• Composites Research
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• v.12 no.5
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• pp.40-53
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• 1999

The interlaminar facture behavior of multidirectional carbon-fiber/epoxy composite laminates under low and high rates of test, up to rate of about 11.4m/s has been investigated using the double cantilever beam specimens. The mode I loasing with rates above 1.0m/s had considerable dynamic effects on the load-time curves and thus revealed higher values of the average crack velocity than thet expected from a simple proportional relationship with the test rate. The modified beam analysis utilizing only the opening displacement and crack length exhibited an effective means for evaluating the dynamic fracture energy $G_{IC}$. Flexural modulus increased gradually with an increase of the test rate, which was utilized in the evaluation of $G_{IC}$. Values of $G_{IC}$ at the crack initiation and arrest were scarcely changed with increasing test rate up to 1.0m/s. However the maximum $G_{IC}$ was much enlarged at 11.4m/s due to the large amount of fiber bridging the crack tip. The larger the initial crack length, the smaller the maximum $G_{IC}$ at high rate.

• Transactions of the Korean Society for Noise and Vibration Engineering
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• v.16 no.2 s.107
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• pp.163-168
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• 2006

The PWR Nuclear Fuel assembly consists of more than 250 fuel rods that are supported by leaf springs in the cells of more than 10 Spacer Grids (SG) along the rod length. Since it is not easy to conduct mechanical tests on a full-scale model basis, the small-scaled rod bundle $(5\times5)$ which is called partial fuel assembly is generally used for various performance tests during the development stage. As one of the small-scaled tests, a flow test should be carried out in order to verify the performance of the spacer grid to obtain the Flow-Induced Vibration (FIV) characteristics of the scaled fuel assembly over the specified flow range. A vibration test should be also performed to obtain the modal parameters of the assembly prior to the flow test. In this study, we want to develop the estimation procedure of the damping ratio for the scaled test assembly. For the damping factor of the partial fuel assembly and the grid cage at the first vibration mode, as one of the vibration tests, a so-called pluck testing has been performed in air as a preliminary test prior to in-flow damping measurement test. Logarithmic decrement method is used for calculation of the damping ratio. Estimated damping ratio of the partial fuel assembly is about $0.7\%$ with reasonable error of $2\%$ for the previous results. Nonlinear behavior of the partial fuel assembly might be stem mainly from the rod-grid support configuration.

• Transactions of the Korean Society of Mechanical Engineers
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• v.13 no.2
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• pp.236-242
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• 1989

In order to investigate the effects of hot corrosion on the creep rupture properties and creep life of 304 stainless steel being used as tube materials of heavy oil fired boiler, the creep rupture tests were carried out at temperature 630.deg.C, 690.deg.C and 750.deg.C in static air for the specimens with or without coating of double layer corrosives according to the new hot corrosion test method simulating the situation commonly observed on superheater tubes of the actual boiler. The double layer corrosives are 85% V$_{2}$O$_{5}$ + 10% Na$_{2}$So$_{4}$ + 5% Fe$_{2}$O$_{3}$ as the inner layer corrosive being once melted at 900.deg. C and crushed to powder, and 10% V$_{2}$O$_{5}$ + 85% Na$_{2}$SO$_{4}$ +5% Fe$_{2}$O$_{3}$ as the outer layer corrosive. As results, in the specimen coated with the double layer corrosives, the rupture strength was extremely lowered and showed a large difference each other. The rupture ductility also lowered remarkably as a result of the brittle fracture mode due to hot corrosion. These results indicate that hot corrosion could essentially alter the creep fracture mechanism. From the metallographic observation, it was clarified that the rupture life of 304 stainless steel subjected to hot corrosion was chiefly determined by the behavior of the aggressive intergranular penetration of sulfides.des.

• Applied Chemistry for Engineering
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• v.8 no.2
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• pp.286-291
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• 1997

Taxol which is recognized as a powerful anticancer reagent was extracted from yew extract and separated by NP-HPLC (Normal-PhaseHigh Performance Liquid Chromatography). The experiments were performed in the isocratic mode with $5{\mu}l$ to $100{\mu}l$ injection volume and 1ml/min mobile phase flow rate. The major mobile phase was hexane and small amounts of ethanol, methanol, 1-propanol and isopropanol were added to change the retention behavior. Prior to a real sample, the artificial mixture of taxol, cephalomannine and 10-deacetyltaxol was tested. They are hard to be separated because of similar chemical structures. The experimental results showed that the proper composition of mobile phase for separating the three components was found 96% hexane and 4% ethanol(vol.%) or 96% hexane, 2% 1-propanol and 2% methanol(vol.%). Compared to the run time of 80 minutes for the binary system, the mixture was separated within 50 minutes with the less amount of mobile phase for the ternary system. Finally, $1{\mu}g$ of taxol was separated from yew tree extracts under the optimum operating conditions.

• Journal of Korean Society of Steel Construction
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• v.14 no.4
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• pp.471-479
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• 2002

In this paper, 18 square CFT columns filled with high-strength concrete were tested under concentric or eccentric axial loading. Two parameters of the experimental program included the buckling length-section depth ratio ($L_K$/D) and the eccentricity of the appled compressive load (e). In additon, mechanical properties such as the compressive concrete strength and compressive and tensile steel strength were measured and incorporated into the material models for the stress-strain relationships of concrete and steel. This model was used in an elasto-plastic analysis in order to predict the behavior of the slender CFT columns. Observtions of the failure mode during the tests under axial loadig were also presented. The strengths obtained from the analysis. Recommendations for Design, and Constructions of CFT structures were presented, as verified by the experimental results.

• Journal of Korean Society of Steel Construction
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• v.22 no.3
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• pp.219-228
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• 2010

This paper describes an experimental research on the structural behavior and the ultimate strength of longitudinally stiffened plates subjected to local, distortional, or mixed-mode buckling under compression. The stiffened plate undergoes local, distortional, or interactive local-distortional buckling according to the flexural rigidity of the plate's longitudinal stiffeners and the width-thickness ratios of the sub-panels of the stiffened plate. A significant post-buckling strength in the local and distortional modes affects the ultimate strength of the longitudinally stiffened plate. Compression tests were conducted on stiffened plates that were fabricated from 4mm-thick SM400 steel plates with a nominal yield stress of 235MPa. A simple strength formula for the Direct Strength Method based on the test results was proposed. This paper proves that the Direct Strength Method can properly predict the ultimate strength of stiffened plates when the local buckling and distortional buckling occur simultaneously or nearly simultaneously.

• Journal of Welding and Joining
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• v.31 no.5
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• pp.71-76
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• 2013

The effect of zirconate having - NH functional group on the T-peel and lap shear strength of $CaCO_3$ containing structural epoxy adhesive for car body assembly was investigated. Curing behavior of epoxy adhesive samples were investigated by differential scanning calorimeter (DSC) techniques. The addition of zirconate up to 7.5 phr did not affect the curing mechanism of epoxy adhesive. While the small amount of zirconate addition less than 1.1 phr increased the cross-linking density, the excess addition of zirconate resulted in the increase of uncross-linked impurity. From the increase of T-peel and lap shear strength and the change of fracture mode from the adhesive failure to the mixed one, it was considered that the small addition of zirconate was effective in improving the adhesion strength of epoxy adhesive to the adherend and inorganic filler surfaces. The formation of uncross-linked impurity with the excess addition of zirconate was considered to decrease the joint strength by decreasing the cohesive strength of the cured epoxy.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.36 no.10
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• pp.1195-1203
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• 2012

Welding is a well-developed, widely used process for permanently joining metal components. However, the mechanical reliability of welded parts still offers room for improvement. A weld region consists of a fusion zone, a partially melted zone, and a heat-affected zone, and each zone has different material properties. In addition, the geometrical shape of a weld bead or fillet influences the mechanical reliability. A precise structural analysis must consider how a local welded region influences the mechanical behavior of the entire structure. This study focuses on an effective modeling scheme for the weld region. It relies on experimental and numerical methods to determine the proper correlation based on experimental results and to propose a modeling scheme for welded parts.

• Korean Journal of Materials Research
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• v.25 no.11
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• pp.630-635
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• 2015

The fatigue strength of a nickel-base superalloy was studied. Stress-controlled fatigue tests were carried out at $700^{\circ}C$ and 5 Hz using triangular wave forms. In this study, two kinds of testing procedures were adopted. One is the conventional tension-zero fatigue test(R = 0). The other was a procedure in which the maximum stress was held at 1000 MPa and the minimum stress was diverse from zero to 1000 MPa at 24 and $700^{\circ}C$. The results of the fatigue tests at $700^{\circ}C$ indicate that the fracture mechanism changed according to both the mean stress and the stress range. At a higher stress range, ${\gamma}^{\prime}$ precipitates are sheared by a/2<110> dislocation pairs coupled by APB. Therefore, in a large stress range, the deformation occurred by shearing of ${\gamma}^{\prime}$ by a/2<110> dislocations, which brought about crystallographic shear fracture. As the stress range was decreased, the fracture mode gradually changed from crystallographic shear fracture to gradual growth of fatigue cracks. At an intermediate stress range, as it became more difficult for a/2<110> dislocation pairs to shear ${\gamma}^{\prime}$ particles, cracks started to propagate in the matrix, avoiding the harder ${\gamma}^{\prime}$ particles. High mean stress induced creep deformation, that is, ${\gamma}^{\prime}$ particles were sheared by {111}<112> slip systems, which led to the formation of stacking faults in the precipitates. Thus, the change in fracture mechanism brought about the inversion of the S-N curves.

• International Journal of Aeronautical and Space Sciences
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• v.12 no.4
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• pp.346-353
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• 2011

In this study, the structural performance tests, i.e., static tests and dynamic tests of the composite wind turbine blade, were carried out by using the embedded fiber Bragg grating (FBG) sensors. The composite wind turbine blade used in the test is the 1/23 scale of the 750 kW composite blade. In static tests, the deflections along the blade were evaluated. Evaluations were carried out with simple beam theory and quadratic fitting method by using the embedded FBG sensors to predict the structural behavior with respect to the load. The deflections were compared to those obtained from the laser displacement sensor and electric strain gauges. They showed good agreement. Modal tests were performed to investigate the dynamic characteristics using the embedded FBG sensors. The natural frequencies obtained from the FBG sensors corresponding to the nine mode shapes of the blade were compared to those from the laser Doppler vibrometer. They were found to be consistent with each other. Therefore, it is concluded that the embedded FBG sensors have a great capability for measuring the structural performances of the composite wind turbine blade when structural performance tests are carried out.