• Title/Summary/Keyword: microstructure effect

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Effect of Annealing Temperature on Magnetic Properties of Dust Cores

  • Mitani, Hiroyuki;Akagi, Nobuaki;Houjou, Hirofumi;Kanamaru, Moriyoshi
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1177-1178
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    • 2006
  • Magnetic Properties of dust cores made of mixtures of atomized pure iron powder and pure alumina powder has been investigated in the temperature range from 673 to 1073K. The effect of annealing on coercivity has been positive effect up to 973K and thus coercivity is gradually reduced form 280A/m (as-compressed) to 160A/m (973K). However, dust cores annealed at 1073K displayed a 15% increasing of coercivity by annealing at 973K. Hysteresis loss shows a tendency similar to coercivity. Microstructure observation of specimens shows grain refinement by recrystallization in the temperature range from 773 to 1073K.

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Fabrication of W-Cu Composite by Resistance Sintering under Ultrahigh Pressure

  • Kwon, Y.S.;Kim, J.S.;Zhou, Z.J.
    • Journal of Powder Materials
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    • v.10 no.3
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    • pp.181-185
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    • 2003
  • Resistance sintering under ultra-high pressure if developed to fabricate W-Cu composite containing 5 to 80v/o copper. The consolidation was carried out under pressure of 6 to 8 GPa and input power of 18 to 23 kW for 50 seconds. The densification effect and microstructure of these W-Cu composites are investigated. The effect of W particle size on ,sintering density was also studied. The micro hardness was measured to evaluate the sintering effect.

The Effect of Chemical Composition of Sintering Atmosphere on the Structure and Mechanical Properties of PM Manganese Steels with Chromium and Molybdenum Additions

  • Sulowski, Maciej;Cias, Andrzej;Stoytchev, Marin;Andreev, Tchavdar
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.561-562
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    • 2006
  • The effect of chemical composition of the sintering atmosphere on density, microstructure and mechanical properties of Fe-3%Mn-(Cr)-(Mo)-0.3%C steels is described. Pre-alloyed Astaloy CrM and CrL, ferromanganese and graphite were used as the starting powders. Following pressing in a rigid die, compacts were sintered at 1120 and $1250^{\circ}C$ in atmospheres having different $H_2/N_2$ ratio and furnace cooled to room temperature. It has been found that the atmosphere composition has negligible effect on the as-sintered properties of the investigated materials.

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Effect of Coiling Temperature on the Annealed Texture in Cu/Nb Added Ultra Low Carbon Steels

  • Jiang, Yinghua;Park, Young-Koo;Lee, Oh-Yeon
    • Korean Journal of Materials Research
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    • v.18 no.2
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    • pp.65-68
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    • 2008
  • The present work was performed to investigate the effect of coiling temperature on the annealed texture in Cu/Nb-added ultra-low-carbon steels. The ultra-low-carbon steels were coiled at 650 and $720^{\circ}C$, respectively. The result showed that the Cu-added ultra-low-carbon steel at a low coiling temperature produced a desirable annealed texture related to good formability. On the other hand, Nb-added ultra-low-carbon steel at a high coiling temperature also produced a desirable texture. This is attributed to the effect of Nb, which retards recrystallization during the coiling process.

Microstructure analysis of DLC thin film fabricated by filtered arc ion plating method

  • Park, Y.P.;Kim, T.G.;Cheon, M.W.
    • Journal of Ceramic Processing Research
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    • v.13 no.spc2
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    • pp.363-367
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    • 2012
  • DLC (diamond liked carbon) coating of the tungsten carbide (WC) alloy core surface for molding a glass aspheric lens improves the quality of glass lens and the molding core and is characterized by high hardness, high elasticity, abrasion resistance and chemical stability. In this study, the effect of DLC coating of a thin film by means of the filtered AIP (arc ion plating) technique was examined on Ra and shape of the coated surface. Roughness before and after DLC coating was measured and the result showed that the roughness was improved after coating as compared to before coating. It was observed that DLC coating of the WC alloy core surface for molding had an effect on improving the roughness and shape of the core surface. It is considered that this will have an effect on improving abrasion resistance and the service life of the core surface.

Effect of Oxygen on the Microstructure and Mechanical Properties of Cr-O-N Coatings (Oxygen 함량에 따른 Cr-O-N 코팅막의 미세구조 및 기계적 특성에 관한 연구)

  • Yun, Jun-Seo;Kwon, Se-Hun;Park, In-Wook;Lee, Jeong-Du;Kim, Kwang-Ho
    • Journal of Surface Science and Engineering
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    • v.42 no.5
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    • pp.220-226
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    • 2009
  • Cr-O-N coatings having different oxygen contents were deposited on Si wafer and SUS 304 substrates by an arc ion plating technique using Cr target in $Ar/O_2/N_2$ gaseous atmosphere. As increasing oxygen content in the coating, the microstructure of Cr-O-N coating changed from polycrystalline having NaCl structure to amorphous structure. Further increase of oxygen content resulted in phase transformation from amorphous to rhombohedral structure. From the variations of d value and average grain size, it was revealed that the maximum solubility of oxygen in Cr-O-N coating was about 21 at.%. And the maximum micro-hardness of 2751HK was obtained in this composition. The lowest friction coefficient was measured in the coating having 34.8 at.% of oxygen. However, more narrow width of wear track was found in the coating having 30.1 at.% of oxygen.

Corrosion Behavior of Solution-Treated Mg-8%Al-X%Zn Casting Alloys (용체화처리된 주조용 Mg-8%Al-X%Zn 합금의 부식 거동)

  • Jun, Joong-Hwan;Hwang, In-Je
    • Journal of the Korean Society for Heat Treatment
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    • v.28 no.3
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    • pp.126-133
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    • 2015
  • The aim of this study is to investigate the effect of solution treatment on the corrosion behavior of Mg-8%Al-(0-1)%Zn casting alloys in 1M NaCl aqueous solution. After the solution treatment, all alloys showed single ${\alpha}$-(Mg) phase microstructure by dissolution of ${\beta}(Mg_{17}Al_{12})$ phase into the ${\alpha}$-(Mg) matrix. The $H_2$ evolution volume decreased with an increase in Zn content, which indicates that the addition of Zn plays a beneficial role in decreasing corrosion rate of the Mg-Al-Zn alloy in solution-treated state. The microstructural evaluations on the corrosion products and corroded surfaces after the immersion test in 1 M NaCl solution revealed that the incorporation of more $Al_2O_3$ and ZnO into the corrosion product, by which the penetration of $Cl^-$ ions is impeded, are thought to be responsible for the better corrosion resistance in relation with the Zn addition.

Effect of Cryogenic Treatment on the Phase Change and Mechanical Property in STD11 steel for Die and Tool (STD11강의 상변화 및 기계적 성질에 미치는 초심냉처리의 영향)

  • Kim, H.J.;Jang, W.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.28 no.3
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    • pp.139-145
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    • 2015
  • Effects of austenitizing, cryogenic treatment and tempering conditions on the phase change, microstructure and Vickers hardness value have been studied in STD11 steel for tool and die. The volume fraction of retained austenite increased with a rise in austenitizing temperature, while the volume fraction of eutectoid $M_7C_3$ carbides decreased. The retained austenite could be reduced by cryogenic treatment i.e., maintaining at $LN_2$ temperature ($-196^{\circ}C$) for 12hrs but a little amount of retained austenite did not transform to martensite further although holding time increased to 24 hrs or more. The microstructure of the quenched and then cryogenictreated specimen showed nano-sized and needle-shaped carbides in matrix due to the decomposition of martensite by tempering, but that of the one without cryogenic treatment still revealed retained austenite by tempering even at $500^{\circ}C$.

The Effect of Al and Sn Additions on Corrosion Behavior of Permanent Mold Casting Magnesium Alloy (금형 주조한 마그네슘 합금의 부식 거동에 미치는 Al 및 Sn의 영향)

  • Kim, Byeong Ho;Seo, Jae Hyun;Park, Kyung Chul
    • Journal of Korea Foundry Society
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    • v.35 no.2
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    • pp.36-43
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    • 2015
  • In this study, the influences of aluminum and tin additions (individual and combined) on corrosion behavior of magnesium alloy have been determined. The studied alloys were fabricated by permanent mold casting method to measure the corrosion properties, a potentiodynamic test, hydrogen evolution test and immersion test were carried out in a 3.5% NaCl solution at pH 7.2. From the results of microstructure analysis, the Mg-9Al-1Zn alloy was found to be composed of ${\alpha}$-Mg and rod-like $Mg_{17}Al_{12}$ phase and the Mg-5Sn-5Al-1Zn alloy was found to be composed of ${\alpha}$-Mg, rod-like $Mg_{17}Al_{12}$ and $Mg_2Sn$ phases. In the case of the Mg-9Sn-1Zn alloy, the microstructure was composed of ${\alpha}$-Mg and eutectic $Mg_2Sn$ phase. With Sn addition (individual and combined), the corrosion resistance of the Mg alloys improved.

Charactetristical Analysis of the Microstructure and the Stress-Strain Curves for the Evaluation of 7xxx Series Aluminum Extrudates (7xxx계급 알루미늄 열간 압출재의 평가를 위한 미세조직과 응력-변형률 곡선의 분석)

  • Lee, S.Y.;Woo, Y.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.31 no.6
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    • pp.307-314
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    • 2018
  • Simple tensile tests and microstructural investigations have been performed on extrudates of high strength aluminum alloys such as 7075, 7021 and 7xxx(Sc) to understand correlation between extruding conditions and extruded properties. Tensile specimens which were taken from different locations at the same cross section of an extrudate were tested at room temperature and with a strain rate of $8.9{\times}10^{-5}/s$. The microstructures according to the locations at the cross section have been observed using optical microscopy and electron back-scattered diffraction (EBSD) mapping to characterize the effect on stress-strain curve. The results could be classified in three types independent of alloying contents and extusion methods. The fine differences in the stress-strain curves were resulted from inhomogenity in the microstructures according to locations of an extrudate which were performed through instantaneous extruding conditions such as temperature, strain rate and strain.