• Title/Summary/Keyword: morpology

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Measurement of Oxygen by FTIR in Silicon wafer process steps (실리콘 웨이퍼 공정스텝에서 FTIR에 의한 산소의 측정)

  • 김동수;정원채
    • Proceedings of the IEEK Conference
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    • 2000.06b
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    • pp.68-71
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    • 2000
  • In this paper, we have measured the oxygen contents by FTIR in silicon wafer various process technology(slicing, lapping, polishing). The measured data are also compared with the data of etching process(KOH, Bright etching). Also we have measured the surface morpology in backside silicon wafer after etching treatment and etch pit density due to OISF after 4 step high temperature annealing process with optical microscope.

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발정 주기에 따른 개 미성숙 난자의 핵발달단계의 비교

  • 이효상;윤희준;이영호;전세진;서영일;조수진;최유진;조성균;공일근
    • Proceedings of the KSAR Conference
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    • 2004.06a
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    • pp.241-241
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    • 2004
  • 본 연구는 발정주기에 따른 개의 미성숙난자의 체외배양 0시간째 핵의 발달단계를 비교ㆍ검토하였다. 발정주기가 다른 개의 난소를 적출 하여 항생제가 첨가된 38℃의 0.9% 생리식염수가 들어있는 보온병에 넣어 2시간 이내에 연구실로 운반하고 난소를 면도날로 세절하여 난포란을 회수하였고, 난구세포 제거 후 Chohan과 Hunter (2003) 방법에 준하여 10 ug/ml Hoechst 33342를 이용한 핵염색을 실시하여 핵의 모양을 판명하였다. 조사된 결과는 SAS 8.0 Package를 이용하여 통계분석을 실시하였다. (중략)

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Fabrication of Ultrathin Polyimide Films by LB Technique (LB법을 이용한 polyimide 초박막의 제작)

  • Kim, J.H.;Yoo, D.S.;Kim, Y.K.;Shon, B.C.;Kang, D.Y.
    • Proceedings of the KIEE Conference
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    • 1993.11a
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    • pp.174-177
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    • 1993
  • The polyimide films were prepared by imidizing the polyamic acid long-chain alkylamine (dimethylhexadecylamine) salt films with a thermal and chemical treatment, where the polyamic acid alkylamine salt film were formed on various substrates by using Langmuir-Blodgett (LB) method. The imidization of polyamic acid alkylamine salt films with various thickness were identified with FT-IR and UV-visible absorption spectroscopies. Atomic Force Microscopy (AFM) have been used to investigate the surface morpology of polyamic acid alkylamine salt and imidized films.

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Effects of the Stand-off Distance on the Weld Strength in Magnetic Pulse Welding (전자기펄스용접에서 용접강도에 미치는 접합간격의 영향)

  • Kim, Sung-Wook;Chun, Chang-Keun;Kim, Sook-Hwan
    • Journal of Welding and Joining
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    • v.26 no.6
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    • pp.48-53
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    • 2008
  • Although Magnetic Pulse Welding(MPW) is not a recently developed technique, it has gained the attention of the automotive industry. MPW has become an accepted welding process because it enables the joining of similar, and dissimilar materials, with a very short cycle time, without the need for filler metal and gases. In this study, the effect of the stand-off distance on the weld strength has been investigated. The compressive strength of the MPW joints was evaluated using UTM. The interface of weld, IMC composition and morpology were studied by SEM and EDS. It was concluded that the stand-off distance and the voltage are the main parameters influencing the strength of weld. In case of too high stand-off distance, it influenced harmful effect because of the resistance of deformation.

An Study on the Change of the critical J-value and the Fracture Morphology of the Vibration - Proof Natural Rubber due to Carbon Black (방진부품용 천연고무의 카본블랙에 의한 임계J값과 파단 모폴로지 변화에 관한 연구)

  • 김재훈;정현용;구병춘
    • Proceedings of the KSR Conference
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    • 2002.10a
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    • pp.72-79
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    • 2002
  • The effects of carbon black on the critical J-value and the surface fracture morpology of the carbon-black filled natural rubbers were investigated. Different kinds of carbon blacks resulted in different critical J-values, surface, and roughness. It was noticed that the critical J-value was almost the same regardless of the length of a pre-crack. In addition, different kinds of carbon blacks resulted in different fracture morphologies, and micro-scale and macro-scale roughnesses. The critical J-value could be linearly expressed by the micro-scale roughness and the macro-scale roughness and it seemed related to the size distribution of carbon black particles. And we also found that the macro-scale ms roughness was more sensitive than the micro-scale ms roughness to the critical J-value by the result of correlation coefficient, r$^2$.

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Oxidation Resistant SiC Coating for carbon/carbon Composites

  • Joo, Hyeok-Jong;Lee, Nam-Joo;Oh, In-Seok
    • Carbon letters
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    • v.4 no.1
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    • pp.24-30
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    • 2003
  • In this study, densified 4D carbon/carbon composites were made from carbon fiber and coal tar pitch through the process of pressure impregnation and carbonization and then followed by carbonization and graphitization. To improve the oxidative resistance of the prepared carbon/carbon composites, the surface of carbon/carbon composites was coated on SiC by the pack cementation method. The SiC coated layer was created by depending on the constitution of pack powder, and reaction time of pack-cementation. The morpology of crystalline and texture of these SiC coated carbon/carbon composites were investigated by XRD, SEM/EDS observation. So the coating mechanism of pack-cementation process was proposed. The oxidative res istance were observed through the air oxidation test, and then the optimal condition of pack cementation was found by them. Besides, the oxidative mechanism of SiC formed was proposed through the observation of SiC coated surface, which was undergone by oxidation test.

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A study of a-Si:H/c-Si interface properties by surface morphology of Si wafer in heterojunction solar cells (실리콘 기판의 표면 형상에 따른 실리콘 이종접합 태양전지의 a-Si:H/c-Si 계면 특성 연구)

  • Kang, Byung-Jun;Tark, Sung-Ju;Kang, Min-Gu;Kim, Chan-Seok;Lee, Jeong-Chul;Kim, Dong-Hwan
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.06a
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    • pp.92-92
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    • 2009
  • 실리콘 기판과 비정질 실리콘 박막 사이의 계면특성은 실리콘 이종접합 태양전지의 효율을 높이는데 있어서 중요한 요소이다. 이종접합 태양전지에서는 n형 실리콘 기판 위에 비정질 실리콘 막을 증착시키는데 이 때 비정질 실리콘 막이 증착되면서 (111)면과 (111)면이 만나는 조직화된 피라미드의 골 사이에서 부분적으로 실리콘의 에피층이 성장하게 된다. 이 에피층이 결정질 실리콘 기판과 비정질 실리콘 막 사이의 계면 특성을 떨어뜨려 이종접합 태양전지의 효율이 감소하게 된다. 본 연구에서는 n형 실리콘 기판을 이용한 고효율 실리콘 이종접합 태양전지 제작을 위하여 실리콘 기판의 조직화 상태를 다르게 하여 셀을 제작하였다. 이에 큰 피라미드 형상의 조직화된 기판 표면, 작은 피라미드 형상의 조직화된 기판 표면, 큰 피라미드 형상을 라운딩 시킨 기판 표면, 작은 피라미드 형상을 라운딩 시킨 기판 표면을 제작하여 기판 종류에 따른 이종접합 태양전지를 제작하여 특성을 비교 하였다.

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Effect of Layered Silicates on Flame retardant and Mechanical Properties of HDPF/$Mg(OH)_2$/Clay Nanocomposites (층상 실리케이트 첨가에 따른 HDPF/$Mg(OH)_2$/Clay 나노복합재의 특성연구)

  • Min, Kyung-Dae;Lee, Kyung-Yong;Lee, Ho-Lim;Kim, Do-Young;Kang, Seung-Hun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.260-260
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    • 2010
  • In recent years, polymer/clay nanocomposites have generated a great interest, both in industry and in academia, because they often exhibit remarkable improvement in material properties when compared with the virgin polymer or conventional micro and macro-composites. Among these properties are stiffness, strength, dimensional stability and permeability. [1-3] The dispersion of hydrophilic silicates in a hydrophobic matrix like Polyethylene (PE) is difficult because of the difference in character between PE and Montmorillonite (MMT). Therefore, it is necessary to modify PE with polar groups, which can increase the hydrophilicity of PE. In this study, High density polyethylene (HDPE)/$Mg(OH)_2$/Montmorillonite (MMT) nanocomposites having a various compositions were prepared by a melt blending technique with an internal mixer and properties namely mechanical, morpology, rheological and thermal properties were investigated

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Synthesis and Characterization of Di and Triblock Copolymers Containing a Naphthalene Unit for Polymer Electrolyte Membranes (고분자전해질 막을 위한 나프탈렌 단위를 포함하는 디 및 트리 블록공중합체의 합성 및 특성분석)

  • KIM, AERHAN
    • Journal of Hydrogen and New Energy
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    • v.27 no.6
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    • pp.660-669
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    • 2016
  • A fluorinated-sulfonated, hydrophobic-hydrophilic copolymer was planed subsequently synthesized using typical nucleophilic substitution polycondensation reaction. A novel AB and ABA (or BAB) block copolymers were synthesized using sBCPSBP (sulfonated 4,4'-bis[4-chlorophenyl)sulfonyl]-1,1'-biphenyl), DHN (1,5-dihydroxynaphthalene), DFBP (decafluorobiphenyl) and HFIP (4,4'-hexafluoroisopropylidenediphenol). All block copolymers were easily cast and made into clear films. The structure and synthesized copolymers and corresponding membranes were analyzed using GPC (gel permeation chromatography), $^1H$-NMR ($^1H$ nuclear magnetic resonance) and FT-IR (Fourier transform infrared). TGA (Thermogravimetric analysis) and DSC (differential scanning calorimetry) analysis showed that the prepared membranes were thermally stable, so that elevated temperature fuel cell operation would be possible. Hydrophobic/hydrophilic phase separation and clear ionic aggregate block morpology was confirmed in both triblock and diblock copolymer in AFM (atomic force microscopy), which may be highly related to their proton transport ability. A sulfonated BAB triblock copolymer membrane with an ion-exchange capacity (IEC) of 0.6 meq/g has a maximum ion conductivity of 40.3 mS/cm at $90^{\circ}C$ and 100% relative humidity.