• Journal of Adhesion and Interface
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• v.3 no.4
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• pp.19-26
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• 2002

In order to study the toughening mechanism of rubber modified polycarbonate, the sequence of development of micro-voids was investigated by real-time small angle X-ray scattering with Synchrotron radiation (SR-SAXS). The used test method was wedge test. The scattering intensity increases with increasing penetration depth of wedge, i.e. applied strain. The increase is due to the micro-void formation during deformation. This micro-void was uniformly developed in matrix and was different from large-void due to internal cavitation of rubber particle and/or debonding between rubber particle and polycarbonate matrix. The micro-void was developed at the critical strain and the radius of micro-void is around $600{\AA}$. Above the critical strain the size of micro-void remains almost constant with increasing applied strain. However, the population of micro-void increased with applied strain.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.31 no.2A
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• pp.121-127
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• 2011

Spatial distribution of void space in concrete materials strongly affects mechanical and physical behaviors. Therefore, the identification of characteristic void distribution helps understand material properties and is essential to estimate the integrity of material performance. The 3D micro CT (X-ray microtomography) is implemented to examine and to quantify the void distribution of a lightweight aggregate concrete using an image analysis technique and probabilistic approach in this study. The binarization and subsequent stacking of 2D cross-sectional images virtually create 3D images of targeting void space. Then, probability distribution functions such as two-point correlation and lineal-path functions are applied for void characterization. The lightweight aggregates embedded within the concrete are individually analyzed to construct the intra-void space. Results shows that the low-order probability functions and the density distribution based on the 3D micro CT images are applicable and useful methodology to characterize spatial distribution of void space and constituents in concrete.

• Journal of the Korean Wood Science and Technology
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• v.36 no.6
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• pp.13-22
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• 2008

Internal voids affecting the mechanical properties of wood composite were classified into two catagories and characteristics of voids were examined according to density variation of strandboard. The void distribution and content of strandboard according to board density were measured by X-ray computed tomography system and analized using image processing software. Prior to investigation, the densities of strandboard were measured by densitometer and the results were showed high correlation with conventional oven drying method. Based on the image analysis conducted on captured images by X-ray tomography, low resolution can be used to capture the macro-voids (between strand) but not the micro-voids (within strands). Intermediate resolution can be used to capture both the macro and the micro-voids and high resolution can be successfully used to capture the majority of the micro-voids. The content of macro-void was measured and content of micro-void was computed by corresponding related equation. The macro-void distribution can be successfully understood and void content can be correctly estimated through the results.

• Proceedings of the Korean Geotechical Society Conference
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• 2010.09a
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• pp.392-403
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• 2010

In this study, a new methodology by using the X-ray CT scan is proposed for estimating void ratio of very fine clayey soil. Since the particle size of the clay is too fine to calculate the volume of void inside the clays, CT scanning tests with a number of clay specimens that were artificially set to have various designated void ratios have been carried out. From the tests, a relationship between the CT values and void ratios is given to be used for estimating the invisible void ratio of very fine clay from a representative CT value scanned. The linear relationship was able to be acquired finally. It is expected that micro X-ray CT scanning can be capable of capturing the void ratio of very fine soils without any errors inherent in the conventional specific gravity tests.

• Journal of the Korean Society for Nondestructive Testing
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• v.37 no.2
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• pp.106-114
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• 2017

This paper presents an automated subsurface micro void detection technique based on pulsed infrared thermography for inspecting epoxy molding compounds (EMC) used in electronic device packaging. Subsurface micro voids are first detected and visualized by extracting a lock-in amplitude image from raw thermal images. Binary imaging follows to achieve better visualization of subsurface micro voids. A median filter is then applied for removing sparse noise components. The performance of the proposed technique is tested using 36 EMC samples, which have subsurface (below $150{\mu}m{\sim}300{\mu}m$ from the inspection surface) micro voids ($150{\mu}m{\sim}300{\mu}m$ in diameter). The experimental results show that the subsurface micro voids can be successfully detected without causing any damage to the EMC samples, making it suitable for automated online inspection.

• Restorative Dentistry and Endodontics
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• v.45 no.1
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• pp.5.1-5.8
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• 2020

Objectives: The obturation quality of MTA, Biodentine, Total Fill BC root canal sealer (RCS), and warm gutta-percha (WGP) in teeth with simulated internal root resorption (IRR) was evaluated by using micro-computed tomography. Materials and Methods: Standardized IRR cavities were created using 40 extracted maxillary central incisor teeth and randomly assigned into 4 groups (n = 10). IRR cavities were filled with MTA, Biodentine, Total Fill BC RCS (bulk-fill form) and WGP + Total Fill BC RCS. Percentage of voids between resorptive cavity walls and obturation material (external void), and inside the filling materials (internal voids) were measured. Results: Total Fill BC sealer in the bulk-fill form presented significantly highest values of external and internal void percentages (p < 0.05). Biodentine showed a significantly lowest external void percentage (p < 0.05). WGP + Total Fill BC RCS presented significantly lower values of internal void percentages than all groups (p < 0.05), except Biodentine (p > 0.05). Conclusion: None of the filling materials were created void-free obturation in resorption cavities. Biodentine may favor its application in teeth with IRR over Angelus MTA and bulkfill form of Total Fill BC.

• The Journal of Advanced Prosthodontics
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• v.8 no.2
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• pp.101-109
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• 2016

PURPOSE. To investigate the void parameters within the resin cements used for fiber post cementation by micro-CT (${\mu}CT$) and regional push-out bonding strength. MATERIALS AND METHODS. Twenty-one, single and round shaped roots were enlarged with a low-speed drill following by endodontic treatment. The roots were divided into three groups (n=7) and fiber posts were cemented with Maxcem Elite, Multilink N and Superbond C&B resin cements. Specimens were scanned using ${\mu}CT$ scanner at resolution of $13.7{\mu}m$. The number, area, and volume of voids between dentin and post were evaluated. A method of analysis based on the post segmentation was used, and coronal, middle and apical thirds considered separately. After the ${\mu}CT$ analysis, roots were embedded in epoxy resin and sectioned into 2 mm thick slices (63 sections in total). Push-out testing was performed with universal testing device at 0.5 mm/min cross-head speed. Data were analyzed with Kruskal-Wallis and Mann-Whitney U tests (${\alpha}=.05$). RESULTS. Overall, significant differences between the resin cements and the post level were observed in the void number, area, and volume (P<.05). Super-Bond C&B showed the most void formation ($44.86{\pm}22.71$). Multilink N showed the least void surface ($3.51{\pm}2.24mm^2$) and volume ($0.01{\pm}0.01mm^3$). Regional push-out bond strength of the cements was not different (P>.05). CONCLUSION. ${\mu}CT$ proved to be a powerful non-destructive 3D analysis tool for visualizing the void parameters. Multilink N had the lowest void parameters. When efficiency of all cements was evaluated, direct relationship between the post region and push-out bonding strength was not observed.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2002.10a
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• pp.284-287
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• 2002

During resin transfer molding(RTM) process, in case of thick parts, resin flow and void formation should be modeled three dimensionally even though for parts of small thickness, resin flow and void formation can be modeled two dimensionally. In this study, numerical simulations of three dimensional mold filling and void formation during RTM process.

• Proceedings of the KSME Conference
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• 2001.06c
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• pp.246-250
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• 2001

In resin transfer molding (RTM), resin is forced to flow through the fiber perform of inhomogeneous permeability. This inhomogeneity is responsible for the mismatch of resin velocity within and between the fiber tows. The capillary pressure of the fiber tows exacerbates the spatial variation of the resin velocity. The resulting microscopic perturbations of resin velocity at the flow front allow numerous air voids to form. In this study, a mathematical model was developed to predict the formation and migration of micro-voids during resin transfer molding. A transport equation was employed to account for the migration of voids between fiber tows. Incorporating the proposed model into a resin flow simulator, the volumetric content of micro-voids in the preform could be obtained during the simulation of resin impregnation.

• Korean Journal of Materials Research
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• v.27 no.12
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• pp.688-694
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• 2017

Porous materials such as polymeric foam are widely adopted in engineering and biomedical fields. Porous materials often exhibit complex nonlinear behaviors and are sensitive to material and environmental factors including cell size and shape, amount of porosity, and temperature, which are influenced by the type of base materials, reinforcements, method of fabrication, etc. Hence, the material characteristics of porous materials such as compressive stress-strain behavior and void volume fraction according to aforementioned factors should be precisely identified. In this study, unconfined uniaxial compressive test for two types of closed-cell structure polyurethane foam, namely, 0.16 and $0.32g/cm^3$ of densities were carried out. In addition, the void volume fraction of three different domains, namely, center, surface and buckling regions under various compressive strains (10 %, 30 %, 50 % and 70 %) were quantitatively observed using Micro 3D Computed Tomography(micro-CT) scanning system. Based on the experimental results, the relationship between compressive strain and void volume fraction with respect to cell size, density and boundary condition were investigated.