• 한국세라믹학회지
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• 제35권12호
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• pp.1249-1256
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• 1998

${\beta}$-Silicon carbide(${\beta}$-SiC) whiskers could be synthesized by the carbothermal reduction of kaolin at tem-peratures between 1400 and 1500$^{\circ}C$. The whiskers were grown up to about 1150 of aspect ratio by VS mechanism (showing tapering tips) and to about 45 of that by VLS mechanism (showing round droplet tips) respectively. Hydrocarbon like methane in the reaction atmosphere promoted the formation of gaseous il-icon monoxide(SiO) from silicon dioxide(SiO2) and subsequently reacted with it to form whiskers. The for-mation of ${\beta}$-SiC whiskers increased with increasing carbon content(to 30 wt%) and reaction temperatures. The max. yield of ${\beta}$-SiC whiskers was 15% at 1500$^{\circ}C$ under 20%CH4/80%H2.

• 한국기계연구소 소보
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• 통권16호
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• pp.83-94
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• 1986

Grinding machine, one of the precision machine tool, requires high accuracy in spindle system. But, recent Inspection and Test reports by KIMM shows high inferio¬rity ratio in home-made grinding machines and points out that this is mainly due to the lack of design ability and assembling technique of spindle system. In this paper, therefore, static stiffness, dynamic characteristics, thermal defor¬mation and error motion of spindle system were studied. With these results, we presented the general data to design and assemble the spindle system. Test of spindle system modified by this study showed that several factors affecting machining accuracy were improved largely.

• 한국경영과학회:학술대회논문집
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• 대한산업공학회/한국경영과학회 2002년도 춘계공동학술대회
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• pp.845-850
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• 2002

In this study we consider a flow-line CONWIP System with Compound Poisson Demands. The processing times of each workstation follow a Coxian-2 distribution. The demands that are not satisfied instantaneously are either backordered or lost according to the number of backordered demands that exist at their arrival instants. For this system we develop an approxi­mation method to obtain the performance measures such as steady state probabilities of the number of parts at each station, the average number of backordered demands and the proportion of the lost demands. Comparisons with simulation have shown that the approximate method provides fairly good results.

• 대한전기학회논문지
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• 제45권3호
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• pp.407-414
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• 1996

In this paper we consider the variable structure control for a class of discrete-time uncertain multivariable systems where the nominal system is linear. Discrete-time switching dynamics are introduced so that a new type of state trajectories called sliding mode may exist on the sliding surface by state feedback. The quantitative analysis for the matched uncertainties will show that every response of the system with the proposed switching dynamics is bounded within small neighborhoods of the state-space origin. Also, by the similarity transformation it will be shown that the eigenvalues of the closed-loop systems are composed of those of the subsystems which govern the range-space dynamics and null-space dynamics. It will be also shown that ideal sliding mode can be obtained in the absence of uncertainties due to one-step attraction to the sliding surface regardless of initial position of states. (author). 12 refs., 2 figs.

• 한국표면공학회지
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• 제29권5호
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• pp.585-592
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• 1996

In order to investigate the influence of gas pressure in PVD deposition conditions, aluminum films were prepared by vacuum evaporation and ion plating. The crystal orientation and morphology of the films affected by argon gas pressures were characterized by using X-ray diffraction (XRD) and scanning electron micrography (SEM) respectively. With the increasing of argon gas pressure, the preferred orientation of aluminum films exhibited (200) and the diffraction peaks of the films became less sharp and broadened. Film's morphology changed from columnar structure to granular structure with the increase of gas pressure. And the properties of these films on corrosion behaviors were estimated by measuring anodic polarization curves in deaerated 3% NaCl solution. The aluminum films which exhibited granular structure with (200) preferred orientation showed good corrosion resistance.

• Bulletin of the Korean Chemical Society
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• 제21권8호
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• pp.813-816
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• 2000

The synthesis of bisphenol A-derived calixarenes has been studied by changing the protecting group of the phe-nol moiety and reaction conditions. Depending on the protecting groups,the corresponding calix[6,7,8]arenes are obtained in different rat ios. For example, whcn mono-p-tert-butyldimethylsilyl-protected bisphenol A is treated with paraformaldehyde and a catalytic amount ofaqueous KOH in refluxing p-xylene with a Dean-Stark water collector for 36 h, the corresponding calix[8]arene, calix[7]arene, and calix[6]arene are producedand separated in the ratio of about 3 : 2 : l and with overall 63% yield. The calixarenes are characterized by NMR spectroscopy and mass analysis. The X-raycrystal structure of the calix[8]arene shows a pleated loop confor-mation, stabilized by intramoIecular hydrogen bonding between the inner phenolic hydroxy groups.

• Bulletin of the Korean Chemical Society
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• 제21권8호
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• pp.817-822
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• 2000

Crack-free hard coating siIica films were prepared by sol-gel processfrom twokinds of silicon alkoxide (tetra-ethoxysilane and methyltrimethoxysilane) and two kinds of alcohol (methanol and isopropyl alcohol) with an acid catalyst,acetic acid. A silicate framework of the precursor solution was investigated by infrared spectros-copy (IR) in the process of hydrolysis and condensation. Theextent of the condensation in the intermediates was elucidated by gel permeation chromatography (GPC) and 29Si-NMR spectroscopy. The hard coating films werecharacterized by IR,scanning electron microscope (SEM), thermo gravimetric analyzer (TGA) and dif-ferential scanning calroimeter (DSC). The synthetic condition for the crack-free and transparent silica film for-mation was optimized interms of starting materials for the precursor solution as well as preparation method of the silica film.

• Archives of Pharmacal Research
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• 제16권1호
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• pp.75-77
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• 1993

The cycloaddition reaction of N-phenyl-C-cinnamonitrilimine 4 to coumarin leads to the for-mation of 3-styrylbenzopyrano[4,3-c]pyrazole derivative 6, whereas 3-phenylsulfonylcoumarin 9 or 3-bromocoumain 10 or 3-cyanocoumarin 11 gives 1-styrylbenzopyrano[3,4]pyrazole derivative 7. Also, the cycloaddition of 4 to 3-acetylocoumarin 15 and 3-benzoylocumain 16 gives the corresponding dihydropyrano[3,4-c]pyrazole adducts 17 and 18 respectively. Oxidation of 17 and 18 gives 7.

• 한국산학기술학회논문지
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• 제18권6호
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• pp.636-645
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• 2017

국방기술정보관리를 위한 정보체계는 국방관련기관에서 개별적으로 보유하고 있는 데이터를 관리하고 적시에 제공하여 사용자의 업무 및 관리자의 의사결정을 지원해야한다. 본 연구의 목적은 국방기술정보관리체계인 DTiMS의 차세대 서비스 구축 방안을 제시함에 있다. 그동안 DTiMS는 법 제도적으로 부여된 임무인 국방과학기술정보 수집 관리 유통 역할을 수행함에 있어 수집관리 분야에 집중되어 왔다. 따라서 서비스 운영에 있어서 기술정보 유통분야 강화 및 수집관리방안 재정립이 필요한 시점이다. 이를 위해 수요자 관점에서 정보의 활용가치를 높일 수 있는 서비스 방향과 무기체계 총수명주기/기술획득 전 순기를 토대로 수집관리대상 기술정보 재정립 방안을 제시하였다. 본 연구에서는 국내 외 유관기관의 관리대상정보와 운영방안을 조사하여 비교 분석하였다. 또한 기존 서비스의 현황분석을 통해 관리대상정보 재정립, 정보관 연관성과 추적성, 사용자 활용성 강화를 위한 인터페이스 적용의 개선과제를 제시했다. 제안된 구축방향은 차세대 국방기술정보통합서비스(Defense Technology inforMation Service, DTiMS) 구축을 통하여 구현하였다. 본 연구의 결과는 향후 무기체계 총수명주기 서비스로 발전하는데 기여할 것으로 기대되며, 국방 기술기획, 연구개발, 정책 의사결정을 효과적으로 지원할 수 있는 도구로써 활용될 것이다.

• 한국소음진동공학회논문집
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• 제13권5호
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• pp.334-340
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• 2003

Exponential window function Is widely used In impact hammer testing to reduce leakage error as well as to get a good S/N ratio. The larger its decaying rate is, the more effectively the leakage errors are reduced. But if the decay rate of the exponential window is too large, the FRF is distorted. And the modal parameters of the system can not be exactly identified by modal analysis technique. Therefore, it is a difficult problem to determine proper decay rate in impact hammer testing. In this paper, amount of the FRF distortion caused by exponential window is theoretically uncovered. A new circle fitting method is also proposed so that the modal parameters are directly extracted from impulse response spectrum distorted by the exponential-windowed impulse response data. The results by the conventional and proposed circle fitting method are compared through a numerical example.