• Title/Summary/Keyword: microscopic structure

Search Result 522, Processing Time 0.022 seconds

Interconnected meso/microporous carbon derived from pumpkin seeds as an efficient electrode material for supercapacitors

  • Gopiraman, Mayakrishnan;Saravanamoorthy, Somasundaram;Kim, Seung-Hyun;Chung, Ill-Min
    • Carbon letters
    • /
    • v.24
    • /
    • pp.73-81
    • /
    • 2017
  • Interconnected meso/microporous activated carbons were prepared from pumpkin seeds using a simple chemical activation method. The porous carbon materials were prepared at different temperatures (PS-600, PS-700, PS-800, and PS-900) and demonstrated huge surface areas ($645-2029m^2g^{-1}$) with excellent pore volumes ($0.27-1.30cm^3g^{-1}$). The well-condensed graphitic structure of the prepared activated carbon materials was confirmed by Raman and X-ray diffraction analyses. The presence of heteroatoms (O and N) in the carbon materials was confirmed by X-ray photoemission spectroscopy. High resolution transmission electron microscopic images and selected area diffraction patters further revealed the porous structure and amorphous nature of the prepared electrode materials. The resultant porous carbons (PS-600, PS-700, PS-800, and PS-900) were utilized as electrode material for supercapacitors. To our delight, the PS-900 demonstrated a maximum specific capacitance (Cs) of $303F\;g^{-1}$ in 1.0 M $H_2SO_4 $ at a scan rate of 5 mV. The electrochemical impedance spectra confirmed the poor electrical resistance of the electrode materials. Moreover, the stability of the PS-900 was found to be excellent (no significant change in the Cs even after 6000 cycles).

Morphological Aspects of Water Treeing in $Co^{60}$ $\gamma$-ray Irradiated Polyethylene ($Co^{60}$ $\gamma$-선으로 조사된 Polyethylene에서 수트리 현상의 구조적 측면에 관한 연구)

  • Lee, B.W.;Kim, J.T.;Koo, J.Y.;Ryu, B.H.
    • Proceedings of the KIEE Conference
    • /
    • 1991.11a
    • /
    • pp.435-438
    • /
    • 1991
  • This work is aimed to clarify the effect of only crosslinking of polyethylene on the water tree propagation and thus the crosslinking of LDPE was made by use of $Co^{60}$ $\gamma$-ray irradiation at room temperature. For this purpose, before water tree testing under same test conditions, injection molded samples were made of LDPE using CNRS laboratory model and also some of them were irradiated under different dose rate for crosslinking. Afterwards, the aged specimens were put into microscopic investigation as a mean to compare their different morphological aspects by use of SEM for the fractured surface. The SEM observation points out that the untreed region in the irradiated PE shows the densed structure whereas that in the LDPE is not closely packed. Also in the water treed region of LDPE, the density and the dimension of voids are higher than those in irradiated PE. Based on our results, it seems that the difference in the PE structure could sufficiently contribute to cause the different water tree propagation of these materials.

  • PDF

Spermatogenesis and its fine structure of the seminiferous epithelium in the Jindo dog (진도견(珍島犬) 정세관상피(精細管上皮)의 정자발생(精子發生)과 미세구조(微細構造))

  • Kim, Yong-hwan;Park, Young-seok
    • Korean Journal of Veterinary Research
    • /
    • v.33 no.1
    • /
    • pp.23-36
    • /
    • 1993
  • To investigate the cycle and relative frequences and the fine structure of seminiferous epithelia in mature Jindo dogs, histologic study was performed. The results obtained were summarized as follows; 1. Type A spermatogonia appeared approximately 1.6 times as many at stage II as compared to stage I while type In spermatogonia appeared small amount in stage III, IV and V. type B spermatogonia were found during the stage VI to VIII, though not detectable during stage I to V. The type B spermatogonia divided at stage VII to produce the preleptotene primary spermatocytes at stage VIII. The number of primary spermatocytes of the leptotene phase markedly increased during stage I to II, and the primary spermatocytes of the pachytene phase were shown the least in number at stage IV. The secondary spermatocytes could be seen only at stage IV. 2. The relative frequencies of each stage from stages I to VIII of the cycle of seminiferous epithelia were 31.6, 11.9, 10.0, 3.2, 8.2, 10.1, 11.7 and 13.2% respectively. 3. On electron microscopic observations, acrosomal vesicle of spermatids appeared larger though the bulk of germ cells were the morphologically same as those of the other animal species. Thread line structures light microscopically observed in the cytoplasm of Sertoli cell were the longitudinal orientation of mitochondria.

  • PDF

A MICROSCOPIC STUDY OF THE EFFECTS OF EXPERIMENTAL RICKETS ON THE DENTAL STRUCTURE OF RATS (실험적구루병에서 백서 치아조직 변화에 관한 현미경학적 연구)

  • Choi, Don-Ok;Lee, Jong-Gap
    • Journal of the korean academy of Pediatric Dentistry
    • /
    • v.7 no.1
    • /
    • pp.75-83
    • /
    • 1980
  • Rickets is not the deposite of minerals in the skeletal tissue and the retardation of skeletal growth in growing in growing animals. This study was undertaken to investigate the histologic effects of experimental rickets on the dental structure of the albino rats, and to show the relationship between the histological effects and the pulpal disease which induced premature loss of the primary teeth. This study was based on material obtained from 40 white rats that were placed on a rachitogenic diet for a period 1 to 56 days after weaning (at 24 days). In addition, a study was made of 25 litter mates, 24 to 80 days, that were fed a normal diet. The following results were obtained: 1. Enamel formation and calcification showed no significant changes and no hypoplasia. 2. Dentin formation and calcification was retarded and disturbed. In the experimental group, predentin/calcified dentin was remarkablly increased. 3. Newly formed dentin showed interglobular texture (less homogenous calcification) and the predentin was significantly wider and thicker, and there was an irregular wave in the basal portion of the rat's incisors. 4. In cementum, Matrix formed at almost a normal rate but calcification was defective. So cementoid tissue was increasesd. 5. The formation of the alveolar bone was at almost a normal rate but calcification was retarded. The trabecular bone was filled with osteoid tissue and thicker than in normal groups.

  • PDF

A Study on the Baroque Characteristics Expressed in Architecture by Richard Meier (리처드 마이어 건축에 표현된 바로크적 특성 연구)

  • Han, Myoung-Sik
    • Korean Institute of Interior Design Journal
    • /
    • v.22 no.3
    • /
    • pp.127-134
    • /
    • 2013
  • Baroque is fundamentally in contrast with renaissance style classicism, which attempted to fix a world view itself as the value of perpetuity. Furthermore, it is interpreted as a topic of incompletion or transformation that is not defined or is not exemplary and which may be enjoyed by people in the classical life, which requires a microscopic concept in contrast with dualism, the central axis of western civilization, namely, rational lucidity. Also, such characteristics are estimated to serve as a lubricant in life while going beyond the formal aesthetic level of art even from a contemporary perspective, and to play a productive role and to have potential. Consequently, this paper assumed that the concepts expressed by the 20th century US contemporary architect Richard Meier of a complex space, namely architectural formative vocabularies such as overlapping, interpenetration, collision, and collage style mixture created by a layered structure, in his architecture are in common with the double surface technique and juxtaposition of a flat structure of Baroque architecture. Then, the paper analyzed and considered the characteristics. The paper considered the following two issues: Such Baroque style formal principle is reinterpreted against a backdrop in which his architectural flow based on the domino theory of Le Corbusier became established as his own unique architectural feature, and it may be proposed as one big flow that enables us to seek again modernistic architecture that attempts to make an architectural space absolute as an atypical formal contour.

Evaluation of Statistical distribution of extreme values of Graphite in Ductile Cast Iron by Image Analyzer (구상흑연주철재의 화상해석에 의한 흑연의 극치통계 평가)

  • Yoon, Myung-Jin
    • Journal of the Korean Society of Manufacturing Process Engineers
    • /
    • v.9 no.6
    • /
    • pp.71-77
    • /
    • 2010
  • Although the problems of defects and nonmetallic inclusion in metal fatigue are very complicated, it is particularly important to view these problems from the perspective that defects and inclusions are virtually equivalent to small cracks. This concept will help one to understand various fatigue phenomena caused by Ductile Cast Iron. For different ferrite-pearlite matrix structure, containing more than 90% spheroidal ratio of graphite, GCD 45-3, GCD 50, GCD 60 series and 70%, 80%, 90% spheroidal ratio of graphite, GCD 40, GCD 45-1, GCD 45-2 series, this paper has carried out image analyzer, estimated maximum and mean size of graphite, investigated correlation. It was concluded as follows. (1) A good quality of Ductile cast iron using in this experiment, the graphite was separated well. The effect of the interaction by graphite was verified by microscopic observation and by fracture mechanics investigation in surface, interior of the specimen. (2)${\sqrt{area}}_{max}$ of graphite can be used to predict fatigue limit of Ductile Cast Iron. The Statistical distribution of extreme values of ${\sqrt{area}}$ may be used as a guide line for the control of inclusion size in the steel making processes.

$^{11}B$ Nuclear Magnetic Resonance Study of Calcium-hexaborides

  • Mean, B.J.;Lee, K.H.;Kang, K.H.;Lee, Moo-Hee;Lee, J.S.;Cho, B.K.
    • Journal of the Korean Magnetic Resonance Society
    • /
    • v.7 no.2
    • /
    • pp.80-88
    • /
    • 2003
  • We have performed $^{11}$ B nuclear magnetic resonance (NMR) measurements to microscopically investigate an electronic structure of the ferromagnetic state in three different compositions of calcium-hexaboride single crystals. Although the crystal structure of Ca $B_{6}$ is cubic and three NMR lines may be expected for the nuclear spin 3/2 of $_{11}$ B, a larger number of NMR resonance peaks have been observed. The frequency and intensity of those peaks distinctively changes depending on the angle between crystalline axis and magnetic field. Analyzing this behavior, we find that the electric field gradient(EFG) tensor at the boron has its principal axis perpendicular to the six cubic faces with a quadrupole resonance frequency $v_{Q}$ 600 kHz. Even though the magnetization data highlight the ferromagnetic hysteresis, $^{11}$ B NMR linewidth data show no clear microscopic evidence of the ferromagnetic state in three different compositions of Ca $B_{6}$ single crystals.s.

  • PDF

Characterization and Taxonomic Classification of S85, a new Microsporidia, isolated from the Silkworm, Bombyx mori L. (가잠에서 분리된 새로운 미포자충(S85)의 특성 및 분류학적 위치(1) - 포자의 미세구조 -)

  • Jo, Se-Yun;Son, Hae-Ryong;Im, Jong-Seong
    • Journal of Sericultural and Entomological Science
    • /
    • v.31 no.2
    • /
    • pp.113-120
    • /
    • 1989
  • A new microsporidia (S85) was isolated from the silkworm, Bombyx mori L. in Suwon, Korea in 1985. The electron microscopic observation of the fine structure of the spore was studied for the characterization of the new microsporidia and its taxonomic position. The sporewall was composed of three different electron dense layers and the spore surface was rouph and wrinkled. The polaroplast has two parts which differed in the arrangement of the lamellae. The polarfilament was isofilar with thirteen coils and it was consisted of eight concentric layers of different electron density. The spore contained a single nucleus and the pansporoblast appeared as a thin ballon-like structure surrounding the spore. The membrane was generally smooth and shown occationally wrinkled.

  • PDF

Atg3-Mediated Lipidation of Atg8 Is Involved in Encystation of Acanthamoeba

  • Moon, Eun-Kyung;Chung, Dong-Il;Hong, Yeon-Chul;Kong, Hyun-Hee
    • Parasites, Hosts and Diseases
    • /
    • v.49 no.2
    • /
    • pp.103-108
    • /
    • 2011
  • Autophagy is a catabolic process involved in the degradation of a cell's own components for cell growth, development, homeostasis, and the recycling of cellular products. Autophagosome is an essential component in the protozoan parasite during differentiation and encystation. The present study identified and characterized autophagy-related protein (Atg) 3, a member of Atg8 conjugation system, in Acanthamoeba castellanii (AcAtg3). AcAtg3 encoding a 304 amino acid protein showed high similarity with the catalytic cysteine site of other E2 like enzymes of ubiquitin system. Predicted 3D structure of AcAtg3 revealed a hammer-like shape, which is the characteristic structure of E2-like enzymes. The expression level of AcAtg3 did not increase during encystation. However, the formation of mature cysts was significantly reduced in Atg3-siRNA transfected cells in which the production of Atg8-phosphatidylethanolamine conjugate was inhibited. Fluorescent microscopic analysis revealed that dispersed AcAtg3-EGFP fusion protein gathered around autophagosomal membranes during encystation. These results provide important information for understanding autophagic machinery through the lipidation reaction mediated by Atg3 in Acanthamoeba.

ULTRAVIOLET MICROSCOPIC STUDY ON LIGNIN DISTRIBUTION IN THE FIBER CELL WALL OF BCTMP

  • Seung-Lak YooN;Yasuo KOJIMA;Lee, Seon-Ho
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
    • /
    • 1999.04b
    • /
    • pp.375-380
    • /
    • 1999
  • In order to improve the optical properties of high yield pulp, bleached chemi-thermo-mechanical pulp (BCTMP) was produced from CTMP of Betula maximowicziana Regel by two staged ozone-hydrogen peroxide bleaching. This pulp was used for the evaluation of the improvement of optical properties, chemical characteristics of lignin in fiber, and the relationship between lignin and optical properties in fiber cell wall. By hydrogen peroxide treatment, the brightness was improved, but the post color number (PC No.) was not. There was little improvement on optical properties by ozone treatment, but his could be solved by using two staged ozone-hydrogen peroxide bleaching. The hydrogen peroxide treatment did not make nay change on chemical characteristics of lignin in cell wall, but by ozone treatment, it was found that the non-aromatic conjugated structure was existed in the surface of cell wall, but this could be removed by hydrogen peroxide treatment in two staged ozone-hydrogen peroxide treatment. Therefore, the optical properties was significantly improved due to the removal of non-aromatic conjugated structure.