• 한국자기학회지
• /
• 제5권5호
• /
• pp.841-845
• /
• 1995

The effect of small addition of Nb on the electrical resistivity and Hall coeffcient of the amorphous $Fe_{83}Zr_{7}B_{10}$ alloy and annealed ones ones below the crystallization temperature were investigated, which has been considered to be suitable for high frequency core material. At room temperature, their resistivities $\rho$ and the spontaneous Hall coeffcients $R_{s}$ are $~1.6\;{\mu}{\Omega}m$ and $~3{\times}10^{-8}m^{3}/As$, respectively. $R_{s}$ and $\rho$ are decreased with increasing temperature from 100 K to room temperature. Side-jump effect was adopted to analyze the effect of the small variation of conentration and annealing. The quantity of $R_{s}/{\rho}^{2}$ at room temperature, which is directly related to the electronic structure of the mother alloy, remained almost a constant except as quenched one as it can be predicted from the side-jump effect. The unexpected temperature dependence of $R_{s}/{\rho}^{2}$ measured at low fields much below Tc is left as a question.

• 한국지반공학회논문집
• /
• 제34권10호
• /
• pp.29-38
• /
• 2018

굴착공 저면에 형성된 슬라임은 현장타설말뚝의 과도한 침하 및 지지력 감소를 야기하므로 콘크리트 타설 전 해당 슬라임에 대한 조사가 요구된다. 본 연구에서는 굴착공 내 전기적 특성을 이용하여 굴착공 저면에 형성된 슬라임을 평가하기 위한 기법으로써 슬라임미터(slime meter)를 개발하였다. 슬라임미터는 전극 및 온도센서가 설치된 프로브 및 로터리엔코더가 설치된 프레임으로 구성되어 굴착공 심도에 따라 온도영향이 고려된 전기비저항을 평가할 수 있다. 슬라임미터의 적용을 위하여 직경 3m, 심도 46.9m의 굴착공에 대해 시험시간 및 위치가 서로 다른 총 3회의 현장실험이 수행되었다. 3회의 현장실험 모두 굴착공 내 유체에서 일정한 전기비저항이 측정되었으나 슬라임 표면이 존재하는 심도에서 전기비저항이 급격히 증가하는 결과를 보였으며, 해당 심도 및 지반 굴착심도의 차를 이용하여 슬라임의 두께를 산정할 수 있었다. 슬라임 두께 산정 결과, 동일 실험위치에서의 슬라임 두께는 시간 경과에 따라 증가하였으며 가장자리에서의 슬라임이 중앙부의 슬라임보다 두껍게 평가되었다. 본 연구에서 개발된 슬라임미터는 간소화된 장비구성으로 굴착공 내 전기비저항을 평가하여 슬라임 두께를 산정하므로 향후 굴착공 저면의 슬라임 평가를 위한 기법으로써 활용될 수 있을 것이라 기대된다.

• 전기학회논문지
• /
• 제63권3호
• /
• pp.367-370
• /
• 2014

The accelerated thermal aging of a CSPE were carried out for 0, 80.82, 161.63 days at $100^{\circ}C$, which are equal to 0, 40 and 80 years, respectively. The volume electrical resistivities of the non-accelerated thermally aged CSPE and the accelerated thermally aged CSPE for 40y and 80y were $9.620{\times}10^{12}{\sim}1.246{\times}10^{13}{\Omega}{\cdot}cm$, $5.066{\times}10^{12}{\sim}7.576{\times}10^{12}{\Omega}{\cdot}cm$ and $7.195{\times}10^{12}{\sim}9.208{\times}10^{12}{\Omega}{\cdot}cm$ at room temperature, respectively. The dielectric constant of the non-accelerated thermally aged CSPE and the accelerated thermally aged CSPE for 40y and 80y were 3.355~4.030, 2.996~3.963 and 3.020~4.776 at room temperature, respectively. After seawater and freshwater flooding, the volume electrical resistivity of the CSPE trend slightly upward according to drying day at room temperature. After seawater flooding, the dielectric constant of the accelerated thermally aged CSPE were not measured. After seawater flooding, bright open pores of the accelerated thermally aged CSPE were partly transferred to dark close pores due to salinity. After freshwater flooding, dark close pores of the accelerated thermally aged CSPE were partly transferred to bright open pores because salinity of them is decreased. An insulation property of a cable in NPPs was decreased because of the seawater flooding, and an insulation property of them was recovered through the freshwater flooding. As a result, it is considered that an insulation property of a contaminated cable through Tsunami can be recovered if it is cleaned quickly.

• 대한전기학회:학술대회논문집
• /
• 대한전기학회 2001년도 추계학술대회 논문집 전기물성,응용부문
• /
• pp.112-114
• /
• 2001

In this letter, we report on the investigation of Si/Ti, Pt/Si/Ti, Co/Si/Ti Ohmic contacts to p-type 4H-SiC. The contacts were formed by a 2-step vacuum annealing at $550^{\circ}C$ for 5 min, $850^{\circ}C$ for 2 min respectively. The contact resistances were measured using the transmission line model method, which resulted in specific $10^{-4}{\Omega}cm^2$, and the physical properties of the contactcontact resistivities in the $9.2{\times}10^{-4}$, $7.1{\times}10^{-4}$ and $4.5{\times}s$ were examined using microscopy, AES(auger electron spectroscopy). AES analysis has shown that, at this anneal temperature, there was a intermixing of the Ti and Si, migration of into SiC. Overlayer of Pt, Co had the effect of decreasing the specific contact resistivity and improving the surface morphology of the annealed contact.

• 한국세라믹학회지
• /
• 제51권5호
• /
• pp.459-465
• /
• 2014

In this study, Si-SiC composites were fabricated using a Si melt infiltration method using ${\beta}$-SiC/C composite powders synthesized by the carbothermal reduction of $SiO_2-C$ precursors made from a TEOS and a phenol resin. The purity of the synthesized SiC-C composite powders was higher than 99.9993 wt% and the average particle size varied from 4 to $6{\mu}m$ with increasing carbon contents of the $SiO_2-C$ precursors. It was found that the Si-SiC composites fabricated in this study consist of ${\beta}$-SiC and residual Si, without any trace of ${\alpha}$-SiC. The 3-point bending strengths of the fabricated Si-SiC composites were measured and found to be higher than 550 MPa, although the density of the fabricated Si-SiC composite was less than $2.9g/cm^3$. The bending strengths and the densities of the fabricated Si-SiC composites were found to decrease with increasing C/Si mole ratios in the SiC-C composite powders. The specific resistivities of the Si-SiC composites fabricated using the SiC-C composite powders were less than $0.018{\Omega}cm$. With increasing C content in the SiC-C composite powders used for the fabrication of Si-SiC composites, the specific resistivity of the Si-SiC composites was found to slightly increase from 0.0157 to $0.018{\Omega}cm$.

• 한국재료학회지
• /
• 제26권4호
• /
• pp.207-211
• /
• 2016

Ti films were deposited on glass substrates under various preparation conditions in a chamber of two-facing-target type dc sputtering; after deposition, the electric resistivity values were measured using a conventional four-probe method. Crystallographic orientations and microstructures, including the texture and columnar structure, were also investigated for the Ti films. The morphological features, including the columnar structures and surface roughness, are well explained on the basis of Thornton's zone model. The electric resistivity and the thermal coefficient of the resistivity vary with the sputtering gas pressure. The minimum value of resistivity was around 0.4 Pa for both the $0.5{\mu}m$ and $3.0{\mu}m$ thick films; the apparent tendencies are almost the same for the two films, with a small difference in resistivity because of the different film thicknesses. The films deposited at high gas pressures show higher resistivities. The maximum of TCR is also around 0.4 Pa, which is the same as that obtained from the relationship between the resistivity and the gas pressure. The lattice spacing also decreases with increasing sputtering gas pressure for both the $0.5{\mu}m$ and $3.0{\mu}m$ thick films. Because they are strongly related to the sputtering gas pressures for Ti films that have a crystallographic anisotropy that is different from cubic symmetry, these changes are well explained on the basis of the film microstructures. It is shown that resistivity measurement can serve as a promising monitor for microstructures in sputtered Ti films.

• 폴리머
• /
• 제29권2호
• /
• pp.156-160
• /
• 2005

Octamethylcyclotetrasiloxane$(D_4)$과 1,3,5-trimethyl-1,3,5-triphenylcyclotrisiloxane$(D_3^{Me,Ph)$을 1,1,3,3-tetramethyl-1,3-divinyldisiloxane(MVS)과 평형중합시켜 실리콘의 Si원자에 dimethyl 및 methylphenyl기가 도입된 $\alpha,\omega-vinyl$ poly(dimethyl-methylphenyl) siloxane prepolymer(VPMPS)를 제조하였으며, 또한 $D_4$와 1,3,5-trimethylcyclotrisiloxane$(D_3^:Me,H})$을 1,1,3,3-tetramethyldisiloxane(MS)와 평형중합시켜 Si원자에 dimethyl 및 methylhydrogen기가 도입된 $\alpha,\omega-hydrogen$ poly (dimethyl-methyl) siloxane prepolymer(HPDMS)를 제조하였다. Poly(acrylic acid)(PAA)을 chelating agent로 하여 nickel(II) nitrate와 iron(III) nitrate를 솔-젤 방법으로 PAA 금속염을 제조하고 이틀을 소결시켜 nickel ferrite 나노 입자를 제조하였다. 제조한 nickel ferrite는 XRD 패턴으로 확인하고 입자의 크기를 TEM으로 측정하였다 1,3-Divinyltetramethyldisilazane(VMS)으로 표면처리한 나노 실리카, nickel ferrite, VPMPS, HPDMS 및 촉매를 고속 교반기에 가하고 $130^{\circ}C$에서 컴파운딩하여 poly(organosiloxane) rubber nanocomposites를 제조하였다. Nickel ferrite 함유한 nanocomposite, POX-30과 POX-50을 각각 제조하였으며 이들의 기계적 및 열전도 특성 그리고 체적 저항을 측정하였다.

• 한국결정성장학회지
• /
• 제5권3호
• /
• pp.215-222
• /
• 1995

Floating zone법으로 $SrTiO_3$에 $Nb_2O_5$를 02wt% 첨가한 단결정을 육성하였다. 결정성장시 성장분위기로는 air와 질소분위기에서 각각 결정을 육성하였으며, 원료봉의 소결온도 따른 성장계면양상을 조사하였다. 성장조건으로는 성장속도는 5mm/hr, 상부축과 하부축의 회전속도는 30rpm이었고, air분위기시 air의 유량은 1.5 ${\ell}/min$, 질소분위기시 질소가스의 유량은 0.5 ${\ell}/min$이었다. 육성한 결정을 XRD, Laue, chemical etching 등의 분석을 하였으며, 질소분위기에서 annealing 한 후 비저항을 측정하였으며 이를 통해 activation energy를 조사하였다.

• 한국해안·해양공학회논문집
• /
• 제27권1호
• /
• pp.1-8
• /
• 2015

우리나라 남서해안은 풍력발전에 최적지로 평가받고 있으며 최근 해상풍력 구조물을 포함하는 해안구조물의 건설이 증가하고 있다. 그러나 우리나라 남서해안의 조차는 3~8 m까지 발생하여 남서해안에 설치되는 풍력기초들은 횡방향력과 조류의 다방향 흐름에 의한 세굴로 전체 구조물에 예상치 못한 진동에 의한 불안정성이 야기될 수 있다. 이 연구에서는 회전식 수리저항성능 실험기를 이용하여 인공지반시료의 수리저항성능을 평가하였으며 전기비저항 측정결과와 비교하여 수리저항성능과 전기비저항 특성과의 상관관계에 대한 연구를 진행하였다. 실험결과 일방향 한계전단응력과 양방향 한계전단응력을 상한계와 하한계로 표시하고 전기비저항 특성과 상관관계를 도시하면 조립토와 세립토가 비교적 명확히 구분되고 한계전단응력과의 상관관계 도출이 가능한 것으로 나타났다.

• 한국안전학회지
• /
• 제5권2호
• /
• pp.32-39
• /
• 1990

The ${\gamma}$-Fe$_2$O$_3$ compounds were oxidized in the furance after gas detecting sensor made molding as the Fe$_3$O$_4$ the synthesized Fe$_3$O$_4$, by ferrous sulfate and sodium hydroxide. Their sensities on carbon monoxide, ethyl alcohol and L. P. G. were measured at various temperatures, respectively. And then their electrical resistivities, thermal properties (D.T.A. ＆ T.G.A.), were examined about their having an effet on the gas-sensing in company with the effect of pure ${\gamma}$-Fe$_2$O$_3$ and the detecting sensor ${\gamma}$-Fe$_2$O$_3$, which reacts with $K_2$CO$_3$ in the hydrothermal coundition, and the electrical conductive mechanism was reflected simultaneously. It was observed that the electrical conductivities and response ratios showed highest value at the endothermic temperature part, 300~35$0^{\circ}C$ of D.T.A.―curve. Consequently, the response ratios and response times of the hydrothermal detecting sensor were higher than that of pure detecting sensor, the specific surface areas were the highest at the endothermic range of D.T.A.-curve. These response ratios of detecting sensor for $K_2$CO$_3$, process at hydrothermal condition on carbon monoxide appeared higher than that on ethyl alcohol and in case of L.P.G. last.