• 제목/요약/키워드: microscopic structure

검색결과 523건 처리시간 0.022초

동합금(銅合金)의 조직상(組織像)에 관(關)한 연구(硏究) (MICROSCOPIC STUDY ON THE STRUCTURE CHANGE OF COPPER BASED ALLOY TO COLD ROLLING AND ANNEALING)

  • 김영해
    • Restorative Dentistry and Endodontics
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    • 제4권1호
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    • pp.7-9
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    • 1978
  • Brass specimen, copper based alloy was prepared in cubic form about $1cm{\times}1cm{\times}1cm$ in volume. The specimens were mechanically compressed in one direction until the dimension distorted to 20%, 40%, 60% and 80% in length. The compressed specimens with 80% distorted in length were then heat treated in $200^{\circ}C$, $300^{\circ}C$, $400^{\circ}C$, $500^{\circ}C$ and $600^{\circ}C$ for 30 minutes. Microscopic examination was made on both compressed and heat treated specimens. The results obtained from the study were as follows: 1. Grain boundary and twin phenomenon was clearly seen in 0% and 20% compressed cases. Slip bands was appeared in 40% cases and distributed equally as well as twin. 2. The first evidence of slip bands was observed in 20% and the bands grew thicker and denser as the compression increased. 3. The density of the bands were reduced after annealing in $200^{\circ}C$ and completely disappeared at $300^{\circ}C$ cases. 4. Recrystallization was noticed unevenly in $300^{\circ}C$ cases and the evidence of twin was observed in these crystallized area. 5. In $400^{\circ}C$ cases the grain boundary was evenly found and the twin phenomenon was clearly observed. Grain boundary and twin was noticeably formed in size according to the annealing temperature increased.

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계통교통신호체계에서의 지체특성과 최적신호주기에 관한 연구 (Optimum Chycle Time and Delay Caracteristics in Signalized Street Networks)

  • 이광훈
    • 대한교통학회지
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    • 제10권3호
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    • pp.7-20
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    • 1992
  • The common cycle time for the linded signals is usually determined for the critical intersecion, just because the cpacity of a signalized intersection depends on the cycle time. This may not be optimal since the interactions between the flow and the spatial structure of the route or the area are disregarded in this case. It is common to separate the total delay incurred at signals into two parts, a deterministic or uniform delay and a stochastic or random delay. The deterministic delays and the stochastic delays on the artery particularly related to signal cycle time. For this purpose a microscopic simulation technique is used to evaluate deterministic delays, and a macroscopic simulation technique based on the principles of Markov chains is used to evaluate stochastic delays with over flow queue. As a result of investigating the relations between deterministic delays and cycle time in the various circumstances of spacing of signals and traffic volume. As for stochastic delays the resalts of comparisons of the macroscopic simulation and Newell's approximation with the microscopic simulation indicate that the former is valid for the degree of saturation less than 0.95 and the latter is for that above 0.95. Newell's argument that the total stochastic delay on an arterial is dominated by that at or caused by critical intersection is certified by the simulation experiments. The comprehensive analyses of the values of optimal cycle time with various conditions lead to a model. The cycle time determined by this model shows to be approximately 70% of that calculated by Webster's.

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한의학의 발전 방향 검토 (The Review of the Direction of Improvement of Oriental Medicine)

  • 신길조
    • 대한중풍순환신경학회지
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    • 제18권1호
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    • pp.1-11
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    • 2017
  • It is difficult to combine oriental and western medicine. Each medicine has a different academic background, perspective on the world, and studying methodology. The claim that two paradigms can not be combined is not obtained from an actual verification, but this means it is so hard to combine two medicines having different backgrounds. The amalgamation of oriental and western medicine should be phased in on the basis of the continuous reciprocal understanding and commitment. First, the strength and weakness of each medicine over the treatment and research are required to be identified. Then, a few complementary areas can be chosen enabling a trial of fusion on a small scale. A cycle of problem solving and a new research can be set by analyzing research results obtained through the implementation over a period of time. In other words, the researchers of oriental and western medicine should repeat a continuous and gradual complementary research process by identifying issues to be improved and complemented through a consensus. Once the methodology obtained through the process of problem solving and proficient implementation is established in a stable condition, a method to widen the fusion area by expanding the operating area and implementation method can be chosen. However, the integral system of oriental medicine shouldn't be substituted by mechanical idea or reductionism. What should be done primarily for oriental medicine is to objectify things through quantification. In particular, the oriental treatment should accept the microscopic diagnosis to determine the structure and observe the biochemical change.

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$LiK_{1-x}Rb_{x}SO_{4}(x=0.1,\;0.2)$의 결정구조 분석 (Structure Analysis of Mixed Crystals, $LiK_{1-x}Rb_{x}SO_{4}(x=0.1,\;0.2)$)

  • 김진규;김윤중;김해진;서일환
    • 한국결정학회지
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    • 제16권2호
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    • pp.75-80
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    • 2005
  • [ $LiK_{1-x}Rb_{x}SO_{4}(x=0.1,\;0.2)$ ]의 결정을 313K에서 수용액법으로 성장시켰다. 결정구조는 X-ray 회절법을 이용하여 동일한 공간군 $P6_{3}(#173)$에서 수행되었다. 동일한 대칭성을 가진 두 화합물은 각각 3회 회전축에 위치하고 있는 Li과 $SO_{4}^{2-}$ 이온들이 서로 무한히 연결된 3차원적 그물구조를 형성하고 있고, 6회 회전축에 위치하고 있는 K와 Rb원자들은 각각 12개와 15개의 O 원자들과 배위를 이루고 있다. K와 Rb의 점유도는(0.91 : 0.09), (0.77 : 0.23)으로 정밀화 하였을 때 가장 안정된 상태에 도달하였다.

생쥐 치아의 화학적 조성, 미세구조 및 Hydroxyapatite 구조 분석 (Analysis of Chemical Composition, Microstructure and Hydroxyapatite Structure for Mouse Teeth)

  • 김은경;전태훈;김창연;남승원;송경;이상길;김윤중
    • Applied Microscopy
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    • 제40권3호
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    • pp.147-154
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    • 2010
  • 본 연구에서는 광학 및 전자현미경 관찰과 전자현미분석을 수행하여 쥐 치아의 미세구조, 화학 조성 및 hydroxyapatite의 결정구조를 파악하였다. 치아의 겉 표면을 둘러싸고 있는 법랑질은 막대들이 일정하게 배열된 구조이며 결정도가 높고 Ca이 많이 침착되어 있다. 그에 비해 상아질은 상아세관이 통과하는 원형의 구멍이 고루 분포되어 있는 스펀지 구조이며 유기질의 존재로 인해 Mg의 분포가 법랑질에 비해 상대적으로 높게 나타났다. Hydroxyapatite 결정들은 법랑질에서는 크기가 큰 막대 형태로 나타났으나 상아질에서는 크기가 작은 침상 형태로 나타났으며, 각 조직의 결정도와 유기질의 유무에 따라 전자회절패턴의 차이를 보였다.

비교적 두꺼운 결정으로부터 얻은 일련의 비 초점 단계의 고전압 HRTEM 영상들에 대한 IWFR 분석의 유용성 실험 (Experiment of Usefulness of IWFR Analysis for High Voltage HRTEM Images with a Series of Defocus Steps Obtained from a Relatively Thick Crystal)

  • 오상호;김윤중;김황수
    • Applied Microscopy
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    • 제38권4호
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    • pp.363-374
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    • 2008
  • 이 논문에서는 비교적 두꺼운 결정에 대한 일련의 고 분해 영상들에 대한 IWFR 분석의 유용성을 실험하였다. 이를 위해 JEOL ARM 1300S를 이용하여 실리콘 결정의 30 nm 두께의 [01-1] 방위와 35 nm 두께의 [11-2]에 대한 일련의 비 초점 단계의 고 분해 영상들을 관찰하였다. 이로부터 두꺼운 시료에 대해서도 IWFR 분석 결과로부터 결정 밑 표면의 파동함수를 얻을 수 있음이 밝혀졌다. 그러나 강한 동역학적 산란에 의한 효과 때문에, 이 함수의 영상패턴은 시료의 원자열 구조의 패턴을 다만 정성적으로만 반영하고 있다. 그럼에도 불구하고 이 패턴은 결정구조의 중요한 단서를 제공할 것임은 의심의 여지가 없다

Toughness and microscopic pore structure analysis of pasture fiber recycled concrete

  • Hailong Wang;Lei Wang;Hong Yang
    • Advances in concrete construction
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    • 제16권3호
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    • pp.141-153
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    • 2023
  • In order to develop and take full advantage of pasture fiber and waste concrete, this article studied how different amounts of pasture fiber influenced the toughness and pore structure of concrete with different replacement rates of recycled fine aggregate. Pasture fiber recycled concrete constitutive equations were established under idealized stiffness and toughness damage rate, based on fracture energy and damage mechanics theories. The relationship between pore structure and toughness was studied utilizing nuclear magnetic resonance and fractal theory. The toughness of text groups (0% (JZ), 10% (ZS10), 20% (ZS20)) first increased and then decreased with increasing amounts of pasture fiber, based on the damage rate of toughness. The toughness of concrete samples with recycled fine aggregate and pasture fiber is negatively correlated to the fractal dimension of small and medium-sized pores with a pore size of 0-500 nm. At a replacement rate of 10% of the recycled fine aggregate, the fractal dimension of the air voids (r: 500-9000 nm, i.e., Lg(r) ∈ [2.7, 3.9]) shows a gradual decrease with the increase of grass fiber dosage, indicating that with such a replacement rate of the recycled fine aggregate, the increase of pasture fiber can reduce the complexity of the pore structure of the air voids (500-9000 nm).

트럭용 커넥팅 로드 소재의 내부 품질에 따른 기계적 특성 연구 (A study on the Mechanical Characteristics by the Internal Quality of Connecting Rod Materials for Trucks)

  • 김동현
    • 한국생산제조학회지
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    • 제7권1호
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    • pp.75-81
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    • 1998
  • We have studied internal quality including chemical compositions, microscopic structure and nonmetallic inclusion of test materials. We have analyzed tensile strength value, hardness value, impact value etc. In analyzing internal quality, all of the test materials showed typical ferrite+pearlite structure. But nonmetallic inclusion showed oxide and sulfide inclusions in medium carbon steels, and sulfide inclusion is S-free cutting steels. In ca+ S-free cutting steels, the calcium aluminate and sulfide complex inclusion had low-melting points as deformation of sulfide and oxide inclusion is existed. It was found that tensile strength and hardness give maximum value in medium carbon steels, where as minimum in Ca + -free cutting steels. But values of elongation, reduction of area impact are reverse. Fracture surface of impact specimen is ductile in free cutting steels but brittle in medium cabon steels.

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An atomistic model for hierarchical nanostructured porous carbons in molecular dynamics simulations

  • Chae, Kisung;Huang, Liping
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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    • pp.403.2-403.2
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    • 2016
  • Porous materials play a significant role in energy storage and conversion applications such as catalyst support for polymer electrolyte membrane fuel cell. In particular, hierarchical porous materials with both micropores (poresize, ${\delta}$ < 2 nm) and regularly arranged mesopores (2 nm < ${\delta}$ < 50 nm) are known to greatly enhance the efficiency of catalytic reactions by providing enormous surface area as well as fast mass transport channels for both reactants and products from/to active sites. Although it is generally agreed that the microscopic structure of the porous materials directly affects the performance of these catalytic reactions, neither detailed mechanisms nor fundamental understanding are available at hand. In this study, we propose an atomistic model of hierarchical nanostructured porous carbons (HNPCs) in molecular dynamics simulations. By performing a systematic study, we found that structural features of the HNPC can be independently altered by tuning specific synthesis parameters, while remaining other structures unchanged. In addition, we show some structure-property relations including mechanical and gas transport properties.

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Trichoderma koningii의 conidiospore로부터의 원형질체 생성에 관한 전자현미경적 연구 (Electron Microscopic Study of Protoplast Formation from the Conidiospore of Trichoderma koningii)

  • 박희문;임헌만;홍순우;하영칠
    • Applied Microscopy
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    • 제14권2호
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    • pp.38-51
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    • 1984
  • Fine structure of dormant and swollen conidiospore from Trichoderma koningii and the mechanism of protoplasting from the conidiospore were studied by scanning and transmission electron microscopy. The cell wall of dormant conidiospore was two-layered structure which consisted of electron dense outer layer and electron transparent inner layer. After 8.5 hrs incubation. the conidiospore was swollen and the outer layer of cell wall shown unequal thickness and partial breakage. Protoplast was released through the pore which has been formed by the breakage of outer layer and dissolution of newly synthesized cell wall for germ-tube formation. Swollen conidiospore and protoplast in releasing process contained various cell organelles and vacuoles with electron dense materials. The protoplast contained looser cytoplasm and had no cell wall materials outside of plasmamembrane.

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