• Title/Summary/Keyword: milling experiment

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Effect of coloring agent dryness on zirconia color (치과용 지르코니아 착색제의 건조정도가 지르코니아 색조에 미치는 영향)

  • Lee, Joo-Hee;Park, Jin-Young;Kim, Hae-Jung;Moon, Yun Hee;Kim, Woong-Chul
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.8
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    • pp.176-182
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    • 2018
  • One of the most important factor of esthetic prosthesis is the color of the teeth. Zirconia is produced in the process of design, milling, coloring, drying, and sintering. The effect of the drying degree of zirconia colorant on the color tone is examined. For the experiment, a total of 45 zirconia specimens(15 for each) were fabricated by using cad/cam system. The zirconia specimens(L block(LAZOR), Z block(Zircos-E block posterior), A block(AlphaZ)) were then subjected to zirconia sintering in accordance with the manufacturer's instructions, using a chemical coloring agent to Non-drying(0sec), intermediate (10sec), and completely dried (10min) temperature holding times. The color tone was measured using a spectrophotometer. The results were analyzed with a One-way analysis of variance and the Tukey post-hoc test (${\alpha}=.05$) The $L^*$ values of L, A specimens, $a^*$ values of A specimens, and $b^*$ values of Z specimens were not statistically different according to the degree of drying (p>0.05), While the $L^*$ value of Z specimen, $a^*$ value of L, Z specimen, $b^*$ values of L, A specimens were statistically different according to the degree of drying(p <0.05). In conclusion, the drying of zirconia colourants improves zirconia brightness and increases the optical properties of the enamel.

Bending strength of alumina coated with bioglass and soda lime glass and the precipitation on the surface of coated alumina in PBS (생체 유리와 소다 유리침투에 따른 알루미나 세라믹의 굴곡 강도 및 PBS에서의 표면 생성물 연구)

  • Yuu, Jae-Yang
    • Journal of Technologic Dentistry
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    • v.30 no.2
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    • pp.39-45
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    • 2008
  • Titanium and its alloys are widely used as dental implants materials because of their excellent mechanical properties. However, the alumina and zirconia ceramics are preferred to use as the substitute of Ti implants because there is a problems in esthetics and biocompatibility in Ti implant. The the glass infiltrated alumina ceramics are studied to increase the toughness and biocompatibility. The 45S5 and soda-lime glass powder was mixed with ethanol at ratio of 1:1 and brushed on the surface of alumina. Then it was heat treated in the electric furnace at $1400^{\circ}C$ from 30 min. to 5 hours. The glass powder was controlled from 200 to $350{\mu}m$ using ball milling. After heat treatment, the glass infiltrated specimen was tested in universal testing machine to measure the bending strength. The surface microstructure of each specimen was observed with SEM. The biocompatibility of 45S5 and soda-lime glass coated alumina was investigated using PBS at $36.5^{\circ}C$ incubator. The specimen was immersed in PBS for 3, 5, 7, 10 days. After that, the surface morphology was investigated with SEM. As the results of experiment, the 45S5 bioglass infiltrated alumina show the increase of bending strength according to the increasing of heat treatment time from 30 min. to 5 hours at $1400^{\circ}C$ Finally the 1370N bending strength of alumina increased to 1958N at 5 hours heat treatment, which shows 1.4 times higher. In contrast to this, the soda lime glass infiltrated alumina ceramics shows the convex curve according to heat treatment time. Thus it shows maximum bending strength of 1820N at 1 hour heat treatment of $1400^{\circ}C$ It gives 1.3 times higher. However, the bending strength of soda lime glass infiltrated alumina is decreasing with increasing heat treatment time after 1 hour. The precipitation on the surface of 45S5 glass infiltrated alumina was revealed as a sodium phosphate ($Na_{6}P_{6}O_{24}6H_{2}O$) and the amount of precipitation is increasing with increasing of immersion time in PBS. In contrast to this, there is no precipitation are observed on the surface of soda lime glass infiltrated alumina. This implies that 45S5 glass infiltrated alumina brings more biocompatible when it is implanted in human body.

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Effects of processing, particle size and moisturizing of sorghum-based feeds on pellet quality and broiler production

  • da Silva, Patricia Garcia;Oliveira, Luana Martins Schaly;de Oliveira, Nayanne Rodrigues;de Moura, Fabio Ataides Junior;Silva, Maura Regina Sousa;Cordeiro, Deibity Alves;Minafra, Cibele Silva;dos Santo, Fabiana Ramos
    • Asian-Australasian Journal of Animal Sciences
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    • v.31 no.1
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    • pp.98-105
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    • 2018
  • Objective: This study aimed to assess the effect of pelleted and expanded sorghum-based feeds prepared with different moisture levels and particle size of ingredients on metabolizable energy, ileal digestibility of amino acids and broiler performance. Methods: The experiment was performed with 720 male broiler chicks of the Cobb strain, with treatments of six replications, with 15 birds each; they were arranged in a completely randomized design and $2{\times}2{\times}2$ factorial scheme (pelleted or expanded feed processing, 0.8% or 1.6% moisture addition in the mixer, and particle size of 650 or 850 microns). Results: Higher pellet quality (pellets, % and pellet durability index [PDI]) was obtained in expanded diets and inclusion of 1.6% moisture. The particle size of 850 microns increased the PDI of final diet. All studied treatments had no significant effect on weight gain and broiler carcass and cut yields. Lower feed conversion occurred for birds fed pelleted feed at 42 d. The highest apparent metabolizable energy (AME) and apparent metabolizable energy corrected to zero nitrogen balance (AMEn) values of feed in the initial rearing phase (10 to 13 days) were observed in birds fed pelleted feed or for feed prepared with 1.6% moisture. The highest ileal digestibility coefficients of amino acids were obtained with the consumption of pelleted feed prepared with a particle size of 650 microns and 1.6% moisture. Conclusion: Pelleted feed prepared with a milling particle size of 650 microns and 1.6% moisture provided increased ileal digestibility of amino acids and AMEn in the starter period. However, the expanded feed improved pellet quality and feed conversion of broilers at 42 days of age. We conclude that factors such as moisture, particle size and processing affect the pellet quality, and therefore should be considered when attempting to optimize broiler performance.

Effect of Fertilizer Application Level considering Irrigation Water Quality on Rice (Oryza sativa L.) Productivity and Agricultural Environment (관개수질을 고려한 시비가 벼의 생산성과 농업환경에 미치는 영향)

  • Uhm, Mi-Jeong;Park, Hyun-Cheol;Kim, Kab-Cheol;Ryu, Jeong;Choi, Joung-Sik
    • Korean Journal of Environmental Agriculture
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    • v.23 no.1
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    • pp.7-14
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    • 2004
  • This study was conducted to investigate the effect on agricultural environment and crop productivity by different amount of applied fertilizer in consideration of irrigation water quality. N, P and K contents of irrigation water used in this experiment were 6.16, 0.26 and 9.37 mg/L, respectively. N, P and K Concentrations of runoff water were lower than those of inflow water during rice cultivation. N, P and K Concentrations of ponded and percolated water were changed according to the amount and time of applied fertilization. During rice cultivation in paddy soil, nitrogen balance was closed to 0 in SFT 50% (50% level of soil testing fertilization), 0.14 kg/ha, but it was 95.3 kg/ha in CF (conventional fertilization) treatment In SW 50% and STF (soil testing fertilization) treatment yield of perfect rice was not greatly different as compared with CF treatment due to the superiority of ripening rate, 1,000 grains weight and milling characteristics. Mechanical paratability of rice was excellent in NF (non fertilization) treatment, STF 50% treatment showed higher in nutrient availability and fertilizers use efficiency than other treatments.

Analysis of Useful Components for Freeze-Dried Persimmon Flower Powder by Cultivar (품종별 감꽃 동결건조 분말의 유효성분 분석)

  • Kim, Jun-Han;Park, Seok-Hee;Mun, Hye-Gyeong;Lee, In-Seon;Kim, Jong-Kuk
    • Food Science and Preservation
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    • v.13 no.6
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    • pp.691-696
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    • 2006
  • This study was carried out to analyze useful component in freeze-dried persimmon flower powder made from six cultivais. The cultivais were Dogunjosang, Kojongsi, Kabjubaeknok, Chalang, Weolhasi and SangjuDungsi. Powder of persimmon flower was prepared by milling after freeze drying at $-70^{\circ}C$. Crude lipid was the highest in Dogunjosang (57.26%). Major free sugars of the persimmon flowers were fructose ($95{\sim}310mg%$), glucose ($75{\sim}281mg%$) and sucrose ($7{\sim}28mg%$). Major organic acids were malic acid (225 mg% in Kabjubaeknok (Jun. 4th)) and tartaric acid (189 mg% in Kabjubaeknok (Jun. 4th)). Predominant free amino acids were hydroxy-L-proline(25.33 mg% in Weolhasi), L-citrulline (58.83 mg% in SangjuDungsi (May 280)) and L-threonine (11.88 mg% in SangjuDungsi (May 280)). Major phenolic compounds in the persimmon flowers were caffeic acid ($1,946{\mu}g/100 g$ in Kabjubaeknok (Jun. 4th)), p-hydioxybenzoic acid($418{\mu}g/100 g$ in SangjuDungsi (May 29th)) and protocatechuic acid($181{\mu}g/100 g$ in Kabjubaeknok(Jun. 1st)). The results suggest that persimmon flowers be potential materials as useful food ingredients.

Fabrication and Characteristics of a Highly Sensitive GMR-SV Biosensor for Detecting of Micron Magnetic Beads (미크론 자성비드 검출용 바이오센서에 대한 고감도 GMR-SV 소자의 제작과 특성 연구)

  • Choi, Jong-Gu;Lee, Sang-Suk;Park, Young-Seok
    • Journal of the Korean Magnetics Society
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    • v.22 no.5
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    • pp.173-177
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    • 2012
  • The multilayer structure of glass/Ta(5.8 nm)/NiFe(5 nm)/Cu(t nm)/NiFe(3 nm)/FeMn(12 nm)/Ta(5.8 nm) as typical GMR-SV (giant magnetoresistance-spin valve) films is prepared by ion beam sputtering deposition (IBD). The coercivity and magnetoresiatance ratio are increased and decreased for the decrease of Cu thickness when the thickness of nonmagnetic Cu layer from is varied 2.2 nm to 3.0 nm. It means that the decrease of non-magntic layer is effected to the interlayer exchange coupling of pinned layer and the spin configuration array of free layer. For experiment of detecting and dropping of magnetic beads we used the GMR-SV sensor with glass/Ta/NiFe/Cu/NiFe/FeMn/Ta structure. From the comparison of before and after for the dropping status of magnetic bead, the variations of MR ratio, $H_{ex}$, and $H_c$ are showed 0.9 %, 3 Oe, and 2 Oe, respectively. The fabrication of GMR-SV sensor was included in the process of film deposition, photo-lithography, ion milling, and MR measurement. Further, GMR-SV device can be easily integrated so that detecting biosensor on a single chip becomes possible.

Fermentation Characteristics for Preparation of Distilled Liquor Made of Mixed Grains (혼합잡곡 증류주 제조를 위한 발효 특성)

  • Lee, Dae Hyoung;Jung, Jae Woon;Lee, Yong Sun;Seo, Jae Soon;Park, In Tae
    • Korean Journal of Food Science and Technology
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    • v.46 no.4
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    • pp.446-455
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    • 2014
  • In this study, we aimed to develop mixed grain-derived hard liquor with enhanced favor and taste. First, fermentation characteristics analysis according to the grain used showed that rice and adlay produced high alcohol outputs of 15.2% and 13.3%, respectively, while that of barley was low at 5.6%. In an experiment in which different amounts sorghum flour were added, the sample without sorghum flour showed an alcohol content of 19.0%. The effect of adding up to 7% ipkuk (koji) was examined in a sensory test. Comprehensive preference increased with increasing amounts of added ipkuk. Fermentation characteristics analyses of distilled liquor into which milled rice (5% degrees of milling of unpolished waxy rice) was added showed that alcohol content and acidity were not greatly affected by its addition. Finally, an analysis of aromatic ingredients showed that the percentage of ethyl palmitate, which produces a smooth aroma, was the highest in distilled liquor made of mixed grains.

Antecedent Decision Rules of Personal Pronouns for Coreference Resolution (Coreference Resolution을 위한 3인칭 대명사의 선행사 결정 규칙)

  • Kang, Seung-Shik;Yun, Bo-Hyun;Woo, Chong-Woo
    • The KIPS Transactions:PartB
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    • v.11B no.2
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    • pp.227-232
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    • 2004
  • When we extract a representative term from text for information retrieval system or a special information for information retrieval and text milling system, we often need to solve the anaphora resolution problem. The antecedent decision problem of a pronoun is one of the major issues for anaphora resolution. In this paper, we are suggesting a method of deciding an antecedent of the third personal pronouns, such as “he/she/they” to analyze the contents of documents precisely. Generally, the antecedent of the third personal Pronouns seem to be the subject of the current statement or previous statement, and also it occasionally happens more than twice. Based on these characteristics, we have found rules for deciding an antecedent, by investigating a case of being an antecedent from the personal pronouns, which appears in the current statement and the previous statements. Since the heuristic rule differs on the case of the third personal pronouns, we described it as subjective case, objective case, and possessive case based on the case of the pronouns. We collected 300 sentences that include a pronoun from the newspaper articles on political issues. The result of our experiment shows that the recall and precision ratio on deciding the antecedent of the third personal pronouns are 79.0% and 86.8%, respectively.

A Study on the Cobalt and Lithium Recovery from the Production Scraps of Lithium Secondary Battery by High Efficient and Eco-friendly Method (이차전지(二次電池) 제조공정(製造工程)스크랩으로부터 고효율(高效率) 親環境(친환경) 코발트(Co)와 리튬(Li)의 회수(回收)에 관(關)한 연구(硏究))

  • Lee, Jeong-Joo;Chung, Jin-Do
    • Resources Recycling
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    • v.19 no.6
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    • pp.51-60
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    • 2010
  • A study on the recovery of cobalt and lithium from Lithium Ion Battery(LIB) scraps has been carried out by a physical treatment - leaching - solvent extraction process. The cathode scraps of LIB in production were used as a material of this experiment. The best condition for recovering cobalt from the anode scraps was acquired in each process. The cathode scraps are dissolved in 2M sulfuric acid solution with hydrogen peroxide at $95^{\circ}C$, 700 rpm. The cobalt is concentrated from the leaching solution by means of a solvent extraction circuit with bis(2-ethylhexyl) phosphoric acid(D2EHPA) and PC88A in kerosene, and then cobalt and lithium are recovered as cobalt hydroxide and lithium carbonate by precipitation technology. The purity of cobalt oxide powder was over 99.98% and the average particle size after milling was about 10 lim. The over all recoveries are over 95% for cobalt and lithium. The pilot test of mechanical separation was carried out for the recovery of cobalt from the scraps. The $Co_3O_4$ powder was made by the heat treatment of $Co(OH)_2$ and the average particle size was about 10 ${\mu}m$ after grinding. The recovery was over 99% for cobalt and lithium each other and the purity of cobalt oxide was over 99.98%.

A Study on the Variations of Impact Strength of Plastics for Various Thicknesses and Notch Formation (두께와 노치생성방법에 따른 플라스틱 수지의 충격강도 변화에 관한 연구)

  • Kim, Hyun;Lee, Dae-Seop;Lim, Jae-Soo;Lyu, Min-Young
    • Polymer(Korea)
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    • v.36 no.1
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    • pp.59-64
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    • 2012
  • The impact strength of material is considered the most important design factor for small and light products. Impact strength is a unique material property, thus the impact strength should not depend upon the geometry of specimen. However it varies according to specimen thickness, notching method, and notch shape. In this study, the variations of impact strength have been investigated according to thickness, notch shape, and notching method of specimen. Engineering plastics such as PC, ABS and POM have been used in this study. Experimental results showed impact strength increased as thickness decreasesd. PC showed the highest increment of impact strength when the thickness was thin. Fractured section of PC showed brittle fracture behavior when the specimen was thick. However it showed ductile fracture behavior when it was thin. The impact strength of in-mold notched specimen showed higher than that of milling notched specimen. PC showed the highest notch sensitivity among the materials used in this experiment.