• 제목/요약/키워드: metal mold

검색결과 560건 처리시간 0.025초

치과용 아말감의 미세경도에 관한 실험적연구 (AN EXPERIMENTAL STUDY ON THE MICROHARDNESS OF DENTAL AMALGAMS)

  • 신동훈
    • Restorative Dentistry and Endodontics
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    • 제8권1호
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    • pp.89-96
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    • 1982
  • The purpose of this study is to identify the phases of four different types, low-copper lathe cut (Type II, class 1) and spherical (Type II, class 2) amalgam alloys which are made by Caulk company and high copper Dispersalloy (Type II, class 3) made by Johnson & Johnson and Tytin (Type I, class 2) made by S.S. White and to determine the Vickers hardness number on the individual phase and four different types of dental amalgam. After each amalgam alloy and Hg measured exactly by the balance was triturated by the mechanical amalgamator (De Trey), the triturated mass was inserted into the cylindrical metal mold which was 4 mm in diameter and 12mm in height and was pressed by the Instron Universal Testing machine (Model 1125) at the speed of 1mm/minute with 143$kg/cm^2$ according to the A.D.A. Specification No. 1. The Specimen removed from the mold, mounted and stored in the room temperature for 7 days. The speciman was polished with the emery paper from #220 to #1200 and finally on the polishing cloth with 0.3 and 0.05 um $Al_2O_3$ powder suspended in water. And then each specimen was etched by Allan's method and washed with Sodium Bisulfinite for 30 seconds. Finally differentiation and metallography on each phase were obtained by using metallographical microscope (Versamet, Union) and microhardness was obtained by using microhardness tester (MVH-2, Torsee). The results were as follows: 1. In the low-copper amalgam, the ${\gamma}$, ${\gamma}_1$ and ${\gamma}_2$ phase were observed and in the high-copper amalgam, the ${\gamma}$, ${\gamma}_1$. ${\epsilon}$ and ${\eta}$ phases were observed but ${\gamma}_2$ phase was not observed. 2. Among the microhardness of each amalgam phase measured under pressing a vickers diamond indenter with 2.0gm load for 30 seconds, e phase has the highest V.H.N (314 ${\pm}$ 20), and in low-copper amalgam 12 phase has the lowest V.H.N. (29${\pm}$1) and ${\eta}$ phase which was observed in high-copper amalgam has 230${\pm}$13 V.H.N and this phase is considerd to contribute to strengthen the handness in amalgam. 3. The V.H.N. measured under pressing a Vickers diamond indenter with 300.0gm load for 30 seconds in low-copper amalgam was lower than that of high-copper amalgam.

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정전압 분극곡선법에 의한 아말감의 부식 거동에 관한 연구 (A STUDY ON THE CORROSION BEHAVIOUR OF AMALGAMS BY USING OF POTENTIOSTATIC POLARIZATION METHOD)

  • 신동훈;엄정문
    • Restorative Dentistry and Endodontics
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    • 제12권1호
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    • pp.39-49
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    • 1986
  • The purpose of this study was to observe characteristic properties through the polarization curves and SEM images from 4 different types of amalgam obtained by using the potentiostats (Princeton EG & G) & SEM (Jeol/35), and to investigate the degree of corrosion on the oxidation peak of the each phase of amalgam. After each amalgam alloy and Hg was triturated as the direction of the manufacturer by means of the mechanical amalgamator (Shofu Co.), the triturated mass was inserted into the cylindrical metal mold which was 12mm in diameter and 10.0mm in height and was condensed by using routine manner. The specimen was removed from the mold and stored at room temperature for about 24 hours. The standard surface preparation was routinely carried out. Anodic polarization measurement was employed to confirm the corrosion behaviour of the amalgams in a 0.9% saline solution (P.H: 6.8-7.0) at $37^{\circ}C$. The initial rest potential (corrosion potential) was determined after 30 minutes of immersion of specimen in electrolyte, and the potential scan was begun at the point of 100mV cathodic from the corrosion potential. The scan rate was 0.17mV/sec. in the study to observe the degree of corrosion of each phase. SEI and EPMA images on the determined oxidation peaks of each amalgam were observed. The results were as follows: 1. In the four anodic polarization curves, low copper amalgams have three oxidation peaks and high copper amalgams have two oxidation peaks, -270mV, +26mV and +179mV(SEC) in the low copper lathe cut, and -300mV, +39mV and +163mV(SEC) in the low copper spherical. -4mV and +154mV(SEC) in the Dispersalloy, and +17mV and +180mV(SEC) in the Tytin as high copper amalgams. 2. ${\gamma}_2$ phase in the low copper amalgam and ${\eta}$ phase in the high copper amalgam were the most corrodible phases and Ag-Cu eutectic in high copper amalgam was the most slowly corroded phase. 3. Low copper amalgam was more susceptible in corrosion than high copper amalgam.

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인공타액에서 아말감의 부식거동에 관한 전기화학적 연구 (ELECTROCHEMICAL STUDY ON THE CORROSION BEHAVIOUR OF DENTAL AMALGAM IN ARTIFICIAL SALIVA)

  • 김영남;엄정문
    • Restorative Dentistry and Endodontics
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    • 제13권2호
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    • pp.221-235
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    • 1988
  • The purpose of this study was to observe characteristic properties through the polarization curves and EMPA images from 4 different types of amalgam obtained by using the potentiostats (EG & G PARC) & EPMA (Jeol JSM-35), to investigate the degree of corrosion of each phase of amalgam on the oxidation peak, and to identify corrosion products from the corroded amalgam by use of X-ray diffractometer(Rigaku). After each amlgam alloy and Hg were triturated as the direction of the manufacturer by means of the mechanical amalgamator(Shofu), the triturated mass was inserted into the cylindrical metal mold which was 12mm in diameter and 10mm in height and was condensed by means of routine manner. The specimen was removed from the mold and stored at room temperature for about 7 days. The standard surface preparation was routinely carried out. Anodic polarization measurement was employed to compare the corrosion behaviours of the amalgams in 0.9% saline solution(pH6.8~7.0) and artificial saliva (pH6.8~7.0) at $37^{\circ}C$. The open circuit potential was determined after 30 minutes' immersion of specimen in electrolyte and the potential scan was begun at the potential of 100mV cathodic from the corrosion potential. The scan rate was 1mV/sec and the surface area of amalgam exposed to the solution was 0.64$cm^2$ for each specimen. All the potentials reported are with respect to a saturated calomel electrode (SCE). EPMA images on the determined oxidation peaks of each amalgam in artificial saliva were observed. X-ray diffraction patterns of each sample were recorded before and after polarization in artificial saliva (Aristaloy, Caulk Spherical, Dispersalloy and Tytin: at +770mV, +585mV, +8.10m V and +680m V respectively) by use of a recording diffractometer. Nickel filtered Cu $K_{{\alpha}_1}$ radiation was used and sample was scanned at $4^{\circ}(2{\theta})/min.$ from $25^{\circ}$ to $80^{\circ}$. The following results were obtained. 1. Oxidation peak potential in artificial saliva shifted to more anodic direction than that in saline solution. 2. The corrosion potential of high copper amalgam was more anodic than the potential of low copper amalgam. 3. The current density was lower in artificial saliva than in saline solution. 4. One of the corrosion products, AgCl was identified by X-ray diffraction analysis. 5. ${\gamma}_2$ phase was the most susceptible to corrosion and e phase was stable in low copper amalgam and ${\eta}$' phase and Ag-Cu eutectic were susceptible to corrosion in high copper amalgam.

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인공타액에서 수종 아말감의 부식시 용해성분 및 표면 부식 생성물에 관한 실험적 연구 (EXPERIMENTAL STUDY ON THE DISSOLUTION COMPONENTS AND CORROSION PRODUCTS OF SEVERAL AMALGAMS IN ARTIFICIAL SALIVA)

  • 조승주;이명종
    • Restorative Dentistry and Endodontics
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    • 제19권1호
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    • pp.1-26
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    • 1994
  • The purpose of this study was to investigate the dissolution components during corrosion of amalgams and to identify surface corrosion products in the modified Fusayama artificial saliva. Four type of amalgam alloys were used: low copper lathe cut amalgam alloy (Cavex 68), low copper spherical amalgam alloy (Caulk Spherical Alloy), high copper admixed amalgam alloy (Dispersalloy) and high copper single composition amalgam alloy (Tytin). Each amalgam alloy and Hg were triturated according to the manufacturer's direction by means of mechanical amalgamator (Capmaster, S.S.White), and then the triturated mass was inserted into the cylindrical metal mold which was 10mm in diameter and 2.0mm in height and condensed with compression of 150kg/$cm^2$ using oil pressor. The specimens were removed from the mold and stored at room temperature for 7 days and cleansed with distiled water for 30 minutes in an ultrasonic cleaner. The specimens were immersed in the modified Fusayama artificial saliva for the periods of 1 month, 3 months and 6 months. The amounts of Hg, Cu, Sn and Zn dissolved from each amalgam specimen immersed in the artificial saliva for the periods of 1 month, 3 months and 6 months were measured using Inductivity Coupled Plasma Atomic Emission Spectrometry (ICPQ-1000, Shimadzu, Japan) and amount of Ag dissolved from amalgam specimen was measured using Atomic Absorption Spectrophotometry (Atomic Absorption/Flame emission spectrophotometer M-670, Shimadzu, Japan). A surface corrosion products of specimens were analysed using Electron Spectroscopy Chemical Analyser (ESCA PHI-558, PERKIN ELMER, U.S.A.). The secondary image and back scattered image of corroded surface of specimens was observed under the SEM, and the corroded surface of specimens was analysed with the EDX. The following results were obtained. 1. The dissolution amount of Cu was the most in high copper admixed amalgam(Dispersalloy) and the least in high copper single composition amalgam(Tytin). 2. Sn and Zn were dissolved during all the experiment periods, and dissolution amounts were decreased as the time elapsed. 3. Initial surface corrosion products were ZnO and SnO. 4. Corrosion of ${\gamma}$ and ${\gamma}_2$ phase in low copper amalgams was observed and Ag-Cu eutectic alloy phase was corroded in low copper spherical amalgam(Caulk Sperical Alloy). 5. Corrosion of ${\gamma}$ and $\eta$' phase in high copper amalgams was observed and Ag-Cu eutectic alloy phase was corroded in high copper admixed amalgam(Dispersalloy). 6. Sn-Cl was produced in the subsurface of low copper amalgams and high copper admixed amalgam.

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분광색채계측기를 이용한 Vita Shade 광중합형 복합레진의 색상 비교 (COMPARATIVE EVALUATION OF LIGHT-CURED COMPOSITE RESINS BASED ON VITA SHADE BY SPECTROCOLORIMETER)

  • 조경이;황인남;최홍란;오원만
    • Restorative Dentistry and Endodontics
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    • 제23권1호
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    • pp.424-432
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    • 1998
  • To get a satisfactory result in the composite resin restorations, it is necessary to choose correct shade. At present, most of the commercial composite resins are based on the Vita Lumin shade guide or Bioform shade guide, but color differences might be expected even using the same shade in various materials. In this study, five kinds of light-cured composite resins with A2 and B3 shade were used to measure and compare the color each other while one porcelain served as a control. All composite resins (Spectrum TPH (SP), VeridonFil- Photo (VE), Z100 (Z100), Charisma (CH), Prodigy (PRO)) were filled in to the metal mold (12 mm diameter, 2 mm depth), followed by compression, polymerization and polishing with wet sandpaper. The specimens of porcelain were fabricated by using the refractory mold for porcelain. After 24 hours, the specimens were placed on the spectrocolorimeter and spectral reflectance were measured under CIE illuminant D65. After measuring the values of $L^*$, $a^*$, $b^*$ and ${\Delta}E^*$, following results were obtained; 1. The $L^*$, $a^*$ and $b^*$ values of both shade of porcelain specimens showed significantly higher than those of resin specimens(p<0.05). 2. In comparing the resin specimens of the A2 shade, differences were significant except $L^*$ values of SP-CH and PRO-VE, $a^*$ values of the VE-SP and $b^*$ values of the VE-Z100 and SP-PRO(p<0.05), 3. In comparing the resin specimens of the B3 shade, differences were significant except $L^*$ values of PRO-SP, $a^*$ values of the SP-PRO and Z100-VE and b* values of the PRO-SP(p<0.05). 4. In comparing the resin specimens of the A2 shade, color differences between materials (${\Delta}E^*$) showed the lowest value of 1.66, and the highest was 5.16. ${\Delta}E^*$ values of the materials of VE-PRO, CH-PRO, SP-PRO, SP-Z100 and SP-CH were lower than 3.3. 5. In comparing the resin specimens of the B3 shade, the lowest value of the ${\Delta}E^*$ was 0.57 and the highest was 5.92. ${\Delta}E^*$ values of Z100-CH and SP-PRO were lower than 3.3. The present study revealed there was perceptible color difference between materials even if they have the same designated shade based on Vita shade guide. The results of the present study suggested that it would be necessary to establish the reproducible and constant color specification system for an esthetic restoration.

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자동차 등속 조인트 샤프트 길이에 따른 내구성 해석을 통한 융합연구 (A Convergence Study through Durability Analysis due to the Shaft Length of Automotive Constant Velocity Joint)

  • 최계광;조재웅
    • 한국융합학회논문지
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    • 제9권8호
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    • pp.179-184
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    • 2018
  • 자동차의 구동방식은 전륜구동, 후륜구동, 4륜구동의 방식이 있다. 구동방식에서 운전자가 원하는 방향으로 전환하는 것과 바퀴에 동력을 전달하여 구동하는 두 가지의 역할을 수행하는데 있어 가장 중요한 부품이 등속 조인트이다. 도로상에서 주행 시에는 노면의 상태에 따라서 동력을 전달하는 부품들에 충격이 가해질 수 있다. 본 연구에서는 각각 샤프트의 길이가 다른 3개의 등속 조인트 각 모델들은 CATIA로 모델링하였고 ANSYS를 이용하여 구조 및 피로해석을 수행하였다. 본 연구 결과로는 Model 2가 다른 모델 대비 뛰어난 내구성을 가짐을 알 수 있었다. 이러한 결과를 이용하여 충격에 대한 내구성을 가지는 등속 조인트 설계를 할 때에 유용한 자료가 될 것이라고 사료되며, 등속 조인트의 디자인을 융합기술에 접목하여 미적 감각을 나타낼 수 있다.

자동차 시트 프레임 지지대 개수에 따른 내구성 해석을 통한 융합연구 (A Convergence Study through Durability Analysis due to the Number of Automotive Seat Frame Supports)

  • 최계광;조재웅
    • 한국융합학회논문지
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    • 제9권8호
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    • pp.155-160
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    • 2018
  • 자동차 시트는 주행시 운전자의 편의와 안전을 제공하는 하나의 부품이다. 최근 그 시트는 의자와 같은 용도 외에 외부의 충격이나 진동으로부터 운전자를 보호하고 편의를 주는 역할을 하고 있다. 자동차의 충돌 안전성 및 내구성과 같이 시트 프레임의 구조적인 기능에 대한 설계가 중요하다. 본 연구에서는 시트 프레임의 구조적인 안전성과 내구성을 높이기 위하여 시트 백 프레임 부분에 환봉을 1개씩 증가하여 시트를 설계하였다. 설계 및 해석 프로그램으로는 CATIA와 ANSYS를 사용하여 본 연구를 수행하였다. 구조해석과 진동해석을 통한 본 연구 결과로서는 Model 4가 타 모델 대비 더 뛰어난 내구성을 가지는 것을 알 수 있었다. 이 결과를 이용함으로서 구조적인 안전성과 내구성을 가진 자동차 시트 프레임 설계를 할 때에 유용한 자료가 될 것이라고 사료되며, 자동차 시트 프레임의 디자인을 융합기술에 접목하여 미적 감각을 나타낼 수 있다.

주물 유동해석의 VR 가시화 (VR Visualization of Casting Flow Simulation)

  • 박지영;서지현;김성희;김명희
    • 한국HCI학회:학술대회논문집
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    • 한국HCI학회 2008년도 학술대회 1부
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    • pp.813-816
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    • 2008
  • 본 연구에서는 주물의 유통해석결과를 3차원 모델로 복원하여 가상현실 디스플레이 상에 가시화 하는 방법을 제안한다. 먼저 기존 CAE 해석 소프트웨어를 사용하여 유한차분법 기반 열유동 수치해석을 수행한다. 이 과정에서는 주물의 설계모델은 그 형태가 규칙적인 사각형 격자에 근사되며 용탕을 주형에 주입하는 것을 시작으로 충전이 완료될 때까지 사전에 정의된 단계수만큼 반복적으로 전체 복셀에 대한 충전도와 온도수치가 기록된다. 다음 단계에서는 그 결과별 입력으로 하여 복셀 단위로 주울 형태를 복원한다. 이 때 유통진행에 따른 각 단계에서 각 복셀의 충전여부와 온도수치를 색상에 대응시켜 복셀의 색상을 결정한다. 복원 모델은 수평형 가상현실 디스플레이 장치인 Projection Table 상에서 가시화 하였으며 액티브 스테레오 방식으로 입체화면을 제공한다.

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주입선 형태가 티타늄 주조관의 변연재현성에 미치는 영향 (THE EFFECT OF SPRUE DESIGN ON THE MARGINAL REPRODUCIBILITY OF CAST TITANIUM CROWNS)

  • 박재경;정창모;전영찬
    • 대한치과보철학회지
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    • 제40권4호
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    • pp.352-364
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    • 2002
  • There has been a great interest in the use of titanium for fixed and removable prostheses in recent because of its excellent biocompatibility. However the high melting temperature and chemical reactivity of titanium necessitates casting systems different from those used in conventional casting. The current titanium casting systems are based on an electric-arc design for melting the metal in an argon atmosphere and its exclusive investment. Despite the new developments in Ti casting systems, inadequate mold filling and internal porosity are frequently observed casting defects. Therefore, the study on the fabrication technique including sprue design to solve these casting defects is still necessary. In this study to evaluate the effect of sprue design on the castability of simulated cast titanium crowns, 10 cylindrical cast crowns for each group with four different sprue design(Single group. Double group, Runner bar group. Reservoir group) were fabricated. An impression of the entire casting margin was made and cut at $90^{\circ}$ intervals, and the sections were photographed in a microscope at $100{\times}$ magnification to record marginal discrepancy. The internal porosities of the cast crowns were disclosed by radiographs. Within the limits of this study. the following conclusions were drawn. 1. The overall mean marginal discrepancies for each group were as follows: Double group, $43.65{\mu}m$; Reservoir group, $50.27{\mu}m$; Single group, $54.17{\mu}m$; Runner bar group, $58.90{\mu}m$ (p<0.05). 2. The mean of marginal discrepancies for wax patterns was $10.65{\mu}m$. 3 The numbers of internal porosity showed the most in Runner bar group followed by Single group, Reservoir group, and Double group.

핫 프레스 포밍을 위한 고열전도성 금형에 대한 연구 (Tough High Thermal-Conductivity Tool Steel for Hot Press Forming)

  • 금종원;박옥조;홍석무
    • 한국기계가공학회지
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    • 제15권3호
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    • pp.130-134
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    • 2016
  • Due to the need for advanced technologies in the automotive industry, the demand for lighter and safer vehicles has increased. Even though various nonferrous metals, like Aluminum, Magnesium and also Carbon Fiber Reinforced Plastic (CFRP), have been implemented in the automotive industry, a lot of technical research and development is still focused on ferrous metals. In particular, the market volume of High Strength Steel (HSS) parts and Ultra High Strength Steel (UHSS) by hot press forming parts has expanded significantly in all countries' automotive industries. A new tool steel, High Thermal-Conductivity Tool Steel (HTCS), for stamping punches and dies has been developed and introduced by Rovalma Company (Spain), and it is able to support better productivity and quality during hot press forming. The HTCS punches and dies could help to reduce cycle time due to their high thermal conductivity, one of the major factors in hot press forming operation. In this study, test dies were manufactured in order to verify the high thermal conductivity of HTCS material compared to SKD6. In addition, thermal deformation was inspected after the heating and cooling process of hot press forming. After heating and cooling, the test dies were measured by a 3D scanner and compared with the original geometry. The results showed that the thermal deformation and distortion were very small even though the cooling time was reduced by 2 seconds.