• Title/Summary/Keyword: microscopic characteristics

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ULTRAVIOLET MICROSCOPIC STUDY ON LIGNIN DISTRIBUTION IN THE FIBER CELL WALL OF BCTMP

  • Seung-Lak YooN;Yasuo KOJIMA;Lee, Seon-Ho
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 1999.04b
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    • pp.375-380
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    • 1999
  • In order to improve the optical properties of high yield pulp, bleached chemi-thermo-mechanical pulp (BCTMP) was produced from CTMP of Betula maximowicziana Regel by two staged ozone-hydrogen peroxide bleaching. This pulp was used for the evaluation of the improvement of optical properties, chemical characteristics of lignin in fiber, and the relationship between lignin and optical properties in fiber cell wall. By hydrogen peroxide treatment, the brightness was improved, but the post color number (PC No.) was not. There was little improvement on optical properties by ozone treatment, but his could be solved by using two staged ozone-hydrogen peroxide bleaching. The hydrogen peroxide treatment did not make nay change on chemical characteristics of lignin in cell wall, but by ozone treatment, it was found that the non-aromatic conjugated structure was existed in the surface of cell wall, but this could be removed by hydrogen peroxide treatment in two staged ozone-hydrogen peroxide treatment. Therefore, the optical properties was significantly improved due to the removal of non-aromatic conjugated structure.

Evaluation of AR Characteristics on Microscopic Fracture Mechanism of A17075/CERP Hybrid Composite (Al 7075/CFRP 하이브리드 복합재료의 미시적 파괴특성에 대한 AE특성평가)

  • 이진경;이준현;윤한기
    • Composites Research
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    • v.15 no.5
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    • pp.1-6
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    • 2002
  • When compared to other composite materials such as FRP and MMC, hybrid composite material is more attractive one due to the high specific strength and the resistance to fatigue. However, the fracture mechanism of hybrid composite material is extremely complicated because of the bonding structure of metals and FRP. Recently, nondestructive technique has been used to evaluate the fracture mechanism of these composite materials. In this study. AE technique has been used to clarify the fracture mechanism and the degree of damage for Al 7075/CFRP hybrid composite material. It was found that AE event, energy and amplitude among AE parameters were effective to evaluate fracture process of Al 7075/CFRP composite material. In addition, the relationship between the AE signal and the characteristics of failure surface using optical microscope was discussed.

Characteristics of the Bacteriophage Resistance Mechanism of Kactococcus lactis subsp.cremoris ATCC 11602-A1 (Lactococcus lactis subsp. cremoris ATCC 11602-A1의 Bacteriophage 저항성 기작에 관한 연구)

  • 이춘화;배인휴
    • Microbiology and Biotechnology Letters
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    • v.22 no.3
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    • pp.233-239
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    • 1994
  • The characteristics of the bacteriophage resistant Lactococcus lactis subsp. cremoris ATCC 11602-A1, the phage-resistant mutant of Lactococcus lactis subsp. cremoris ATCC 11602, was examined. Electron microscopic study of phage adsorption to A1 revealed that after 10 min. incubation of the host-phage mixture, A1 did not show phage adsorption, and after 60 min. did not show a real burst and the release of new phage particles which could be detected in the mixture of its parent strain and phage. However, the phage adsorption rate of A1 after SDS treatment increased to 98%. Moreover, when the cell walls from A1 and parent strain, and the polysaccharide(PS) and peptidoglycan(PG) of their cell wall were mixed with phage and incubated for 15 min., PS and PG from A1 did not bind phage, but only SD-treated cell wall bound phage, and the cell wall and PS of parent strain bound phage. Both A1 and parent strain treated with 0.2 N HCl-and 5% TCA(100$$C) did not bind phage. The results suggest that the phage receptor is still present in the cell wall of the A1, but a cell wall constituent hydrolyzed by SDS blocks phage adsorption by masking the phage receptor. It also suggests that the phage receptor of parent strain is associated with PS of the cell wall.

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Fracture Mechanism of Gas Turbine Compressor Blades in a Combined Cycle Power Plant (복합화력발전소 가스터빈 압축기 블레이드에 대한 손상원인 고찰)

  • Yang, Kyeong-Hyeon;Song, Oh-Seop;Cho, Cheul-Whan;Yun, Wan-No;Jung, Nam-Geun
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.20 no.11
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    • pp.1025-1032
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    • 2010
  • Gas turbine compressor blades used in a combined cycle power plant are possibly damaged and fractured during their operation. There are two possible causes of the failure of compressor blades; one is a defect of material quality which can be detected through some microscopic inspections for the fracture section, the other is high cycle fatigue problem caused by vibration and can be diagnosed by carrying out dynamic characteristics analysis for the blades. In this paper, in order to determine the cause of the failure of compressor blades in a combined cycle power plant, examination of the fracture section and the propagation mechanism of the crack via stress analysis are performed. Dynamic characteristics analysis via FRF estimation is also performed to identify the cause of failure.

Development of Retro-reflective Fiber(I) - Making of Slit Yarn and Manufacturing of Fabric using in the Warp Threads - (재귀반사 섬유의 개발(I) - Slit Yarn의 제조와 경사에 Slit Yarn 사용에 의한 직물제조 -)

  • Jeong, Dong-Seok;Park, Sang-Woon;Kweon, Il;Chun, Tae-Il
    • Textile Coloration and Finishing
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    • v.29 no.3
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    • pp.139-147
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    • 2017
  • In this study, interesting area of development is retro-reflective thin film and then slitting to form retro-reflective material to be conbined with other fibers to form having retro-reflective characteristics, which slitting yarn can then be to provide fabrics. Glass beads are microscopic spherical size with diameters ranging from several microns to several millimeters. Applying the effects of optical property, glass beads are consumed for road safety used to make traffic signs, safety clothing and others. Glass beads retro-reflective films can be turned into slit yarns through slitting yarn process. The slit yarns can be combined into textiles using diverse methods such as weaving to provide a fabric having retro-reflective characteristics. Lightness and Luminance was increased with decreasing of interval of slit yarn in the fabric. Also, the hue is shifted greenish and bluish with interval of slit yarn.

A study on the phase transition characteristics of the $Ba(La_{1/2} Nb_{1/2})O_3-Pb(Zr, Ti)O_3$ ceramics ($Ba(La_{1/2} Nb_{1/2})O_3-Pb(Zr, Ti)O_3$ 세라믹의 상전이 특성에 관한 연구)

  • 류기원;배선기;박인길;이영희
    • Electrical & Electronic Materials
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    • v.8 no.2
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    • pp.190-195
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    • 1995
  • Temperature dependences of the dielectric constant K(T), remanent polarization $P_{r}$, (T), effective birefringence overbar .DELTA.n(T), transmitted light intensity and quadratic electro optic coefficient R(T) of the two-stage sintered xBa(L $a_{1}$2/N $b_{1}$2/) $O_{3}$-(1-x)Pb(Z $r_{y}$ $Ti_{1-y}$) $O_{3}$(x=0.085, 0.09, 0.40.leq.y.leq.0.70) ceramics were investigated. Increasing the PbZr $O_{3}$ contents, the crystal structure of a specimen was changed from a tetragonal phase to a rhombohedral and cubic phase, and the phase transition was showed a diffuse phase transition(DPT) characteristics. In the compositions which located on the PE-FE phase boundary, the discrepancy was observed between the Curie temperature and temperature which a microscopic polarization and effective birefringence were disappeared.red.d.

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An Experimental Study on the Leakage Characteristics and Durability Evaluation of an LPLi Injector (LPLi 인젝터의 누설특성 및 내구평가에 관한 실험적 연구)

  • Choi, Young;Kim, Chang-Up;Oh, Seung-Mook;Kang, Kern-Yong
    • Journal of ILASS-Korea
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    • v.12 no.4
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    • pp.204-210
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    • 2007
  • The worldwide energy problem and global warming cause the need of alternative fuels which feature low carbon-dioxide emission and another energy source. Liquefied Petroleum Gas (LPG) is one of the alternative fuels widely used as domestic and transportational fuel. The third generation LPLi fuel supply system has merits in the increase of engine power and low emissions. The injectors used in LPLi system should overcome a leakage problem and satisfy the durability conditions. Therefore, 1000 hour durability test of the injectors was carried out throughout this research. First, the spray pattern and the penetration length of the selected injectors is graphically shown. Next, the leakage amount with respect to the injection cycle is introduced. Finally, the shapes of nozzle holder and nozzle tip after durability test was investigated by analyzing the microscopic image of the injector tip. The variation in the shape of nozzle tip mainly due to the residue of rubber materials is found to be the reason for leakage.

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Characteristics of Hydrothermal Chlorite and Its Interstratification with 7-${\AA}$ Phase in Rhyodacitic Tuff, Western Pusan, Korea (열수변질기원 녹니석과 이에 수반된 혼합층상 광물의 특징)

  • 추창오;김수진
    • Journal of the Mineralogical Society of Korea
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    • v.13 no.4
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    • pp.196-204
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    • 2000
  • We present characteristics of hydrothermal chlorite and its interstratification with 7-$\AA$ mineral phase that occur in the propylitic alteration zone of the Bobae sericite deposit formed in rhyodacitic tuff. Chlorite is found as disseminated fine-grained aggregate or replacement materials of precursor minerals such as Fe-oxides and amphibole. Based on X-ray diffraction(XRD), all chlorites belong to IIb polytype and the (060) reflections averaging $1.53~1.54\AA$ indicate a trioctahedral structure. Chemical compositions of chlorite show that the Fe/(Fe+Mg) values are mostly in the range of 0.44~0.53, and cation deficiencies in octahedral sites range from 0.06 to 0.37. Under scanning electron microscope(SEM) chlorite occurs as well-crystallized aggregates and is subparallely stacked in interstices or between grain boundaries of associated minerals. transmission electron microscopic(TEM) images reveal that chlorite shows regular layers with $14-\AA$ spacings, locally interstratified with $7-\AA$ or $21-\AA$ periodicities. The $21- \AA$ periodicity corresponds to the sum of the $d_{001}$ values of chlorite and $7-\AA$ phase. The chlorite packet coexisting with 7-$\AA$ layers displays abundant defects such as edge dislocations and layer terminations. Selected-area electron diffraction(SAED) indicates that chlorite and $7-\AA$ phase are randomly interstratified in the mixed-layer areas. We propose a lateral change of layers for the polymorphic transition of $7-\AA$ phase to chlorite.e.

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Experimental Study on Fatigue Crack Initiation and Propagation due to Fretting Damage in Press-fitted Shaft (압입축에 발생하는 프레팅 피로균열 발생 및 진전 특성 실험)

  • Lee, Dong-Hyong;Kwon, Seok-Jin;Choi, Jae-Boong;Kim, Young-Jin
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.6 s.261
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    • pp.701-709
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    • 2007
  • To clarify the characteristics of surface damage due to fretting in press-fitted shaft, experimental methods were applied to small scale specimen with different bending load condition. Fatigue tests and interrupted fatigue tests of press-fitted specimen were carried out by rotate bending fatigue test. Macroscopic and microscopic characteristics were examined using scanning electron microscope (SEM), optical microscope or profilometer. It is found that small fatigue cracks are nucleated early in life regardless of bending stress, and thus the most portion of fatigue life on press fits can be considered to be crack propagation process. Most of surface cracks are initiated near the contact edge, and multiple cracks are nucleated and interconnected. Furthermore, the fretting wear rates at the contact edge are increased rapidly at the initial stage of total fatigue life. It is thus suggested that the fatigue crack nucleation and propagation process is strongly related to the evolution of surface profile by fretting wear in press fits.

Characteristic Effects of Buffer Layers on Organic Light Emitting Devices

  • Park, Jae-Hoon;Lee, Yong-Soo;Kwak, Yun-Hee;Choi, Jong-Sun
    • KIEE International Transactions on Electrophysics and Applications
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    • v.11C no.3
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    • pp.43-48
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    • 2001
  • The stability and efficiency of organic light emitting devices are the most critical problems to be solved. The devices based on tris-8-(hydroxyquinoline) aluminum ($Alq_3$) and N,N-diphenyl-N,N-bis(3-methylphenyl)-1, 1-biphenyl-4,4-diamine (TPD) were used to study the effects of buffer layers on their characteristics. We have investigated the characteristic effects of CuPc (copper phthalocyanine) and pentacene buffer layers on the device characteristics, the (5${\sim}$20 nm thick) CuPc layers and the (10${\sim}$20 nm thick) pentacene layers were deposited. Efficiency was slightly improved and the turn-on voltages of the devices with the buffer layers were observed to have lower values than those of the devices without the buffer layers. It is believed that this result is attributed to the improvement of hole injection capability through the buffer layers into hole transport layer (HTL). We have also studied the atomic force microscopic images of the TPD layers deposited on the buffer layer and the bare ITO.

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