• Title/Summary/Keyword: morphological characteristics of powder

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Effect of the Inert Ceramic Powder on the Electrical and Mechanical Properties of the Polymer Electrolytes (비활성 세라믹 분말이 고분자 전해질의 전기적, 기계적 특성에 미치는 영향)

  • Kim, Dong-Won;Park, Jung-Ki;Kim, Chang-Jung;No, Kwang-Soo
    • Korean Journal of Materials Research
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    • v.3 no.3
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    • pp.237-244
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    • 1993
  • The characteristics of composite polymer electrolytes obtained by adding a fine ceramic powder($\gamma-{LiAlO}_{2}$) with a diameter of $1{\mu}$m to a poly(ethylene oxide)/lithium trifluoromethane sulfonate (LiC$F_3$S$O_3$) complex are described in terms of morphological and mechanical behavior. The addition of uniformly dispersed ceramic powder greatly improves the electrical and mechanical properties of solid polymer electrolytes at ambient temperature. For the composite polymer electrolytes under this study, the optimum composition of the $\gamma-{LiAIO}_{2}$ in the composite for maximum ionic conductivity was found to be 20 wt%.

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ZnO Nanostructure Characteristics by VLS Synthesis (VLS 합성법을 이용한 ZnO 나노구조의 특성)

  • Choi, Yuri;Jung, Il Hyun
    • Applied Chemistry for Engineering
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    • v.20 no.6
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    • pp.617-621
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    • 2009
  • Zinc oxide (ZnO) nanorods were grown on the pre-oxidized silicon substrate with the assistance of Au and the fluorine-doped tin oxide (FTO) based on the catalysts by vapor-liquid-solid (VLS) synthesis. Two types of ZnO powder particle size, 20nm, $20{\mu}m$, were used as a source material, respectively The properties of the nanorods such as morphological characteristics, chemical composition and crystalline properties were examined by X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDX) and field-emission scanning electron microscope (FE-SEM). The particle size of ZnO source strongly affected the growth of ZnO nanostructures as well as the crystallographic structure. All the ZnO nanostructures are hexagonal and single crystal in nature. It is found that $1030^{\circ}C$ is a suitable optimum growth temperature and 20 nm is a optimum ZnO powder particle size. Nanorods were fabricated on the FTO deposition with large electronegativity and we found that the electric potential of nanorods rises as the ratio of current rises, there is direct relationship with the catalysts, Therefore, it was considered that Sn can be the alternative material of Au in the formation of ZnO nanostructures.

Morphological Characteristics and Material Comparison of Native Orostachys species (Orostachys japonica (Maxim.) A. Berger, Orostachys minuta (Kom.) A. Berger, Orostachys chongsunensis Y. N. Lee) (자생 바위솔(바위솔, 정선바위솔, 좀바위솔)의 형태적 특성과 성분 비교)

  • Jung, J.H.;Park, N.B.
    • Journal of Practical Agriculture & Fisheries Research
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    • v.21 no.2
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    • pp.5-13
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    • 2019
  • Orostachys species grow from anywhere in Korea. This variety, which lives in the harsh areas of the beach and mountains, is known to have as much change as it was isolated. It has been used as a medicine for a long time, and now the flower is beautiful and has been developed for horticulture. As a result of morphological characteristics and component analysis of three Orostachys species, the following results were obtained. 1. Orostachys species showed two types of leaves according to the growing environment. O. japonica (Maxim.) A. Berger and O. minuta (Kom.) A. Berger were lanceolate, and O. chongsunensis Y. N. Lee was obovate. 2. The leaves were all green. However, some of the O. japonica (Maxim.) A. Berger had white powder. Some of the O. minuta (Kom.) A. Berger was green with red spots on the back. O. chongsunensis Y. N. Lee showed strong gray before flowering but weak green when flowering. 3. The thorns of the leaves were O. japonica (Maxim.) A. Berger and O. minuta (Kom.), but O. chongsunensis Y. N. Lee was not. 4. Whether it was a leaf dot or not, there were dots in O. japonica (Maxim.) A. Berger and there were dots on the O. minuta (Kom.) and the O. chongsunensis Y. N. Lee. 5. The flowers were all white, and the stamens were red in O. japonica (Maxim.) A. Berger and O. minuta (Kom.) A. Berger and white in O. chongsunensis Y. N. Lee. 6. It was confirmed that the ingredients in Orostachys species contained kaempferol, quercetin, flavonoid etc., which have high antioxidant activity.

Material Characteristics of Ti-6Al-4V Alloy Manufactured by Electron Beam Melting for Orthopedic Implants (전자빔 용해 방법으로 제조된 정형외과 임플란트용 Ti-6Al-4V 합금의 재료 특성 분석)

  • Gang, Gwan-Su;Jeong, Yong-Hun;Jang, Tae-Gon;Yang, Jae-Ung;Jeong, Jae-Yeong;Park, Gwang-Min;U, Su-Heon;Park, Tae-Hyeon
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2018.06a
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    • pp.25-25
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    • 2018
  • Electron beam melting (EBM) is one of powder based additive manufacturing technology used to produce parts for high geometrical complexity and directly with three-dimensional computer aided design (CAD) model. It is kind of the most promising methods with additive manufacturing for a wide range of medical applications, such as orthopedic, dental implant, and etc. This research has been investigated the microstructure and mechanical properties of as fabricated and hot iso-static pressing (HIP) processed specimens, which are made by an Arcam A1 EBM system. The Ti-6Al-4V titanium alloy powder was used as a material for the 3 dimensional printing specimens. Mechanical properties were conducted with EBM manufacturing and computer numerical control (CNC) machining specimens, respectively. Surface morphological analysis was conducted by scanning electron microscopy (SEM) for their surface, dissected plan, and fractured surface after tensile test. The mechanical properties were included tensile stress-strain and nano-indentation test as a analysis level between nano and macro. As following highlighted results, the stress-strain curves on elastic region were almost similar between as fabricated and HIP processed while the ductile (plastic deformed region) properties were higher with HIP than that of as fabricated processed.

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Pharmacognostical Evaluation of Seed of Butea monosperma Kuntze

  • Srivastava, Manjoosha;Srivastava, Sharad Kumar;Khatoon, Sayyada;Rawat, A.K.S.;Mehrotra, Shanta
    • Natural Product Sciences
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    • v.8 no.3
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    • pp.83-89
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    • 2002
  • Butea monosperma Kuntze, commonly known as 'Palash', is employed in various indigenous systems of medicine against several diseases and almost every part of the plant has diversified medicinal properties. The seeds are used as anthelmintic, aperient, digesti and to treat piles, skin diseases and abdominal troubles. They also have the property of reducing 'Kapha' and 'Vata' (in Ayurveda). In the present paper a detailed pharmacognostical evaluation of seeds has been undertaken. The study includes macro- and micro-scopical details, fluorescence powder study and HPTLC fingerprinting. The seed is characterized by finely ridged seed coat and palisade-like malpighian cells, discontinuous transparent linea lucida in upper half of malpighian layer and simple & oblong hilum. The study also concludes that the seed samples procured from different places have similar morphological and physico-chemical characteristics. These observations are also supported by similar TLC profiles. The estimation of heavy metals (to detect permissible toxic limits), and fatty acid composition have been carried out. An attempt has also been made to see the ecological and edaphic variations, if any.

Isolation and Properties of Amino Acid Antimetabolite from Streptomyces sp. 182-27 (Streptomyces sp. 182-27 균주가 생산하는 아미노산 대사길항물질의 정제와 특성)

  • 박부길
    • Microbiology and Biotechnology Letters
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    • v.20 no.3
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    • pp.335-343
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    • 1992
  • A Streptomyces strain No. 182-27, which produced amino acid antimetabolite, was isolated from soil. During the course of screening for new amino acid antimetabolites from the culture broths of Actinomycetes, we found that the strain produced a substance active against Gram-positive bacteria and its activity was reversed by L-Ieucine on the synthetic minimal agar medium in the culture broth. The morphological and cultural characteristics serve to identify the producing organism strain 182-27 as the Streptomyces, although the species of this strain should be resolved in further studies. Fermentation was carried out in the synthetic medium at $28^{\circ}C$ for 78 hours. The fermentation yield reached about 2 mg per liter of the broth. Purification was done by ion exchange resin, active carbon, silica gel column chromatography and obtained 20 mg of pure active substance from the 20 $\ell$ culture broth. The 182-27 substance was obtained as white powder, mp 18SoC. From the physicochemical characteristics of the substance, it was amino acid like substance but unknown about its chemical structure. It is active against some Gram-positive bacteria and reversed by L-Ieucine.

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Preparation of Nickel Powders by the Reduction of Hydrazine from Diethanolamine Solutions (DEA 용액으로부터 히드라진의 환원 반응에 의한 니켈 분말 제조)

  • Choi, Eun-Young;Lee, Yoon-Bok;Yoon, Suk-Young;Kim, Kwang-Ho;Kim, Sin-Chun;Rhyim, Yaung-Mok;Kim, Hyong-Kuk;Kim, Ynng-Do
    • Journal of the Korean Ceramic Society
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    • v.42 no.6 s.277
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    • pp.432-436
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    • 2005
  • Nickel powders synthesized by the reduction of hydrazine of nickel salts fiom diethanolamine(DEA) solution, and investigated the morphological characteristics of nickel powders with the addition of hydrazine, reaction temperature, the composition of mixed solvents. The addition of hydrazine in DEA solution largely affected on size control of nickel powders. Under $N_2H_4/Ni^{2+}$ molar ratio= 1.5 and 2.0 conditions, spherical nickel powders in the submicron range obtained, owing to higher the reduction rate. An increase of temperature increased the size of nickel particles. At $220^{\circ}C$ for 40 min, the nickel powders composed of polyhedral particles with high crystalline in the submicron range. The mixed volume ratio of TEA to DEA affected on the increase of particle size and the inhibition of agglomerate between particles.

Preparation of Nickel Powders by the Reduction of Ni(OH)2 Reactant Slurries from Nonaqueous Media (비수용성 매질로부터 Ni(OH)2 반응슬러리의 환원반응에 의한 니켈 분말의 제조)

  • Choi Eun Young;Lee Yoon Bok;Yoon Suk Young;Kim Kwang Ho;Kim Jin Chun;Rhyim Young Mok;Kim Hyong Kuk;Kim Yang Do
    • Korean Journal of Materials Research
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    • v.15 no.5
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    • pp.334-339
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    • 2005
  • Nickel Powders were synthesized by the reduction of $Ni(OH)_2$ reactant slurries from nonaqueous media, and the morphological characteristics of nickel powders with the addition of NaOH, the composition of mixed solvents, reaction temperature and reaction time were investigated. The NaOH addition changed the structure of agglomeration in the submicron range. As the volume ratio of TEA to DEA increased, the powders slightly suppressed the agglomeration between particles and their size increased. The reaction temperature on size and shape of nickel powders was significant. As reaction time was shortened from 40 min to 0.3 min at $220^{\circ}C$, size distribution of nickel powders was transferred to a narrow size distribution owing to the presence of smaller particles with below $1.0\;{\mu}m$.

Production of Biopolymer Flocculant by Bacillus subtilis TB11

  • Yoon, Sang-Hong;Song, Jae-Kyeung;Go, Seung-Joo;Ryu, Jin-Chang
    • Journal of Microbiology and Biotechnology
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    • v.8 no.6
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    • pp.606-612
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    • 1998
  • A microbial flocculant-producing gram-positive bacterium, strain TE11, was isolated from soil samples, and was identified as Bacillus subtilis by using the Midi system, the Biolog system, 16S rDNA sequence analysis, and some physiological and morphological characteristics. The maximum flocculant capsular biopolymer of TE11 strain (BCP, 4.9mg/ml) was obtained when it was grown in GA broth medium containing 3% glutamic acid, 2% glycerol, 0.5% citric acid, 0.5% $NH_4$Cl, 0.05% $MgSO_4.7H_2O,\; 0.05%\;K_2HPO_4\;,\; and\; 0.004%\; FeC1_3. 6H_2O,\; pH 7.2,\; at\; 30^{\circ}C$ for 70 h with shaking. When glycerol was used as an additional carbon source in the GA medium, TE11 produced only flocculant BCP without any by-product. The flocculant (BCP) was found to aggregate suspended kaolin and activated charcoal powder without cations, and its flocculating activity was significantly enhanced by the addition of bivalent cations such as $Ca^{2+}.Zn^{2},\; and\; Mn^{2+}$. The flocculation activity by addition of $Ca^{2+}$ was high in an acidic pH 4.0. In the case of $Zn^{2+}$, high flocculating activity remained without significant loss in the broad range of pH 4.0 to 9.0.

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Studies on the Red Pigment Produced by Monascus sp. in Submerged Culture. Part I Isolation of Strain and Cultural Conditions of Pigment Produced (액침진탕 배양에 의한 Monascus sp..가 생산하는 적색색소에 관한 연구 제1보 균주의 분리 및 색소생산 배양 조건)

  • 김현수;김두현;양호석;변유량;유주현
    • Microbiology and Biotechnology Letters
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    • v.7 no.1
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    • pp.23-30
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    • 1979
  • Fungi which produce red pigment were isolated from tapioca chips, Korean Koji, air, and plant leaves. Among the Fungi, T-1 strain was selected as test strain. This strain was identified as a Monatcus sp. by the morphological propeties. Various culture conditions, and physical and physiological characteristics of red pigment were studied. According to the studies of culture conditions, optimum condition was found to be pH 6.5; 4 days of incubation; temperature, 32~33 c: 3.5% of Tapioca chips powder as carbon source, 0.2% of sodium nitrate as nitrogen source and 100 ml of medium in the 500 ml Erlenmyer flask at a rotary shaker (rpm180) as aeration condition. Also effective levels of vitamins, amino acids and inorganic compounds was found to be l$\mu\textrm{g}$/ml of folic acid and niacin; 0.3% of L-arginine, L-glutamic acid and L-proline; and 0.001% of manganese dioxide giving good results.

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