• Title/Summary/Keyword: micron size

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An Experimental Study on Enhancement of the Filter Efficiency by the Image Effect of Charged Particle (대전된 입자의 영상효과에 의한 필터효율 향상에 관한 실험적 연구)

  • Lee, Chang-Sun;Jeong, Hae-Young;Kim, Sang-Soo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.6
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    • pp.760-768
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    • 2000
  • Filter efficiency of electrically charged particle in uncharged fibrous filter was measured. In previous studies, the effect of charged particle on filter efficiency was investigated but there was difficulty in measuring of image effect that is appeared at the charged small particle. We could easily measure the image effect with charging small particles by photoelectric charging. The spark discharge aerosol generator and a differential mobility analyzer (DMA) were used to generate sub-micron monodisperse particles (${\leq}200$ nm). The generated particles were charged in photoelectric charging process using ultraviolet lamp and electric field. The filter efficiency of the charged particles, classified by another DMA, was measured in filter tester using a condensation nucleus counter (CNC) as function of particle diameter, particle charge and airflow velocity. It is shown that the filter efficiency increases with increasing charge number of the particle and is affected by particle size and flow velocity. Single fiber filter efficiency mainly depends on image force parameter and peclet number. The peclet number was not considered at previous other papers. We propose a modi fied experimental correlation as function of image force parameter and peclet number.

Comparative Study on Ejection Phenomena of Droplets from EHD Jet by Hydrophobic Coating of Nozzle (노즐의 소수성 코팅에 의한 EHD 제트의 액적 토출 현상 비교 연구)

  • Kim, Yong-Jae;Choi, Jae-Yong;Son, Sang-Uk;Ahn, Ki-Cheol;Keum, Hyun-Joon;Lee, Suk-Han;Byun, Do-Young;Ko, Han-Seo
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1742-1746
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    • 2008
  • An EHD (Electro-Hydro-Dynamic) jet for electrostatic inkjet head shows advantages to print micro-size patterns using various inks because it can generate sub-micron droplets and can use highly viscous inks. Thus, many researchers in industrial fields are concerned about the EHD jet in these days. Since the basic principle of the EHD jet is to form a droplet from an apex of meniscus at the end of the nozzle, the ejection mechanism can be changed by the shape of the meniscus. The stable ejection of the droplet is greatly affected by the shape of the meniscus which is also influenced by surface characteristics of the nozzle, electric potential and ink properties. Experiments have been performed using the nozzles with hydrophilic and hydrophobic coatings in this study. The hydrophobic nozzle forms the stable droplets in wider range of the electric potential than the hydrophilic nozzle does.

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Determination of the Uranium Backgrounds in Lexan Films for Single Particle Analysis using FT-TIMS technique

  • Park, Su-Jin;Park, Jong-Ho;Lee, Myung-Ho;Song, Kyu-Seok
    • Mass Spectrometry Letters
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    • v.2 no.2
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    • pp.57-60
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    • 2011
  • As background significantly affects measurement accuracy and a detection limit in determination of the trace amounts of uranium, it is necessary to determine the impurities in the Lexan detector film for single particle measurements by thermal ionization mass spectrometry coupled with fission track technique (FT-TIMS). We have prepared various micro sizes of the blank Lexan detector film using a micromanipulation technique for uranium measurements by TIMS. Few tens of fg of uranium background with no remarkable dependency on the film sizes were observed in the blank Lexan films with the sizes from $50{\times}50\;{\mu}m^2$ to $300{\times}300\;{\mu}m^2$. Based on the determination of the uranium background in the Lexan film, any background correction is necessary in the isotopic analysis of a uranium single particle with micron sizes when the particle bearing Lexan film is dissected with less than $300{\times}300\;{\mu}m^2$ size. The isotopic analysis of a uranium particle in U030 standard material using TIMS was carried out to verify the applicability of the Lexan film to the single particle analysis with high accuracy and precision.

Economic Evaluation through Thermal Efficiency Elevation in Hot Air Drying Tower (열풍건조로의 열효율 향상을 위한 개선방안 연구)

  • Kim, Dong-Kyu;Kum, Jong-Soo;Kim, Jong-Ryeol;Kim, Sang-Jin;Chung, Yong-Hyun;Kim, Dong-Kyu;Kong, Ki-Bong
    • Journal of Fisheries and Marine Sciences Education
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    • v.20 no.3
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    • pp.500-507
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    • 2008
  • Hot air drying is a method that let moistures evaporate by heat exchange between heating air and dry target. This way is dominating more than about 70% of dryers that the use extent is wide fairly, and is established in domestic than dryer that use conduction or radiation etc. Most of research about drying had been emphasized in size of device through analysis for these dry phenomenon plain, heating topology, and aspect of form and so on by dry target's special quality, and research about device development or waste heat withdrawal technology in energy utilization efficiency side is slight real condition. Therefore, in this study, Investigated numerically about thermal efficiency elevation that is leaned against as that change the temperature of inlet and outlet in heat exchanger of the hot air drying tower.

Ag-Cu Powders Prepared by Electrical Wire Explosion of Cu-plated Ag Wires (동도금한 은선재의 전기선폭발에 의해 제조한 Ag-Cu분말)

  • Kim, Won-Baek;Park, Je-Shin;Suh, Chang-Youl
    • Journal of Powder Materials
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    • v.14 no.5
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    • pp.320-326
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    • 2007
  • Ag-Cu alloy nano powders were fabricated by the electrical explosion of Cu-plated Ag wires. Ag wires of 0.2mm diameter was electroplated to final diameter of 0.220 mm and 0.307 mm which correspond to Ag-27Cu and Ag-68Cu alloy. The explosion product consisted of equilibrium phases of ${\alpha}-Ag$ and ${\beta}$-Cu. The particle size of Ag-Cu nano powders were 44 nm and 70 nm for 0.220 mm and 0.307 mm wires, respectively. The Ag-Cu nano powders contained less Cu than average value due to higher sublimation energy compared to that of Ag. As a result, micron-sized spherical particles formed from liquid droplets contained higher Cu content.

Formation of CH3NH3PbBr3 Perovskite Nanocubes without Surfactant and Their Optical Properties

  • Kirakosyan, Artavazd;Yun, Seokjin;Kim, Deul;Choi, Jihoon
    • Journal of the Korean institute of surface engineering
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    • v.51 no.1
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    • pp.79-85
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    • 2018
  • We systematically investigated the optical properties of sub-micron sized methylammonium lead tribromide ($CH_3NH_3PbBr_3$) cubes in the range of 100 to 700 nm, which were prepared by a surfactant-free precipitation method. We found that despite the strong absorbance, their photoluminescence quantum yield (PLQY) is very low as 0.009~0.011 % for whole range of sizes. Surfactant-free synthesis approach results in nanocubes that has no surface passivating reagents (e.g. surfactants) on their surface. As-prepared particles contain a large number of surface defects that may cause the low PLQY. The role of the surface defects were investigated in their photoluminescence decay process, which can be correlated with the particle size. Larger particles are characterized by a slower decay rate compared to smaller particles due to a large number of surface defects in the smaller particles that trap more excitons in the fluorescence decay process. These experimental results provide new insights into the fundamental relationship between surface state and optical properties.

Thermal and Mineralogical Characterization of Ca-Montmorillonite from Gampo Area (감포지역(甘浦地域) Ca-몬모릴로나이트의 열적(熱的) 및 광물학적(鑛物學的) 특성(特性))

  • Moon, Hi-Soo;Choi, Sun Kyung;Kim, Moon Young
    • Economic and Environmental Geology
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    • v.21 no.2
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    • pp.175-184
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    • 1988
  • Ten under 2 micron size fractions of the montmorillonite from Yongdongri area, Gyeongsangbug-Do were studied using X-ray powder diffraction, cation exchange measurement, differential thermal analysis, thermogravimetric analysis, differential thermal scanning calorimetry and chemical analysis. Montmorillonites occurring at same deposit show limited variation in chemical composition whereas in thermal properties they do not. Their dehydroxylation endothermic peaks are "abnormal" type with a small range of variation of peak temperature reflecting tetrahedral substitution of Al for Si. Data from DSC show that divalent-cation saturated montmorillonite has relatively a higher endothermic heat capacity than monovalent-cation saturated montmorillonite, indicating that cations with higher electronegativity hold more water molecules.

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Fabrication of Electrostatic Electron Lens for Electron Beam Microcolumn using the Laser Micromachining (레이저 미세가공 기술을 이용한 초소형 전자빔 장치용 정전장 전자렌즈의 제작)

  • Ahn, Seung-Jun;Kim, Dae-Wook;Kim, Ho-Seop;Kim, Yeong-Jeong;Lee, Yong-San
    • Korean Journal of Materials Research
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    • v.11 no.9
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    • pp.792-796
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    • 2001
  • For electron beam lithography and SEM(scanning electron microscopy) applications, miniaturized electrostatic lenses called a microcolumn have been fabricated. In this paper, we report the fabrication technique for 20~30$\mu\textrm{m}$ apertures of electron lenses based on silicon and Mo membrane using an active Q-switched Nd:YAG laser. Experimental conditions of laser micromachining for silicon and Mo membrane are improved. The geometrical structures, such as the diameter and the preciseness of the micron-size aperture are dependent upon the total energy of the laser pulse train, laser pulse width, and the diameter of laser spot.

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Investigation of Demixing Phenomena of a Polymer Solution During the Phase Inversion Process

  • Han, Myeong-Jin;D. Bhattacharyya
    • Proceedings of the Membrane Society of Korea Conference
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    • 1995.04a
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    • pp.11-15
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    • 1995
  • Polysulfone (PS) membranes were prepared by the phase inversion process using water or isopropanol as nonsolvent. The Flory-Huggins theory for a ternary system nonsolvent/solvent/polymer is applied to describe the thermodynamic equilibria of the components. The calculated ternary phase equilibria show that demixing of a PS binary solution with n-methylpyrrolidone (NMP) will be fast in a water coagulation bath and will be delayed in an isopropanol bath. The prepared membranes were characterized by SEM, gas adsorption-desorption measurement, and permeability test. The membrane, which is precipitated by fast demixing in a water bath, has nodular structures in the skin region and includes finger-like cavities in the sublayer. The membrane coagulated by isopropanol has a very dense and thick skin structure, which is formed by delayed demixing. The membrane coagulated by isopropanol showed considerably lower pore volume and surface area compared to that observed with water coagulation method. With dimethylformamide (DMF) as solvent and 2-3 wt% of water, the solution can show the liquid-liquid phase separation due to agglomation of the polymer-lean phase from the homogeneous solution. The membranes, which were coagulated near an equilibrium state, show the large (micron size) round pores in the whole membranes. The pores do not contribute the permeation characteristics.

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Micro Pre-concentration and Separation of Metal Ions Using Microchip Column Packed with Magnetic Particles Immobilized by Aminobenzyl Ethylenediaminetetraacetic Acid

  • Kim, Y.H.;Kim, G.Y.;Lim, H.B.
    • Bulletin of the Korean Chemical Society
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    • v.31 no.4
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    • pp.905-909
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    • 2010
  • Magnetic beads (Dynabeads$^{(R)}$) embedded in ~1 micron size polystyrene beads bearing surface carboxylic acid groups were modified with aminobenzyl ethylenediaminetetraacetic acid (ABEDTA) to concentrate or separate metal ions using pH gradients on micro and nano scales. The immobilization of ABEDTA was achieved by amide formation. The presence of the metal chelating functional group in the fully deprotonated form was confirmed by FT-IR. The chelation efficiency of beads was tested by determining metal ions in supernatant using GFAAS when pH gradients from 3 to 7. Mixtures of Cu and Mg and of Cd and Mn (at 10 ng/mL of metal) were separated as the difference in formation constant with the functional group of ABEDTA. The separation was repeated twice with relative standard deviation of <18%. A polydimethylsiloxane (PDMS) microchip column packed with EDTA-coated magnetic beads was optimized to concentrate metal ion for practical applications by eluting a Cu solution of micro scale at pH 3.