, and other-consciousness) were integrated in the meta-analysis. Leisure consumers' consumption behavior was classified as antecedents of purchase (overall conspicuous consumption tendency, overall symbolic consumption tendency, personality, high price, high quality, brand seeking, fashion seeking, enjoyment, other person (interpersonal) consideration, position, reference group, and attitude), purchase (purchase intention, unplanned purchase, purchase, and expenditure), and post-purchase (satisfaction, repurchase, and post-purchase). The data used in the meta-analysis was comprised of correlation coefficients, and the meta-analysis was performed using the R-program. Results: The overall mean effect size of face on leisure consumers' consumption behavior was .248. It was found that the effect size was the largest in the order of shame-consciousness face, formality-consciousness face, and other-consciousness face. Among the types of leisure consumers' consumption behavior categorized as dependent variables, the effect size was found to be largest in the order of position, attitude, reference group, post-purchase behavior, brand seeking, personality, trend seeking, etc. In addition, it was found that the leisure types moderated the effect size of face on leisure consumers' consumption behavior. The effect size was found to be largest in the order of skin diving, baseball, various leisure participation, dance, gambling, golf, etc. Conclusions: Face moderately or significantly influence leisure consumers' consumption behavior.

Evaluation of Punching Shear Safety of a Two-Way Void Plywood Slab System with Form (거푸집 패널이 부착된 2방향 중공슬래브의 뚫림 전단 안전성 평가)

  • Hur, Moo-Won;Woo, Hyung-Sik;Park, Jung-Min;Kang, Hyun-Wook;Park, Tae-Won
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.25 no.5
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    • pp.182-189
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    • 2021
  • VPS(Void Plywood Slab System, VPS) has optimized the shape of the hollow material. In addition, it has a function to prevent the floating of the hollow material and the separation due to the working load. In this study, the punching shear capacity of flat plate was performed using Void Plywood Slab System with form work panel proposed in the previous study. As a result of the test, the strength of the VSPS specimen in which the hollow material was placed beyond 2.0 times the column width from the loading point was reduced by 9.4% compared to the reference specimen. However, the strength value was about 1.57 times higher than the design value suggested by KBC 2016. It was found that there was no change in stiffness compared to the reference specimen until shear failure occurred in the VSPS specimen in which the hollow material was placed. It can be seen that this experiment is being destroyed by shear as the flexural reinforcing bars are sufficiently reinforced.

Remission of Progesterone-induced Diabetes Mellitus after Ovariohysterectomy in an Intact Female Dog

  • Kim, Ill-Hwa;Choi, Jin-Young;Hwang, Dae-Youn;Kang, Hyun-Gu
    • Journal of Veterinary Clinics
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    • v.36 no.1
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    • pp.74-77
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    • 2019
  • A 10-year-old, 8.28 kg, intact female Cocker Spaniel was presented with continuous polyuria and polydipsia. The dog had proestrus bleeding 5 weeks earlier, and hyperglycemia, glucosuria, ketouria, and high level of serum fructosamine in laboratory findings. Based on hyperglycemia, glucosuria, ketouria, and ketosis, the patient was tentatively diagnosed as diabetes mellitus (DM) with ketouria. After diagnosis, 5 to 7 U/body porcine lente insulin was administered during 11 days from initial presentation as the remission of DM for the dog. But, blood glucose was still high level. Because there was no reaction to porcine lente insulin, it was replaced by 4-10 U/body neutral protamine Hagedorn (NPH) during 3 days. But, NPH also did not regulate blood glucose level. Because insulin therapy failed to regulate blood glucose level, the dog was considering insulin-resistant diabetes. The dog was tentatively diagnosed with progesterone-resistant DM on the basis of the history that had revealed proestrus bleeding 5 weeks earlier. Progesterone level was moderate high (43.7 ng/ml; reference range, 15.0-90.0 ng/ml). Ovariohysterectomy (OHE) was performed to remove the cause of the dog's diabetes. After OHE 11 days, blood glucose was gradually declined by insulin treatment. Consequently, blood glucose was well controlled in reference range without insulin treatment after 2 months. This case is a report on progesterone-induced DM treated with OHE and insulin treatment during the diestrus.

Haptoglobin Concentration in the Cord Blood of Uninfected Korean Newborns

  • Choi, Seong Jin;Lee, Byoungkook;Ahn, Kwangjin;Uh, Young
    • Perinatology
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    • v.29 no.4
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    • pp.165-169
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    • 2018
  • Objective: Highly sensitive haptoglobin measurement should be used in neonates because the haptoglobin concentration in neonates is lower than that of adults. The aim of this study was to establish the reference values of haptoglobin levels in the cord blood of uninfected neonates. Methods: The cord blood of 29 preterm and 51 term babies was collected, and data from the mother and the newborn were recorded. The haptoglobin concentrations of 80 cord blood samples were simultaneously measured by enzyme-linked immunosorbent assay (ELISA; Assaypro, St Charles, MO, USA) and immunoturbidimetry assay (Roche Diagnostics, Basel, Switzerland). C-reactive protein (CRP) was also measured by immunoturbidimetry assay (Roche Diagnostics, Switzerland). Results: Mean values of CRP and ELISA haptoglobin were not significantly different between preterm and term babies. The 2.5 percentile and 97.5 percentile values of ELISA haptoglobin concentration were as follows: 80 neonates, 0.01 mg/dL and 0.59 mg/dL; 29 preterm babies, 0.08 mg/dL and 0.18 mg/dL; and 51 term babies, 0.07 mg/dL and 0.23 mg/dL. There were no differences in ELISA haptoglobin concentration according to maternal underlying diseases, delivery method, usage of antibiotics or steroids before delivery, gestational age, gender of baby, or twin gestation. Conclusion: A highly sensitive haptoglobin method should be used to determine the haptoglobin concentration in Korean newborns because the reference values of cord blood haptoglobin concentration in Korean newborns are less than the lower detection limit for commonly used immunoturbidimetric haptoglobin measurement methods.