• Title/Summary/Keyword: mixture process

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Silicon Carbide Coating by Thermal Decomposition of tetramethylsilane

  • YOON Kyung-Hoon
    • Proceedings of the Korean Ceranic Society Conference
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    • 1986.12a
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    • pp.211-225
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    • 1986
  • Silicon carbide coating has been studied using a graphite substrate, a mixture of tetramethylsilane and hydrogen or argon at deposition temperature (T) of 950 to $1200^{\circ}C$ total pressure of 20 to 50 torr and carrier gas flow rate of 0 to 901/h. Deposition kinetic study has shown that a transition, from a surface reaction limited process to a diffusion limited one, takes place near $1100^{\circ}C$. Deposition rate depends directly upon the experimental parameters. The influence of the main process parameters is also discussed to relate the physiochemical properties of the coating to the deposition conditions.

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Property of New SEGLESS that is Segregation-free Steel Powder Mixture for Warm Compaction

  • Nishida, Satoshi;Furuta, Satoshi
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.731-732
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    • 2006
  • Recently warm compaction techniques are focused on and commercialization of one high-density compaction process in the P/M industry. Another development is a new SEGLESS using a developed lubricant that reduces ejection force at room temperature compaction. It is possible to achieve high-density by reducing lubricant amount. In this paper we confirmed that green density was $7.35g/cm^3$ at 686MPa of compaction pressure when the new SEGLESS was applied to relatively lower temperature warm compaction process, such as $80^{\circ}C$.

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Preparative Resolution of the Pindolol Enantiomers

  • Shibru, Asegahegn-Workaferhaw;Tran, Quoc-Trung;Kim, Kyeong-Ho
    • Proceedings of the PSK Conference
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    • 2003.10b
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    • pp.220.3-220.3
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    • 2003
  • Enantiomers of pindolol were prepared by chromatographic method. Racemic pindolol was derivatized with S-(-)-menthyl chloroformate((-)-MCF) forming its diastereomer, R-(+)-pindolol-(-)-MCF and S-(-)-pindolol-(-)-MCF. The diastereomer mixture was then chromatographically resolved to each diastereomer. Each diastereomer was further hydrolyzed with alkali to each enantiomer quantitatively. Racemization was not occurred in this process. Pindolol enantiomers were recovered producing good yield over 30% over all process.

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Manufacturing of the Permalloy Soft Magnet by Powder Injection Molding Process

  • W. Y. Jeung;Park, J. W.
    • Proceedings of the Korean Magnestics Society Conference
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    • 2000.09a
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    • pp.217-227
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    • 2000
  • The permalloy soft magnet was produced by powder injection molding process. Rheological characteristics of mixtures, debinding conditions and the magnetic properties of permalloy after sintering ware investigated. The permalloy soft magnet with a permeability of 14200 could be obtained by preparing a mixture with a powder loading of 65.4 vol.% and PP/PEG binder system, solvent extraction, thermal debinding and subsequent sintering at 1350 $^{\circ}C$ in hydrogen. The permalloy soft magnet sintered in hydrogen showed a 95 % of theoretical density and a magnetic induction of 13.2 kG at the applied magnetic field of 50 Oe

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A study on exposure of organic solvents in manufacturing industry (제조업 산업장의 유기용제 노출에 관한 연구)

  • Moon, Deog-Hwan;Kim, Jeong-Ha;Kim, Pil-Ja;Park, Myung-Hee;Hwang, Yong-sik;Lee, Chae-Kwan;Lee, Chang-Hee
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.11 no.3
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    • pp.219-228
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    • 2001
  • Objective : For the purpose of preparing the fundamental data and health promotion and control program on organic solvents in air of manufacturing industry. Methods : The author surveyed number of organic solvent components which was used in working site and also determined the organic solvents concentration in air of 927 manufacturing industries and 1,267 working process with gas chromatography(NIOSH manual) for five years from 1995 to 1999. Results : Mean number of solvents components by type of industry, working process was number of 12. There were exceeded to TLV of 1,2-dichloroethane in textile manufacturing industry N,N-dimethyl furan in tanning and dressing of leather ; luggage, handbags, saddlery, harness and footwear manufacturing industry and chemical and chemical product manufacturing industry by type of industry. There were exceeded to TLV of 1,2-dichloroethane in handwriting and drawing process, cellosolve in adhesive spreading process, N,N-dimethly furan in production of solvent process and adhesion process by working process Total exceeded rate to threshold limit values of organic solvents mixture were 12.9% for EI(Exposure index) and 10.0% for Em(Estimation of mixture) by type of industry, 11.3% for EI and 8.2% for Em by type of working process. The highest exceed rate was 36.7% for EI in tanning and dressing of leather ; luggage handbags, saddlery, harness and footwear manufacturing industry and 29.0% for Em in textile manufacturing industry. The highest exceeded rate was 23.1% for EI and 12.5% for Em in adhesive spreading process by working process. Mean values of total subjects by type of industry and type of working process were $0.7{\pm}1.8$ for EI and $0.7{\pm}1.7$ for Em respectively. Conclusions : As above results, the author suggest that it makes the environmental control program on 1.2-dichloroethane, N,N-dimethyl furan, cellosolve by kind of organic solvent and on textile manufacturing industry, tanning and dressing of leather ; luggage, handbags, saddlery harness and footwear manufacturing industry by type of industry, and on handwriting, drawing process and adhesive spreading process and adhesion process by type of working process.

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The Technology for Reduction of Color Difference to Exhaustion Dyeing (흡진염색에서의 색상차이 감소 기술)

  • 김기정
    • Journal of the Korean Professional Engineers Association
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    • v.33 no.5
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    • pp.45-48
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    • 2000
  • DyeMax-L system(a real-time dyeing measuring system) which can do on line monitoring of dyeing process and measurement of the exhaustion of individual dye in mixtured dyes were developed By using the instrument, the compatability of mixture dyes and changes of exhaustion behavior of each dye with the variation of dyeing auxiliaries and dyeing conditions to get factors for control of dyeing

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