• 제목/요약/키워드: nitration

검색결과 128건 처리시간 0.02초

환원판이 결합된 원통셸의 진동해석 (Vibration Analysis of Combined Cylindrical Shells with an Annular Plate)

  • 김영완;정강
    • 한국소음진동공학회논문집
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    • 제13권10호
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    • pp.767-776
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    • 2003
  • The theoretical method is developed to Investigate the nitration characteristics of the combined cylindrical shells with an annular plate joined to the shell at any arbitrary axial position. The structural coupling between shell and plate is simulated using two types of artificial springs a translational spring is introduced for translational coupling and a rotational spring is used for rotational coupling. The springs are continuously distributed along circumferential direction. Using the Rayleigh-Ritz method the natural frequencies and mode shapes of the combined shell with an annular plate examine. The effect of Inner-to-outer radius ratio, axial position of annular plate and length-to-radius ratio of shell on vibration characteristics of combined cylindrical shells is studied. The theoretical results are verified by comparison with FEM results.

Indoprofen의 합성 (Synthesis of Indoprofen)

  • 최홍대;강병원;마정주;윤호상
    • 약학회지
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    • 제35권4호
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    • pp.314-318
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    • 1991
  • A convenient method for the synthesis of indoprofen, which is a potent antiinflammatory agent, w described. Ethyl $\alpha$-(4-aminophenyl)propionate was prepared by nitration of ethyl $\alpha$-phenylpropionate, followed by reduction. Ethyl $\alpha$-[4-(1, 3-dioxo-2-iso-indolinyl)phenyl]propionate was obtained from condensation reaction of phthatic anhydride and ethyl $\alpha$-(4-aminophenyl)propionate. Indoprofen was prepared by reduction of ethyl $\alpha$-[3-(1, 3-dioxo-2-iso-indolinyl)phenyl]propionate with zinc dust-acetic acid, followed by hydrolysis of the resultant ethyl $\alpha$-[4-(1-oxo-2-iso-indolinyl)pheriyl]propionate.

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진동응답을 최소화하는 비구속형 제진보의 제진 부위 최적설계 (Optimal Treatment of Unconstrained Visco-elastic Damping Layer on Beam to Minimize Vibration Responses)

  • 이두호
    • 한국소음진동공학회논문집
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    • 제15권7호
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    • pp.829-835
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    • 2005
  • An optimization formulation of unconstrained damping treatment on beam is proposed to minimize vibration responses using a numerical search method. The fractional derivative model is combined with RUK's equivalent stiffness approach in order to represent nonlinearity of complex modulus of damping materials with frequency and temperature. Vibration responses are calculated by using the modal superposition principle, and of which design sensitivity formula with respect to damping layout is derived analytically. Plugging the sensitivity formula into optimization software, we can determine optimally damping treatment region that gives minimum forced response under a given boundary condition. A numerical example shows that the proposed method is very effective in suppressing nitration responses by means of unconstrained damping layer treatment.

Fresh 콘크리트의 초기 강도 증가를 고려한 진동규준치 제안 (Suggestion of Vibration Criteria for Fresh Concrete Considering Early Strength Increase)

  • 박선준;박연수;강성후;김홍기;김응록
    • 한국소음진동공학회논문집
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    • 제12권6호
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    • pp.453-460
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    • 2002
  • In this paper, vibration criteria for fresh concrete are suggested considering relationship of strength and ages of concrete. Vibration criteria of fresh concrete subjected to construction vibration are not to be certain in abroad countries without question within a country. Before 12 hours cured, vibration criterion is suggested 0.25 cm/s. Used 4.0 cm/s by vibration criterion after 28 days. And the interval extent used relation with strength and ages of concrete. Vibration criteria proposed in this paper are thought may satisfy properties of fresh concrete as well as generally used those in domestic. Also, the actual ground vibrations due to pile driving have been measured, and data are analyze using the nitration equation applying to reliability index.

정사각형 외팔보에서의 일대일 공진 (One to One Resonance on the Quadrangle Cantilever Beam)

  • 김명구;박철희;조종두
    • 한국소음진동공학회논문집
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    • 제15권7호
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    • pp.851-858
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    • 2005
  • The response characteristics of one to one resonance on the quadrangle cantilever beam in which basic harmonic excitations are applied by nonlinear coupled differential-integral equations are studied. This equations have 3-dimensional non-linearity of nonlinear inertia and nonlinear curvature. Galerkin and multi scale methods are used for theoretical approach to one-to-one internal resonance. Nonlinear response characteristics of 1st, 2nd, 3rd modes are measured from the experiment for basic harmonic excitation. From the experimental result, geometrical terms of non-linearity display light spring effect and these terms play an important role in the response characteristics of low frequency modes. Nonlinear nitration in the out of plane are also studied.

시일의 마멸로 인한 다단터빈펌프의 위험속도 변화

  • 김영철;이동환;이봉주
    • 유체기계공업학회:학술대회논문집
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    • 유체기계공업학회 1998년도 강연회 및 연구개발 발표회 논문집
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    • pp.203-209
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    • 1998
  • Rotordynamic analysis of a multistage turbine pump using finite element method is performed to investigate the effects of seal wear on Its system behavior. Stiffness and damping coefficients of the 2-axial grooved bearing are obtained as functions of rotating speed. Stiffness and damping coefficients of plane annular seals are calculated as functions of rotating speed as well as seal clearance. As the clearance of seals become larger, these stiffness and damping coefficients decrease drastically so that there can be significant changes in whirl natural frequencies and damping characteristics of the pump rotor system. Although a pump is designed to operate with a sufficient seperation margin from the 1st critical speed, seal wear due to long operation may cause a sudden increase in nitration amplitude by resonance shift and reduce seal damping capability.

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층별변위 유한요소법에 기초한 점탄성층을 갖는 원통형 복합적층 패널의 진동해석 (Vibration Analyses of Cylindrical Hybrid Panel with Viscoelastic Layer Based on Layerwise Finite Elements)

  • 오일권;성태홍
    • 한국소음진동공학회논문집
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    • 제15권12호
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    • pp.1361-1369
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    • 2005
  • Based on a full layerwise displacement shell theory, the nitration and damping characteristics of cylindrical sandwiched panels with viscoelastic layers are investigated. The transverse shear deformation and the normal strain of the cylindrical hybrid panels are fully taken into account for the structural damping modelling. The present finite element model Is formulated by using Hamilton's virtual work principle and the cylindrical curvature of hybrid panels is exactly modeled. Modal loss factors and frequency response functions are analyzed for various structural parameters of cylindrical sandwich panels. Present results show that the full layerwise finite element method can accurately predict the vibration and damping characteristics of the cylindrical hybrid panels with surface damping treatments and constrained layer damping.

치수공차가 고려된 광디스크 드라이브의 방진마운트 설계에 관한 연구 (A Study on the Design of Rubber Mount for Anti-vibration of an Optical Disk Drive Considering the Dimensional Tolerance)

  • 김국원;김남웅
    • 한국소음진동공학회논문집
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    • 제12권9호
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    • pp.661-667
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    • 2002
  • With the increase of storage density, high rotational speed and high access technologies in optical disk drive, mechanical issues, mainly noise and vibration, become critical. Up to now the researches of rubber mount for anti-vibration focused on how to calculate the static and the dynamic stiffness of rubber mount and loaned out consideration of the dimensional tolerance of rubber mount for anti-vibration. This paper presents the effects of dimensional tolerance of rubber mount for anti-nitration on the dynamic characteristics of optical disk drive by finite element analysis and dynamic test. The relation between dimensional tolerance and dynamic characteristics of optical disk drive is observed and discussed.

이민기를 포함하는 비스 또는 트리 크라운에테르의 합성 (V) (Syntheses Bis or Tri Crown Ethers Containing Imine Group(V))

  • 장승현;김정성
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2003년도 제5회 영호남 학술대회 논문집
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    • pp.110-113
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    • 2003
  • We report herein synthetic results obtained six new types of bis-benzocrown ethers containing imine group. Bis crown ethers l~3 are aminobenzo-15-crown-5-ether linked with terephthalaldehyde, isophthalaldehyde, phthaldehyde respectively by imine reaction. Bis crown ethers l~3 are different distances in each crown ether rings. Bis crown ether 4 has large cavity in crown ethers. Functionalized crown ether 5 is synthesized amonobenzo-l5-crown-5-ether and terephthaladehyde same ratio at one to one. Bis crown ether 6 has phothosensitive linkage between crown ethers. Bis crown ether 7 is prepared by amonobenzo-l5-crown-5-ether and triethyl ortho formate. 4'-Nitrobenzo-crown ethers and 3',4'-dinitrobenzo-crown ethers were prepared by nitration of benzo crown ethers, obtained from the reaction of catechol and oligoethylene glycol ditosylate. Crown ethers containing aldehyde group were synthesized from the reaction of 3,4-dihydroxybenzaldehyde and corresponding ditosylate respectively. The synthesized crown ethers were characterized respectively by IR, NMR. GC-Mass.

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Cr 및 Nb 복합탄화물에 의한 철계 MAG용접 오버fp이의 내마모 특성 (Wear Resistance Characteristics of Iron System MAG Weld Overlays with Chromium and Niobium Carbide Composite)

  • 김종철;박경채
    • Journal of Welding and Joining
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    • 제20권3호
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    • pp.54-59
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    • 2002
  • Overlays is a treatment of the surface and near-surface regions of a material to allow the surface to perform functions that are distinct from those frictions demanded far the bulk of the material. Welding, thermal spray, quenching, carburizing and nitration have been used as the surface treatment. Especially, weld overlay is a relatively thick layer of filler metal applied to a carbon or low-alloy steel base metal for the purpose of providing a wear resistant surface. In this study, weld overlay was performed by MAG welding on the base metal(SS400) with filler metal which contain composite powders($Cr_3C_2+Mn+Mo+NbC$) and solid wire(JIS-YGW11). Characteristics of hardness and wear resistance on overlays were analyzed by EDS, EPMA, XRD and microstructures. Carbide formations were $M(Cr, Fe)_7C_3$ and NbC phases. And carbide volume fraction, hardness and specific wear resistance of overlays were increased with increasing powder feed rate and decreasing wire fred rate. Hardness and wear resistance were almost proportioned to carbide volume fraction of overlay.