• Title/Summary/Keyword: microscopy (electron, scanning)

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Evaluation on the Applicability as Filler materials of Ni-Based Super Alloying Nano Size Powder by Pulsed Wire Evaporation(PWE) Method (전기폭발법으로 제조된 니켈기 초내열합금 나노분말의 용가재로의 응용가능성에 관한 평가)

  • Kim, Gyeong-Ho;Lee, Min-Gu;Kim, Gwang-Ho;Lee, Chang-Gyu;Kim, Heung-Hui
    • Proceedings of the KWS Conference
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    • 2005.11a
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    • pp.168-170
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    • 2005
  • Nickel base brazes containing boron and silicon as melting point depressants are used extensively in the joining and repair of hot-section components in next generation nuclear reactor and aero-engine. Therefore, the present study has investigated the preliminary applicability of nickel based alloying nano powders. Nano Ni-based alloying powders synthesized by Pulsed Wire Evaporation (PWE) method. It's powder morphology and phase transformation temperature were analyzed by scanning electron microscopy, transmission electron microscopy, and differential scanning calorimeter(DSC). The powder particle size was approximately 10${\sim}$100nm and exhibits a quite even equiaxed shape. The results of DSC measurement show that both the nano Inconel 625 nano powder and Inconel 718 nano powder presents similar liquidus temperatures approximately $1373^{\circ}C$ and $1380^{\circ}C$ respectively.

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The Characteristic in Mg Alloy with Burning and Plasma Electrolyte Oxidation Surface Treatment (Mg Alloy의 Burning과 Plasma Electrolyte Oxidation 표면처리에 대한 연구)

  • Yu, Jae-In;Choi, Soon-Don;Jang, Ho-Kyeoung
    • Journal of the Korean Vacuum Society
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    • v.19 no.5
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    • pp.326-330
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    • 2010
  • The surface oxidation of magnesium was performed by burning and PEO treatment method. The scanning electron microscopy (SEM), EDS, and I-V characteristics have been applied to the study of the oxidation status. The sample formed by buring method shows weaker corrosion-resistant property than that by PEO method, but this shows more conducting property.

Aging of Melt Spun Ribbons in Cu-Based Shape Memory Alloys at High Temperature (Melt Spinning된 Cu-Al-Ni-X계 형상기억합금 리본의 고온시효)

  • 최영택
    • Journal of Powder Materials
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    • v.2 no.3
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    • pp.208-215
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    • 1995
  • The aging effects on the characteristics of the melt spun Cu based shape memory alloys have been investigated by the microhardness test, X-ray diffraction, differential scanning calorimetry, scanning electron microscopy and transmission electron microscopy. After aged for specific times, hardness of the ribbons began to increase and shape memory capacity diminished. At the initial stage of aging the austenitic transformation temperatures increased gradually, but at last became nearly constant: That is, the aging deteriorated the thermal stability. The increase in hardness was due to the formation of the $\gamma_2$ precipitates. The loss in the shape memory capacity was due to the decrement of solute atoms in the matrix by the formation of the $\gamma_2$ precipitates. In this study, it was confirmed that Mn is an effective element for Improving the thermal stability.

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The Tissue Types of Stroma in Some Species of Hypoxylon (Hypoxylon속 자낭자좌 조직의 형태 연구)

  • Lee, Yang-Soo
    • Applied Microscopy
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    • v.27 no.4
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    • pp.453-460
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    • 1997
  • The tissue types of stromata were observed intensively in four species of Hypoxylon under a scanning electron microscope (SEM). These stromata were sectioned with a freezing fracture method for observation. Several tissue types were recognized and stable in each species. This study presents the most intensive observation of tissue types of each layer of stromata. It will be useful for taxonomic criteria for the species level. However, the tissue types can not be major taxonomical criteria for the genus Hypoxylon.

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Electron Microscopic. Study on Mucous Glands in Frog Skin (개구리(Rana catesbeiana) 피부점액선(皮膚粘液腺)에 관한 전자현미경적(電子顯微鏡的) 연구(硏究))

  • Kang, Kyung-Hee;Jeon, Jin-Seok
    • Applied Microscopy
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    • v.25 no.1
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    • pp.86-95
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    • 1995
  • This study was accomplished to investigate the ultrastructure of mucous glands in dorsal skin of frog (Rana catesbeiana) by means of scanning and transmission electron microscopes. The dorsal skin of Rana catesbeiana is composed of epidermis and dermis. The cutaneous mucous glands consist of inner glandular epithelial cells and outer myoepithelial cells. Glandular epithelial cells are divided into four types by the microscopic ultrastructure; ER-rich cell, round secretory granule-containing cell, foam-like granule mass-containing cell, mitochondria-rich cell. Myoepithelial cell has a long elliptical nucleus and filled with fibrous materials in the cytoplasm. As a result of scanning microscopic observation, the surface of dorsal skin is covered with cutaneous protrusions. The opening sites of the mucous glands are irregularly distributed in dorsal skin.

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Eletron Microscopic Observation of Calcium-Acetylated Seaweed Alginate Gel

  • Jin Woo Lee
    • Journal of Life Science
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    • v.9 no.1
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    • pp.45-49
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    • 1999
  • Seaweed alginate was acetylated by activated carbon immobilized Pseudomonas syringae in a fluidized bed, up-flow reactor. The acetylation degree of seaweed alginate was about 30%. Calcium-acetylated seaweed alginate gel bead was made and compared to calcium-seaweed alginate gel bead by the scanning electron microscopy (SEM). Structural difference of two gel beads may results from increased viscosity and decreased affinity of acetylated seaweed alginate for calcium ion. On the basis of interior and exterior structure of calcium-acetylated seaweed alginate gels and property of acetylated seaweed alginate, it seems that acetylated seaweed alginate is used for the supporter for electrophoresis and packing materials for liquid chromatography and gel filtration.

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Preventive Effect of Sugar-free Chewing Gum Containing Maltitol on Dental Caries in situ

  • Lee, Eun-Jung;Jin, Bo-Hyoung;Paik, Dai-Il;Hwang, In-Kyeong
    • Food Science and Biotechnology
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    • v.18 no.2
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    • pp.432-435
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    • 2009
  • The preventive effect of chewing gum containing maltitol, xylitol, gum base, and sugar on remineralization were investigated. The clinical study consisted of 8 weeks' randomized, double blind, controlled, cross-over clinical trials including 24 healthy adults had chew gum. After each test week, remineralization effect was evaluated by measuring microhardness and scanning electron microscopy (SEM). Microhardness of experimental chewing gum containing maltitol or xylitol was significantly higher than that of sugar gum (p<0.005). Images of SEM showed the remineralization effect of gum containing gum base, maltitol, or xylitol compared with sugar gum. Maltitol and xylitol gums were more effective in remineralization than sugar gum. It was concluded that maltitol and xylitol can be used as sugar substitute to prevent dental caries.

Effects of pore structures on electrochemical behaviors of polyacrylonitrile-based activated carbon nanofibers by carbon dioxide activation

  • Lee, Hye-Min;Kim, Hong-Gun;An, Kay-Hyeok;Kim, Byung-Joo
    • Carbon letters
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    • v.15 no.1
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    • pp.71-76
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    • 2014
  • Activated carbon nanofibers (ACNF) were prepared from polyacrylonitrile (PAN)-based nanofibers using $CO_2$ activation methods with varying activation process times. The surface and structural characteristics of the ACNF were observed by scanning electron microscopy and X-ray diffraction, respectively. $N_2$ adsorption isotherm characteristics at 77 K were confirmed by Brunauer-Emmett-Teller and Dubinin-Radushkevich equations. As experimental results, many holes or cavernous structures were found on the fiber surfaces after the $CO_2$ activation as confirmed by scanning electron microscopy analysis. Specific surface areas and pore volumes of the prepared ACNFs were enhanced within a range of 10 to 30 min of activation times. Performance of the porous PAN-based nanofibers as an electrode for electrical double layer capacitors was evaluated in terms of the activation conditions.

Facile Hydrothermal Synthesis and Characterization of the $CeO_2$ Nanorings

  • Arul, N. Sabari;Kim, Tae Whan;Mangalaraj, Devanesan
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.455-455
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    • 2013
  • $CeO_2$ nanorings were synthesized by using a surfactant free hydrothermal method. The surface morphology, structural and optical properties of the synthesized $CeO_2$ was investigated by using scanning electron microscopy (SEM), X-ray diffraction (XRD), and ultraviolet-visible (UV) spectroscopy measurements. SEM images showed that the surface morphology of the formed $CeO_2$ appeared as nanorings. The XRD pattern of $CeO_2$ nanorings showed the presence of the polycrystalline $CeO_2$ phase readily indexed to the cubic fluorite structure of the $CeO_2$. The mean crystallite size of the $CeO_2$ was calculated using the Scherrer equation from the XRD line broadening of the (111) planes of the cubic $CeO_2$. The UV-Visible spectroscopy spectrum of the $CeO_2$ nanorings exhibited a strong UV absorption band around 350 nm.

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Fabrication of amorphous carbon thin film using laser ablation technique (레이저 층착법에 의한 비정질 탄소계 박막의 제작)

  • ;;;K. Oura
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11a
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    • pp.484-487
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    • 2001
  • Amorphous carbon thin films were deposited using laser ablation technique on Si(100) substrates at different temperatures. In this study, effects of the substrate temperature on the properties of amorphous carbon films were systematically investigated. The surface morphologic and structural properties of the films were studied by scanning electron microscopy (SEM) and raman spectroscope, respectively. With increasing of the substrate temperature, the surface morphologies were changed singnificantly. Moreover the intensity ratio of D-band and G-band and the full width at half maximum of these bands were dependent on substrate temperatures.

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