• 제목/요약/키워드: mechanical wet-milling

검색결과 23건 처리시간 0.032초

Synthesis of Cathode Material-Nickel Sulfides by Mechanical Alloying for Sodium Batteries

  • Liu, Xiaojing;Ahn, Hyo-Jun;Ahn, In-Shup
    • 한국분말재료학회지
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    • 제19권3호
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    • pp.182-188
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    • 2012
  • In this study, fine cathode materials $Ni_3S_2$ and $NiS_2$ were synthesized using the simple, convenient process of mechanical alloying (MA). In order to improve the cell properties, wet milling processes were conducted using low-energy ball milling to decrease the mean particle size of both materials. The cells of Na/$Ni_3S_2$ and Na/$NiS_2$ show a high initial discharge capacity of 425 mAh/g and 577 mAh/g respectively using wet milled powder particles, which is much larger than commercial ones, providing some potential as new cathode materials for rechargeable sodium-ion batteries.

Synthesis and Densification of Nanostructured $Al_2O_3-(Zro_2+3%Mol\;Y_2O_3)$ Bioceramics by High-Frequency Induction Heat Sintering

  • Kim, Sug-Won;Khalil, Khalil Abdel-razek
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.527-528
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    • 2006
  • Nanostructured Alumina - 20 vol% 3YSZ composites powder were synthesized by wet-milling technique. The starting materials were a mixture of Alumina micro-powder and 3YSZ nano-powders. Nano-crystalline grains were obtained after 24 h milling time. The nano-structured powder compacts were then processed to full density at different temperatures by high-frequency induction heat sintering (HFIHS). Effects of temperature on the mechanical and microstructure properties have been studied. $Al_2O_3-3YSZ$ composites with higher mechanical properties and small grain size were successfully developed at relatively low temperatures through this technique.

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미세정밀밀링 가공을 위한 검사시편의 가공조건에 따른 표면거칠기에 대한 영향 분석 (The Effect of Surface Roughness according to Machining Conditions of Test Specimen for Precision Micro-milling Machining)

  • 심민섭;김동현;이춘만
    • 한국정밀공학회지
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    • 제32권1호
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    • pp.49-55
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    • 2015
  • Recently, many researchers and industry are looking for ways to decrease the use of lubricants because of economical and environmental reasons. One of the lubrication technologies is the MQL method. This study presents a research of MQL and Wet milling processes of Al 6061 material. For this experiment, the test specimen is suggested, and various machining conditions are applied. And, shape of micro-pattern which has been recently spotlighted is included in the test specimen. In order to compare MQL with Wet machining, several milling experiments were carried out, varying feed rate, cutting speed, depth of cut, etc. Finally, the surface roughness results of machining tests according to the process conditions were measured. It is expected that the results of machining experiments can be used to predict the surface roughness of various MQL milling processes.

기계적 합금화법으로 제조된 고온 수전해용 Ni/YSZ 전극의 미세구조 특성 (Microstructural Characteristics of Ni/YSZ Cermet for High Temperature Electrolysis by Mechanical Alloying)

  • 박근만;채의석;홍현선;추수태
    • 한국재료학회지
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    • 제14권10호
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    • pp.743-748
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    • 2004
  • Modified Ni/YSZ cermets for high temperature electrolysis were synthesized by the direct ball milling of Ni and YSZ powder. The ball milling was carried out in dry process and in ethanol with varying milling time. While the dry-milling decreased the average size from 65 to $80{\mu}m$, the wet-milling decreased the average size down to $10{\mu}m$. In addition, very fine particles less than $0.1{\mu}m$ were observed in the wet-milling condition. The subsequent process of cold-pressing and sintering at $900^{\circ}C$ for 2 h did not affect the particle size of dry-milled powder. The electrical conductivity of the dry-milled Ni/YSZ cermet showed the value of $5{\times}10^{2}\;S/cm$ and this value was increased to $1.4{\times}10^{4}\;S/cm$ after the sintering at $900^{\circ}C$ for 2 h.

산화납의 특이상전이 (The Specficity of Phase Transitions of Lead Monoxide)

  • 김정욱;최성철;이응상
    • 한국세라믹학회지
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    • 제30권8호
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    • pp.623-628
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    • 1993
  • Lead monoxide has two phases at room temperature. One is a yellow orthorhombic phase, the other is a redtetragonal phase. Sometimes two phases are hybrided. The specificity of phase transitions of lead oxide is found during the milling of the batch including lead oxide. The pure orthorhombic phase of PbO can be transformed to the tetragonal phase perfectly by wet ball milling (milling liquid is distilled water) without thermal energy. However, when ethyl alcohol, isopropyl alcohol and aceton are used as milling liquid, respectively, the hybrid form of orthorhombic andtetragonal phases is obtained by wet ball milling. From the hybrid form heat-treated at $600^{\circ}C$ for 3hrs, this work results that mechanical phase transition of orthorhombic phase make a new form as distorted type orthorhombic phase of PbO.

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고온 수전해 전극용 modified Ni/YSZ cermet 제조 및 전극특성 (Preparation and characteristics of modified Ni/YSZ cermet for high temperature electrolysis)

  • 채의석;박근만;홍현선;추수태;윤용승
    • 한국수소및신에너지학회논문집
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    • 제15권2호
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    • pp.98-107
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    • 2004
  • Modified Ni/YSZ cermets for high temperature electrolysis were synthesized by dry or wet mechanical alloying methods. The Ni/YSZ composit particle was directly fabricated from the ball milling of Ni and YSZ powder or obtained from the reduction of NiO/YSZ particle after the ball milling of NiO and YSZ. In the case of the NiO/YSZ composite particle, the dry milling increased the average particle size whereas the wet milling decreased the size. The dry milling showed that fine YSZ particles were distributed over large Ni surfaces while Ni and YSZ particles similar in size were well mixed in the wet milling method. These features were the same in the Ni/YSZ composite particle prepared from Ni and YSZ powders. The electrical conductivity of the wet-milled Ni/YSZ cermet showed the highest value of $2{\times}10^2S/cm$ among the specimens and this value was increased to $1.4\times10^4S/cm$ after the sintering at $900^\circ{C}$ for 1 h.

제분방법을 달리하여 제조한 8품종 변이체벼의 쌀빵가공성 비교 (Comparison of Some Characteristics Relevant to Rice Bread made from Eight Varieties of Endosperm Mutants between Dry and Wet Milling Process)

  • 강미영;한지연
    • 한국식품과학회지
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    • 제32권1호
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    • pp.75-81
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    • 2000
  • 아밀로오스함량, 당함량, 전분입자의 형태 등에 차이를 보이는 8품종 변이체 벼들의 쌀빵가공성에 대한 제분방법(습식 및 건식)의 차이에 대해서 검토하였다. 이들 8품종의 최대수분흡수량은 품종에 따라 상당히 차이가 있어 shr.은 61.5%, 분질미는 48.4%였고, 화청벼 남풍벼 및 그들의 변이체들은 아밀로오스 함량이 낮은 품종의 쌀일수록 최대 수분흡수량은 증가하고 있었다. 건식제분에 의해서 제조한 쌀빵이 성형성, 기계적인 물성(경도, 탄력성, 응집성. 씹힘성) 및 관능검사에 의한 질감의 면에서 습식제분의 경우보다 우수하였다.

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MA 316L ODS 및 Wet 316L ODS 스테인리스강에서 충격에너지에 미치는 소결 공정의 영향 (Effects of the Sintering Variable on Impact Energy in MA 316L ODS and Wet 316L ODS Stainless Steels)

  • 김성수;한창희;장진성
    • 한국분말재료학회지
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    • 제17권2호
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    • pp.113-122
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    • 2010
  • Two kinds of oxide-dispersion-strengthened (ODS) 316L stainless steel were manufactured using a wet mixing process(wet) and a mechanical alloying method (MA). An MA 316L ODS was prepared by a mixing of metal powder and a mechanical alloying process. A wet 316L ODS was manufactured by a wet mixing with 316L stainless steel powder. A solution of yttrium nitrate was dried after being in the wet 316L ODS alloy. The results showed that carbon and oxygen were effectively reduced during the degassing process before the hydroisostatic process (HIP) in both alloys. It appeared that the effect of HIP treatment on increase in impact energy was pronounced in the MA 316L ODS alloy. The MA 316L ODS alloy showed a higher yield strength and a smaller elongation, when compared to the wet 316L ODS alloy. This seemed to be attributed to the enhancement of bonding between oxide and matrix particles from HIP and to the presence of a finer oxide of about 20 nm from the MA process in the MA 316L ODS alloy.

산화물 분산강화형 316L 스테인리스강의 제조와 특성 연구 (Fabrication and Characterization of ODS 316L Stainless Steels)

  • 김민호;류호진;김성수;한창희;장진성;권오종
    • 한국분말재료학회지
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    • 제16권2호
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    • pp.122-130
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    • 2009
  • Austenitic oxide-dispersion-strengthened (ODS) stainless steel was fabricated using a wet mixing process without a mechanical milling in order to reduce contaminations of impurities during their fabrication process. Solution of yttrium nitrate was dried after a wet mixing with 316L stainless steel powder. Carbon and oxygen contents were effectively reduced by this wet processing. Microstructural analysis showed that coarse yttrium silicates of about 150 nm were formed in austenitic ODS steels with a silicon content of about 0.8 wt%. Wet-processed austenitic ODS steel without silicon showed higher yield strength by the presence of finer oxide of about 20 nm.

Changes of Micro- and Nanoscopic Morphology of Various Bioresources by Different Milling Systems

  • Jang, Jae-Hyuk;Lee, Seung-Hwan;Lee, Min;Lee, Sang-Min;Kim, Nam-Hun
    • Journal of the Korean Wood Science and Technology
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    • 제45권6호
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    • pp.737-745
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    • 2017
  • This study was carried out to investigate the changes in micro- and nanoscopic morphology of cellulose nanofibrils (CNFs) from various bioresources by investigating various mechanical milling systems. Mechanical milling in herbaceous bioresources was more effective than in woody bioresources, demonstrating lower energy consumption and finer morphology. The milling time to reach nanoscopic size was longer in woody bioresources than in herbaceous bioresources. Furthermore, at the same level of wet disk milling time, CNFs from herbaceous bioresources showed more slender morphology than those from woody bioresources. Tensile properties of nanopaper prepared from CNFs of herbaceous bioresources were higher than those of woody bioresources. The highest tensile strength was found to be 77.4 MPa in the nanopaper from Evening prim rose.