• 제목/요약/키워드: measurement validation

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Validation, Measurement Uncertainty, and Determination of Bixin and Norbixin in Processed Foods of Animal Resources Distributed in Korea

  • Ga-Yeong Lee;Choong-In Yun;Juhee Cho;Young-Jun Kim
    • 한국축산식품학회지
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    • 제43권6호
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    • pp.949-960
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    • 2023
  • This research aimed to validate a high-performance liquid chromatography method for the quantitative determination of bixin and norbixin in various foods. The Diode Array Detector (495 nm) technique was used. Method was validated for specificity, linearity, limit of detection (LOD), limit of quantification (LOQ), precision, and accuracy, and the measurement uncertainty was assessed. The calibration curve showed excellent linearity (r2≥0.9999) over the tested concentration range of 0.2-25 mg/L. The LOD and LOQ were 0.03-0.11 and 0.02-0.05 mg/L for bixin and norbixin, respectively. The intra-and inter-day accuracies and precisions were 88.0±1.3-97.0±0.5% and 0.2%-2.6% relative SD (RSD) for bixin and 88.2±0.8-105.8±0.8% and 0.3%-2.7% RSD for norbixin, respectively. Inter-laboratory validation for accuracy and precision was conducted in three laboratories, and these results all met the AOAC guidelines. In addition, the relative expanded uncertainty (<22%) satisfied the CODEX recommendation. Furthermore, products distributed in Korea were monitored for annatto extracts using the proposed method to demonstrate its application. The developed analytical method is reliable for quantifying bixin and norbixin in various foods.

Auditory Model Design for Objective Audio Quality Measurement

  • Dongil Seo;Park, Se-Hyoung;Ryu, Seung-wan;Jaeho Shin
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 2002년도 ITC-CSCC -3
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    • pp.1717-1720
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    • 2002
  • Objective quality measurement schemes that in- corporate properties of the human auditory system. The basilar membrane(BM) acts as a spectrum analyzer, spatially decomposing the signal into frequency components. Each filterbank is an implementation of the ERB, gam-machirp function. This filterbank is level-dependent asymmetric compensation filters. And for the validation of the auditory model, we calculate the CPD. Quality measurement is obtained from the result.

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Single-Run FRF 측정을 통한 실차 모달 시험 및 모드맵 검증 (Full Vehicle Modal Testing using Single-Run FRF Measurement and Mode Map Validation)

  • 이근수;정승균;김증한
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 2008년도 추계학술대회논문집
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    • pp.387-388
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    • 2008
  • Finding reasonable flexural modes from the full vehicle modal testing has always been a difficult job to N&V engineers due to FRF inconsistency, nonlinearity, heavy damping and, in many cases, interactions between global body structural modes and massive isolate/non-isolated subsystem modes. This paper provides a brier overview of the mode map validation using single-run FRF measurement with highly sensitive accelerometers fur the full vehicle modal analysis and then it can be used to characterize the vehicle's global/local vibration performances, especially customer perceived "structural feel" typically below 40Hz.

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웹기반 정보시스템 이용자정보만족도(Flow) 측정모델의 교차문화 검증에 관한 연구 (A Study on Cross-Cultural Validation of Web-Based User Information Satisfaction (Flow) Measurement Model)

  • 정진택
    • 디지털융복합연구
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    • 제6권2호
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    • pp.157-164
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    • 2008
  • The current research utilized as its target population who are current users of web based information system in Korea. The research validated the dimensions by studying he constructs within the context of the web based information system user population. Correlation was found between Flow dimensions retained as components of a ross-Cultural Model. It was determined that these two dimensions-Intrinsic Interest and Control-are significant predictors of user success. The Cross-Cultural Model was validated, and it is therefore suggested as a basis for further study of user success indicators in he cross-cultural enterprise environment.

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A Validation Model for the Statistical Power Balance Method Using a Reverberation Chamber

  • Lee, Young Seung;Choi, Sung Woong;Park, Seung Keun
    • Journal of electromagnetic engineering and science
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    • 제13권3호
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    • pp.192-194
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    • 2013
  • This paper proposes a validation model using a reverberation chamber for verification of the effectiveness and accuracy of the statistical power balance (PWB) method. The PWB method treats electromagnetic (EM) field distributions in certain environments as a representative value of an "ensemble" average, so a reverberation chamber is utilized as a testing apparatus to experimentally simulate the sets of measurement field "ensemble" inside a complex environment. Measurements are performed with various test conditions for environmental loss using flat absorbers, and front and side doors of the chamber. Comparison between the PWB analysis and the measurement results shows good agreement, indicating the usefulness of this statistical analysis method for stating the electromagnetic field inside the EM zone as a representative value to general structures.

휴대용 근적외선 분광분석기를 이용한 비침투 혈당 측정 (Non-invasive Blood Glucose Measurement by a Portable Near Infrared (NIR) System)

  • 강나루;우영아;차봉수;이현철;김효진
    • 약학회지
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    • 제46권5호
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    • pp.331-336
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    • 2002
  • The purpose of this study is to develop a non-invasive blood glucose measurement method by a portable near infrared (NIR) system which was newly integrated by our lab. The portable NIR system includes a tungsten halogen lamp, a specialized reflectance fiber optic probe and a photo diode array type InGaAs detector; which was developed by a microchip technology based on the lithography. Reflectance NIR spectra of different parts of human body (finger tip, earlobe, and inner lip) were recorded by using a fiber optic probe. The spectra were collected over the spectral range 1100 ∼ 1740 nm. Partial least squares regression (PLSR) was applied for the calibration and validation for the determination of blood glucose. The calibration model from earlobe spectra presented better results, showing good correlation with a glucose oxidase method which is a mostly used standard method. This model predicted the glucose concentration for validation set with a SEP of 33 mg/dL. This study indicated the feasibility for non-invasive monitoring of blood glucose by a portable near infrared system.

PERUPS (PERFORMANCE UPGRADE SYSTEM) FOR ON-LINE PERFORMANCE ANALYSIS OF A NUCLEAR POWER PLANT TURBINE CYCLE

  • KIM SEONGKUN;CHOI KWANGHEE
    • Nuclear Engineering and Technology
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    • 제37권2호
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    • pp.167-176
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    • 2005
  • We developed the PERUPS system to aid the on-line performance analysis for the turbine cycle of the YongGwang 3 and 4 nuclear power plants. Procedure of measurement validation is included in the performance calculation to obtain heat balance. Precision of on-line performance calculation is increased via practical modifications of standard calculation algorithms based on the PTC (Performance Test Code). The proposed system also provides useful Web-based aids for performance analysis, including performance data management, a graphic viewer for heat balance and turbine expansion lines, and synthesized reports of performance.

유전체 코호트 연구의 주요 통계학적 과제 (Statistical Issues in Genomic Cohort Studies)

  • 박소희
    • Journal of Preventive Medicine and Public Health
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    • 제40권2호
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    • pp.108-113
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    • 2007
  • When conducting large-scale cohort studies, numerous statistical issues arise from the range of study design, data collection, data analysis and interpretation. In genomic cohort studies, these statistical problems become more complicated, which need to be carefully dealt with. Rapid technical advances in genomic studies produce enormous amount of data to be analyzed and traditional statistical methods are no longer sufficient to handle these data. In this paper, we reviewed several important statistical issues that occur frequently in large-scale genomic cohort studies, including measurement error and its relevant correction methods, cost-efficient design strategy for main cohort and validation studies, inflated Type I error, gene-gene and gene-environment interaction and time-varying hazard ratios. It is very important to employ appropriate statistical methods in order to make the best use of valuable cohort data and produce valid and reliable study results.

카메라영상에 의한 DGPS-GIS기반 차선변경 지원시스템의 평가 및 신뢰성 검증 (Assessment and Reliability Validation of Lane Departure Assistance System Based on DGPS-GIS Using Camera Vision)

  • 문상찬;이순걸;김민우;주다니
    • 한국자동차공학회논문집
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    • 제22권6호
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    • pp.49-58
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    • 2014
  • This paper proposes a new assessment and reliability validation method of Lane Departure Assistance System based on DGPS-GIS by measuring lanes with camera vision. Assessment of lane departure is performed with yaw speed measurement and determination method for false alarm of ISO 17361 and performance validation is executed after generating departure warning boundary line by considering deviation error of LDAS using DGPS. Distance between the wheel and the lane is obtained through line abstraction using Hough transformation of the lane image with camera vision. Evaluation validation is obtained by comparing this value with the distance obtained with LDAS. The experimental result shows that the error of the extracted distance of the LDAS is within 5 cm. Also it proves performance of LDAS based on DGPS-GIS and assures effectiveness of the proposed validation method for system reliability using camera vision.