• Journal of Powder Materials
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• v.5 no.3
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• pp.210-219
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• 1998

The W-Cu composite powders were synthesized from W and Cu elemental powders by ball-milling process, and their microstructural changes and sintering behaviors were evaluated. The ball milling process was carried out in a 3-dimensional mixer (Turbula mixer) using zirconic ($ZrO_2$) ball and alumina ($Al_2O_3$) vial up to 300 hrs. The ball-milled W-Cu powders revealed nearly spherical shape. Microstructure of the composite powders showed onion-like structure which consists of W and Cu shells due to the moving characteristic of Turbula mixer. The W and Cu elements in the composite powders milled for 300 hrs were homogeneously distributed, and W grain size in the ball-milled powder was smaller than 0.5 $\mu\textrm{m}$. Fe impurity introduced during ball milling process was very low as of 0.001 wt%. The relative sintered density of ball-milled W-Cu specimens reached about 94% after sintering at $1100^{\circ}C$.

• Journal of Welding and Joining
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• v.14 no.4
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• pp.62-70
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• 1996

Al or Al-alloy have been known to be able to be claded on various materials by using explosive welding process, however, the intermetallic layer frequently formed along the interface have made this process very complicated. In this study, it was focussed to select the process variables, which can get rid of interfacial layer in the Al-claded steel plate. As a result, it was demonstrated that there was a certain range of explosive thickness which did not form the intermetallic phase as well as the non-bonded area. On the other hand, ultasonic tests performed for identifying the presence of interfacial layer nondestructively showed that it could be applied for the intended purpose but its result was weakly related with the microstructural quality of interface.

• Korean Journal of Materials Research
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• v.25 no.10
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• pp.509-515
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• 2015

MAO ceramic coatings were prepared on AZ61 magnesium alloy for various processing times ranging from 5 to 60 min, in an electrolyte solution based on silicate-fluoride. The mechanical, electrochemical and, microstructural properties and the phase compositions of the coating layers were investigated. In this work, unlike previous studies, coatings with high amounts of the $Mag_2SiO_4$ phase were formed which contained small amounts of MgO and $MgF_2$ at a processing condition of 30 min. A microstructural analysis revealed that the porosity of the coatings was reduced considerably with an increase in the processing time, together with a change in the pore geometry from an irregular to a spherical shape. Potentiodynamic polarization and mechanical testing results showed that the coatings acquired after a processing time of 30 min were superior to all of the others.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.536-537
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• 2006

In the present work, the sintering behavior of high strength Al-5.6Zn-2.5Mg-1.6Cu (in wt.%) alloy compacts prepared from elemental powders was investigated. Microstructural evaluation was accompanied by XRD and DSC methods in order to determine the temperature and chemical composition of the liquid phases formed during sintering. It was found that three transient liquid phases are formed at 420, 439 and 450 $^{\circ}C$. Microstructural study revealed the progressive formation of sintered contacts due to the presence of the liquid phases, although the green compact expands as a result of the melt penetration along the grain boundaries. While Zn melts at ${\sim}420\;^{\circ}C$, the intermetallic phases formed between Al and Mg were found to be responsible for the formation of liquid phase and the dimensional change at higher temperatures.

• Journal of the Korean Society for Heat Treatment
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• v.34 no.2
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• pp.60-65
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• 2021

In this study, the effect of pressure type and foaming agent on the microstructural change of Al foam produced by powder compact processing was investigated. Better foaming characteristic is easily obtained from extrusion process with strong plastic deformation and preheating than that by uniaxial pressing with preheating. In current powder compact foaming process using TiH2/MgH2 mixture as a foaming agent, a temperature of 670℃ and addition of 30% MgH2 in TiH2 foaming agent was chosen as the most suitable foaming condition. The aluminum (Al) foams with maximum porosity of around 70%, relatively regular pore size and distribution were successfully produced by means of the powder metallurgy method and extrusion process.

• Korean Journal of Materials Research
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• v.10 no.9
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• pp.619-623
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• 2000

Alumina membrane was prepared by sol-gel coating method using boehmite powder(${\Upsilon}-AlOOH$). The supported and the unsupported alumina membrane were fabricated to investigate the phase transformation and change of microstructure. It is important to control the homogeneous pore size and distribution in application of filtering process. The ${\theta}-to\;{\alpha}-AL_2O_3$ phase transformation (XRD) and the change of microstructure was investigated using scanning electron microscopy(SEM). XRD patterns showed that the supported membrane had $100^{\circ}C$ higher ${\theta}-to\;{\alpha}-AL_2O_3$ transformation temperature compared to the unsupported membrane. The similar effect was also observed for microstructural change of the membrane.

• Korean Journal of Metals and Materials
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• v.50 no.1
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• pp.13-22
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• 2012

Forged and flat-bar rolled STD11 tool steel shows anisotropic dimensional change during heat treatment. The dimensional change in the rolling direction is larger than that in the transverse direction. The cause of the anisotropic dimensional change is that the steel is anisotropic in composition, microstructure and other properties. The decrease of anisotropic distortion in tool steel is important for making better precision cold working dies. In this study, the effect of ingot weight and hot rolling reduction ratio on the anisotropic dimensional change of STD11 during heat treatment has been studied. Dimensional change was evaluated by simulating a real heat treatment process, including gas quenching and tempering. Experimental results showed that all the rolled flat-bar products had anisotropic distortion to some degree, but the anisotropic distortion was reduced as hot rolling ratio increased. Ingot weight had a little effect on anisotropic distortion. Microstructural observation showed that the anisotropic dimensional change of STD11 tool steel was closely related to the amount, shape and distribution of coarse carbides.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.05a
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• pp.139-142
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• 2004

Nickel base superalloys are widely used for high temperature applications due to heat resisting capability and corrosion resistance at high temperatures. Superalloys with many strengthening alloying elements are frequently used in powder form to alleviate harmful effects of alloy segregation. HIP (hot isostatic pressing) and DB (diffusion bonding) as a form of solid-state bonding process is used to make turbine components, such as integrated turbine rotors. HIP/DB process requires many technical overcomes related to dimensional changes as well as microstructural control. In this research, HIP/DB process for nickel base superalloys, Udimet 720 and MM 247, were investigated with a view to control the dimensional change during the consolidation process. Simple disc-shaped cans were used to select the conceptual die design for the control of the dimensional change especially in radial direction. The change in the shape of consolidated shape was investigated using commercial FE code with constitutive equations fur low temperature plasticity deformation.

• 한국정보디스플레이학회:학술대회논문집
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• 2008.10a
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• pp.1445-1447
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• 2008

Micro crystal structure of polycrystalline MgO film is controlled by adjusting the energy of particles arrived at the substrate during deposition. The change of crystal structure affects on the total area of (200) surface where the oxygen vacancies are formed easily, resulting in the change of secondary electron emission (SEE) coefficient($\gamma$).

• Journal of the Korean Ceramic Society
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• v.34 no.4
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• pp.351-356
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• 1997

The origin of the variation of initial permeability in manganese-zinc ferrite polycrystals with a content of hematite was investigated. Initial permeability showed maximum with hematite content while there was no significant change in microstructure. Saturation magnetization increased with hematite content. So the variation of initial permeability was not explained on the basis of microstructural change or saturation magnetization. Temperature dependence of initial permeability revealed magnetocrystalline anisotropy was the origin of the variation of initial permeability. The change in magnetocrystalline anisotropy was ascribed to the variation in ferrous ion concentration. Therefore the variation of initial permeability in manganese-zinc ferrite polycrystals with a content of hematite was due to ferrous ion concentration via magnetocrystalline anisotropy.