• Title/Summary/Keyword: micro-powder

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Synthesis of Titanium Silicide by Electro-Discharge-Sintering of Ti and Si Powder Mixture (Ti 및 Si 혼합 분말의 전기방전소결에 의한 Titanium Silicide의 합성 연구)

  • Cheon Y. W.;Oh N. H.;Kim Y. H.;Byun C. S.;Lee S. H.;Lee W. H.
    • Journal of Powder Materials
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    • v.12 no.6 s.53
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    • pp.447-452
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    • 2005
  • The synthesis and consolidation of titanium silicide by electro-discharge-sintering has been investigated. As-received Ti powder was in flaky shape and the mean particle size was $45.0{\mu}m$, whereas the mean particle size of the pre-milled Si powder with angular shape was $8.0{\mu}m$. Single pulse of 2.5 to 5.0 kJ/0.34g-elemental Ti and pre-milled Si powder mixture with the composition of $Ti-37.5at.\%$ Si was applied using $300{\mu}F$ capacitor. The solid with $Ti_5Si_3$ phase has been successfully fabricated by the discharge with the input energy more than 2.5kJ in less than $129{\mu}sec.$ Hv values were found to be higher than $1000kgf/mm^2$. The formation of $Ti_5Si_3$ occurred through a fast solid state diffusion reaction.

Fabrication of Fe Foam using Slurry Coating Process (슬러리 코팅 공정을 이용한 Fe 폼의 제조에 대한 연구)

  • Yun, Jung-Yeul;Park, Dahee;Yang, Sangsun;Wang, Jei-Pil
    • Resources Recycling
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    • v.26 no.6
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    • pp.97-101
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    • 2017
  • Metal foams have a cellular structure consisting of a solid metal containing a large volume fraction of pores. In particular, open pores which are penetrable pores are necessary for industrial applications such as in high temperature filters and as support for catalysts. In this study, Fe foam with greater than 90% porosity and 2-mm pore size was successfully fabricated using a slurry coating process and the pore properties were characterized. The Fe and $Fe_2O_3$ powder mixing ratios were controlled to produce Fe foam samples with different pore sizes and porosity. First, the slurry was prepared through the uniform mixing of powders, distilled water, and polyvinyl alcohol(PVA). The amount of slurry coated with the PU foam increased with increasing $Fe_2O_3$ mixing powder ratio, but the shrinkage and porosity of the Fe foams decreased, respectively, with increasing $Fe_2O_3$ mixing powder ratio.

Setting and Micro-structures of the Cement Pastes Using Sugar-Based Super Retarding Agents (당류계 초지연성 혼화제를 사용한 시멘트 페이스트의 응결 및 미시구조 특성)

  • Jeong, Yeong-Jin;Hyun, Seung-Yong;Han, Jun-Hui;Kim, Jong;Han, Min-Cheol
    • Journal of the Korea Institute of Building Construction
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    • v.23 no.6
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    • pp.703-714
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    • 2023
  • This research conducts a series of tests to investigate the setting retarding properties and strength development in cement pastes incorporating various types and dosages of sugar-based super retarding agents. Six such agents, including Sucrose, Sugar powder, Saccharin, Aspartame, Stevioside, and Mogroside, commercially available, were selected for evaluation. The study also examines the micro-structural properties of these cement pastes. The test mixtures were prepared using a 27.5% water-to-cement ratio and ordinary Portland cement. Micro-structural analyses were conducted using Scanning Electron Microscopy(SEM), X-Ray Diffraction(XRD), and Energy Dispersive Spectroscopy(EDS). The findings reveal that the incorporation of sucrose, sugar powder, and stevioside significantly retards the setting time. Particularly, adding 0.1% sucrose extended the setting time by approximately two-fold compared to the control(Plain) mixture. Most mixtures, barring those with sugar powder and stevioside, exhibited compressive strength comparable to the Plain mixture. Notably, with 0.2% sucrose, strength measurements were not feasible at 1 day, but at 3 days, the strength gains aligned with the Plain mixture. XRD, SEM, and EDS analyses confirmed the hydration delay(set retarding) of C3S due to sucrose, with further quantitative corroboration provided by EDS. SEM was used to verify the presence or absence of hydration products. The study concludes that sucrose, as a sugar-based retarder, offers effective set retarding capabilities and compressive strength development in concrete.

Development of Blue Light Cut Films Using a Roll-to-Roll Nano Micro Coating System

  • Hwang, Joong Kook;Shina, Hoon-Kyu;Chang, Sang-Mok
    • Transactions on Electrical and Electronic Materials
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    • v.17 no.3
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    • pp.178-181
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    • 2016
  • In this study a coating experiment was performed to fabricate blue light cut films, which represent a 390~430 nm cut off rate of more than 40% and a transmittance rate of more than 90%, using a roll-to-roll nano micro coating system. The study also analyzed the characteristics of the blue light cut films. Thus, the hardness, which is more than 3H, is ensured through fabricating films using a Sol-Gel process that will determine the proper hardness level. Also, the experiment shows excellent results by cutting blue light through a mixing blue light powder.

A Study on Optimum Splitting Conditions of Flat Nylon/PET Micro Fiber Fabrics (편평단면구조를 갖는 분할형 N/P극세사 직물의 최적분할조건에 관한 연구)

  • 손은종;이영목;김연상;이경주;권은희;최영근
    • Proceedings of the Korean Fiber Society Conference
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    • 2002.04a
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    • pp.376-376
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    • 2002
  • 편평분할사는 복합방사법에 의한 편평 단면 형태의 분할형 초극세섬유로서, 기존 오렌지 형태인 Nylon/PET 극세사의 품종 다양화된 형태이다 분할은 Nylon과 PET의 비상용성인 특징을 이용, 물리적인 가공과 화학적인 가공에 의해 이루어지며 기존오렌지 형태의 PET/Nylon극세사에 비해 분할성이 우수하다고 보고되고 있다. 편평분할사의 용도는 Micro powder조의 Suede직물 등의 여성용 의류, 기능성 스포츠웨어, 2차 오염방지성이 우수하여 반도체 등의 정밀산업의 닦음천(Wiping Cloth)등의 크리너(Cleaner)용으로도 사용되어 질 수 있다. (중략)

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Machining of the Inject Mould for Forming the Dot Pattern of LGP of TFT-LCD (TFT-LCD의 도광판 패턴 사출성형용 금형가공)

  • 박동삼;최영현;하민수
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.1215-1219
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    • 2003
  • Light Guide Panel(LGP) is a key part of backlight unit(BLU) which transforms line-light of lamp to surface-light. Dot pattern is formed on the injected LGP surface by screen printing. This dot pattern is composed of several ten thousands micro dots of diameter 150-180$\mu\textrm{m}$ or so. The dot patterning by screen printing causes low productivity and low performance of TFT-LCD. This research develops the micromachining technology for LGP mould which could form micro dot pattern by injection molding, removing the existing screen printing process.

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Novel Micro Gas Generator of Carbon Dioxide for Actuation and Gas Source (구동력과 가스 제공을 위한 이산화탄소 발생기)

  • Choi Yo Han;Son Sang Uk;Lee Seung S.
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.29 no.7 s.238
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    • pp.970-975
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    • 2005
  • This paper presents a novel microgenerator of $CO_2$ (carbon dioxide) gas. $NaHCO_3$ (sodium bicarbonate) in a chamber is decomposed by the underlaid microheater. Alternatively, water droplet is caged by paraffin layer and released by heating. The released water dissolve HOC(COOH)$(CH_2COOH)_2$ (citric acid) powder and then, $NaHCO_3$ reacts with the solubilized HOC(COOH)$(CH_2COOH)_2$ and $CO_2$ is produced. Micropumps actuated by $CO_2$ generation were fabricated. A portable micro cell incubator of which pH is controlled by the produced $CO_2$ is also presented as one of the further applications.

Fabrication of Graphene Supercapacitors for Flexible Energy Storage

  • Habashi, M. Namdar;Asl, Shahab Khameneh
    • Korean Journal of Materials Research
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    • v.27 no.5
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    • pp.248-254
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    • 2017
  • In the present work, graphene powder was synthesized by laser scribing method. The resultant flexible light-scribed graphene is very appropriate for use in micro-supercapacitors. The effect of the laser scribing process in reducing graphene oxide (GO) was investigated. GO was synthesized using a chemical mixture of GO solution; then, it was coated onto a LightScribe DVD disk and laser scribed to reduce GO and create laser-scribed graphene (LSG). The CV curves of pristine rGO at various scan rates showed that the ultimate product possesses the ability to store energy at the supercapacitor level. Charge-discharge curves of pristine rGO at two different current densities indicated that the specific capacitance ($C_m$) increases due to the reduction of the discharge current density. Finally, the long-term charge-discharge stability of the LSG was plotted and indicates that the specific capacitance decreases very slightly from its primary capacitance of ${\sim}10F\;cm^{-3}$ and that the cyclic stability is favorable over 1000 cycles.

Magnesium Sulfate Resistance of Concrete Containing Waste Glass (폐유리를 혼입한 콘크리트의 황산마그네슘 저항성에 관한 연구)

  • Kim, Young-Su;Jeong, Yoo-Jin;Lee, Dong-Un
    • Journal of the Korea Institute of Building Construction
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    • v.9 no.3
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    • pp.109-116
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    • 2009
  • The magnesium sulfate solution digestion test carried out for resistance of concrete containing waste glass powder on magnesium sulfate attack. Moreover, it yielded S.D.F index was used for the criteria of quantitative assessment to the resistance of magnesium sulfate for the purpose of evaluation of chemical deterioration on concrete. Furthermore, to evaluate for micro-cracks within concrete and external corrosion, the weight variation of specimens and the dynamic elasticity were compared and analyzed and also the applicability was examined using the analysis of product of hydration through out observing external deformation and micro-structural deformation.

Study on the Thermal Characteristics of Concrete Using Insulation Performance Improve Material Complex (단열성능향상 재료를 혼합 사용한 콘크리트의 열전도 특성에 관한 연구)

  • Park, Young-Shin;Kim, Jung-Ho;Kang, Sung-Hyuk;Kim, Se-Hwan;Ryu, Dong-Woo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2013.11a
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    • pp.40-41
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    • 2013
  • The energy consumption by buildings approximately reaches 25% of total korea energy consumption. The greatest part in the buildings of the energy consumption is building facade. but a few research projects on concrete compising more than 70% of outsider of buildings has been tried. This research is structural insulation concrete what improved insulation performance using micro form admixture and calcined diatomite powedr and lightweight aggregate.

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