• 제목/요약/키워드: microstructural change

검색결과 316건 처리시간 0.031초

식이 Vitamin E가 Streptozotocin 유발 당뇨쥐 신장조직에서의 병리조직학적 변화에 미치는 영향 (Effects of Vitamin E on the Microstructural Changes of Renal Tissue in Streptozotocin-Induced Diabetic Rats)

  • 이순재;곽오계;임정교
    • 한국식품영양과학회지
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    • 제28권3호
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    • pp.663-669
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    • 1999
  • The purpose of this study was to investigate the effects of vitamin E on the histochemical change of kidney tissue in diabetic rats. Sprague Dawley male rats weighing 100$\pm$10g were randomly assigned to one normal and three STZ induced diabetic groups, which were subdivided into vitamin E free diet(DM 0E group), 40mg vitamin E per kg diet(DM 40E group) and 400mg vitamin E per kg diet(DM 400E group). Vitamin E level of normal group was 40mg per kg diet. Diabetes was exper imentally induced by intravenous injection of 55mg/kg of body weight of streptozotocin(STZ) in citrate buffer(pH 4.3) after 4 weeks feeding of experimental diets. Animals were sacrificed at the 6th day of diabetic states. The contents of thiobarbituric acid(TBARS) in kidney were increased 119%, 84% and 33% in DM 0E, DM 40E and DM 400E groups, respectively, compared to normal group. That of DM 400E group was decreased 39% compared to DM 0E group. Content of 2 microglobulin in urine in DM 0E, DM 40E, and DM 400E groups were increased by 248%, 181%, and 164%, respectively, compared to normal group. The diabetic groups showed the regressive lesion such as renal tubule, intumescence of epithelial cell, vacuolization. The results of the observation through electronic microscope showed the mitochondria shape of proximal tubule epithelial cell, irregular array, increase of ribosome, and irregular arrangement of small villosity, etc. These types of changes appeared severer in DM 0E group than in DM 400E group. These results indicate that the TBARS productions on kdney in STZ induced diabetic rats were increased, consequently those leaded to damage of renal tubule and minuteness structure. But a large quantity vitimin E supplementation was suppressed in TBARS production and improved in peroxidative damage of renal tissue so that relieved degenerative changes of renal tubule epithelial cell.

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자기유도법에 의한 합금강의 템퍼링 온도에 따른 기계적성질과 임피던스 특성과의 관계에 관한 연구 (A Study on the Relationship between Mechanical Property and Impedance Characteristics with respect to Tempering Temperature in Alloy Steels by Electromagnetic Method)

  • 조경식;장홍근;이주석;배종수
    • 비파괴검사학회지
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    • 제8권1호
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    • pp.38-43
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    • 1988
  • Microstructure and mechanical properties of most steels change by heat treat treatment. Such variation of stucture and properties of steel cause an impedance change on electromagnetic induction coil. The objective of this study is, by searching the relationship between the mechanical property or microstructural changes and impedance value of induction coil, to examine the applicablity of a monitoring the heat treated condition of products nondestructively.

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Advances in modelling the mechanisms and rheology of electrorheological fluids

  • See, Howard
    • Korea-Australia Rheology Journal
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    • 제11권3호
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    • pp.169-195
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    • 1999
  • An electrorheological fluid (ERF) is typically a suspension of semi-conducting solid particles dispersed in an insulating carrier fluid, and shows a dramatic change in rheological properties when an external electric field is applied. This rapid and reversible change in flow properties has potential application in many electronically controlled mechanical devices, but the development of efficient devices and optimal materials for ERF is still hindered by incomplete understanding of the fundamental physical mechanisms involved. In recent years there have been considerable advances In relating microstructural models to the rheological behaviour, and these will form the basis of this review. Results of the theoretical calculations and simulations will be compared to the key experimental evidence available. An overview of the fundamental physical concepts behind electrorheological fluid behaviour will also be presented.

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Annealing Effect of Local Anisotropy Field in Amorphous Co66Fe4Ni1B14Si15 Ribbon

  • Kim, C.G.;Jeong, M.H.;Jeong, M.H.;Yoon, S.S.;Yu, S.C.
    • Journal of Magnetics
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    • 제3권4호
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    • pp.123-126
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    • 1998
  • The magneto-impedance (MI) has been measured in the annealed Co66Fe4Ni1B14Si15 amorphous ribbon for the evaluation of anisotropy field. MI at the frequency of 10 MHz is related to the transverse permeability from rotational magnetization depending on the local anisotropy field. MI varies sensitively with the annealing temperature, reflecting the change of anisotropy field distribution. The local anisotropy fields evaluated from MI Profiles are discussed in terms of the magnetic softness and microstructural change by the annealing.

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초음파현미경을 이용한 Co 기 초내열 합금 열화재의 비파괴평가 (Nondestructive Evaluation for Thermally Degraded Co-base Superalloy by Scanning Acoustic Microscope)

  • 김정석;송진헌;권숙인;임재생;박익근
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2004년도 춘계학술대회
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    • pp.336-341
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    • 2004
  • This research investigates the feasibility of ultrasonic microscope for nondestructive assessment of thermal degradation in artificially aged commercial Co-base superalloy, FSX414. This alloy has been used for high temperature structure applications such as stationary gas turbine blade and nozzle chamber in fossil plant. Microstructural change was found that the fine carbides became coarser and spheroidized in matrix as aging time increased. The leaky surface acoustic wave velocity gradually decreases by a maximum of 4.7% with increasing aging time up to 4,000hours. However, the longitudinal wave velocity has a little change. Also, it has a good correlation between leaky surface acoustic wave velocity and Vickers hardness. Consequently, LSAW can be used to examine the degree of degradation in thermally aged Co-base superalloy.

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열처리 조건에 따른 미세 강선의 굽힘 피로 특성 변화 (Effects of Patenting Temperature on the Bending Fatigue Resistance of the Steel Filaments used for Automotive Tire)

  • 양요셉;배종구;박찬경
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2008년도 춘계학술대회 논문집
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    • pp.454-457
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    • 2008
  • Effects of patenting temperature on bending fatigue resistance of pearlitic steel filaments were investigated experimentally. The fatigue resistance of steel filaments was carried out by using hunter machine, specially designed for ultra fine-sized steel wires, in the controlled conditions. The transmission electron microscopy (TEM) was used for observing the overall microstructure. It revealed that the fatigue resistance as well as tensile strength increased together with increase of patenting temperature from 510 to $600^{\circ}C$, while the endurance ratio ($\sigma_e/\sigma_{TS}$) of filaments decreased. It is believed that this variation of mechanical properties with change of patenting temperature should be strongly influenced by the change of microstructure. The bending fatigue properties of steel filaments were discussed based on microstructural parameters.

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5, 100 mtorr의 증착압력에서 스퍼터 증착한 구리박막층이 Cu/Cr 박막과 폴리이미드 사이의 접착력에 미치는 영향 (The effects of Cu thin films sputter deposited at 5 and 100 mtorr on the adhesion between Cu/Cr film and polyimide)

  • 조철호;김영호
    • 한국표면공학회지
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    • 제29권3호
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    • pp.157-162
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    • 1996
  • The effects of microstructural change on the adhesion strength between Cu/Cr film and polyimide have been studied. Cr films (50 nm thick) and Cu films (500 or 1000 nm thick) were deposited on polyimide by DC magnetron sputtering. During Cu deposition the Ar pressure was 5 or 100 mtorr. The microstructure was observed by SEM and the adhesion was measured by T-peel test. Plastic deformation of peeled metal strips was characterized quantitatively by using XRD technique. The film in which Cu is deposited at 100 mtorr has higher adhesion strength than the film in which Cu is deposited at 5 mtorr. And in the film with same deposition pressure of 100 mtorr, the adhesion strength is increased as the deposited thickness increases from 500 to 1000 nm. The adhesion change of Cu/Cr can be interpreted as the difference in plastic deformation.

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초음파 비선형파라미터를 이용한 무산소동 저주기피로와 2.25Cr 페라이트강의 등온열화 평가 (Characterization of Low-cycle Fatigue of Copper and Isothermal Aging of 2.25Cr Ferritic Steel by Ultrasonic Nonlinearity Parameter)

  • 김정석
    • 열처리공학회지
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    • 제35권5호
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    • pp.239-245
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    • 2022
  • The purpose of this study is to evaluate the degree of microstructural change of materials using ultrasonic nonlinear parameters. For microstructure change, isothermal heat-treated ferritic 2.25Cr steel and low-cycle fatigue-damage copper alloy were prepared. The variation in ultrasonic nonlinearity was analyzed and evaluated through changes in hardness, ductile-brittle transition temperature, electron microscopy, and X-ray diffraction tests. Ultrasonic nonlinearity of 2.25Cr steel increased rapidly during the first 1,000 hours of deterioration and then gradually increased thereafter. The variation in non-linear parameters was shown to be coarsening of carbides and an increase in the volume fraction of stable M6C carbides during heat treatment. Due to the low-cycle fatigue deformation of oxygen-free copper, the dislocation that causes lattice deformation developed in the material, distorting the propagating ultrasonic waves, and causing an increase in the ultrasonic nonlinear parameters.

표면처리 시간에 따른 임플란트 미세구조의 변화;SLA와 TB 표면 임플란트 (Microstructural Change of Implant Surface conditioned with Tetracycline-HCI;SLA and TB surface implant)

  • 우정아;허익;권영혁;박준봉;정종혁
    • Journal of Periodontal and Implant Science
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    • 제35권4호
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    • pp.921-937
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    • 2005
  • Mechanical and chemical methods are the two ways to treat the implant surfaces. By using mechanical method, it is difficult to eliminate bacteria and by-products from the rough implant surface and it can also cause the structural change to the implant surface. Therefore, chemical method is widely used in order to preserve and detoxicate the implant surface more effectively. The purpose of this study is to evaluate the effect of tetracylcline- HCl on the change of implant surface microstructure according to application time. Implants with pure titanium machined surface, SLA surface and $TiO_2blasted$ surface were used in this study. Implant surface was rubbed with sponge soaked in 50mg/ml tetracycline - HCl solution for $\frac{1}{2}$ min., 1min., $1\frac{1}{2}$ min., 2 min., and $2\frac{1}{2}min.$ respectively in the test group and with no treatment in the control group. The sponge was soaked in every 30 seconds. Then, the specimens were processed for scanning electron microscopic observation. Based upon the analysis of photographs by three dentists who are not related with this study, the results were obtained as follows; 1. In the pure titanium machined surfaces, the control specimen showed a more or less rough machined surface composed of alternating positive and negative lines corresponding to grooves and ridges. After treatment, machining line was more pronounced for the control specimens. but in general, test specimens were similar to control. 2. In the SLA surfaces, the control specimen showed that the macro roughness was achieved by large-grit sandblasting. Subsequently, the acid-etching process created the micro roughness, which thus was superimposed on the macro roughness. Irrespective of the application time of 50mg/ml tetracycline - HCl solution, in general, test specimens were similar to control. 3. In the $TiO_2blasted$ surfaces, the control specimen showed the rough surface With small pits. The irregularity of the $TiO_2blasted$ surfaces with 50mg/ml tetracycline - HCl solution was lessened and the flattened areas got wider after 1 minute.

LNG 저장탱크 내조용 9% Ni강의 SAW 용접열영향부내 파괴인성 변화 평가 (Change in Fracture Toughness within Heat-Affected Zone of SA-Welded 9% Ni Steel)

  • 장재일;이정석;이백우;주장복;권동일;김우식
    • 대한기계학회논문집A
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    • 제26권3호
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    • pp.528-536
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    • 2002
  • As one step for the safety performance of LNG storage tank, the change in fracture toughness within the X-grooved weld heat-affected zone (HAZ) of newly developed 9% Ni steel, which was submerged arc (SA)-welded, was investigated. Both crack initiation fracture toughness and crack arrest fracture toughness were evaluated by the crack tip opening displacement (CTOD) tests and compact crack arrest (CCA) tests. As the evaluated region approached the fusion line, each test result shorted different tendency, that is, crack initiation toughness decreased while crack arrest toughness increased. The results were discussed through the observation of the microstructural change.