• Title/Summary/Keyword: material tests

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Estimation of Empirical Fatigue Crack Propagation Model of AZ31 Magnesium Alloys under Different Specimen Thickness Conditions (AZ31 마그네슘합금의 시편두께 조건에 따른 실험적 피로균열전파모델 평가)

  • Choi, Seon Soon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.2
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    • pp.646-652
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    • 2014
  • It is the primary aim of this paper to propose the empirical fatigue crack propagation model fit to describe a crack growth behavior of AZ31 magnesium alloys under the different specimen thickness conditions. The empirical models estimated are Paris-Erdogan model, Walker model, Forman model, and modified-Forman model. The parameters of each model are estimated by maximum likelihood method. The statistical crack growth data needed for an estimation of empirical models are obtained by fatigue crack propagation tests under the three cases of specimen thickness. It is found that the good empirical models fit to describe a crack growth behavior of AZ31 magnesium alloys under the different specimen thickness conditions are Paris-Erdogan model and Walker model. It is also verified that a fatigue crack growth rate exponent of a empirical model may be a material constant at the specimen thickness conditions of 4.75mm and 6.60mm.

A Study on the Separation of Mercury from Spent Mercury Batteries (단추형 폐수은 전지로부터 수은 분리에 관한 연구)

  • 손정수;박경호
    • Resources Recycling
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    • v.3 no.1
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    • pp.32-37
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    • 1994
  • Mercury in spent button type batteries can be separated and recovered with vacuum distillation method. It was found that mercury in the battery began to distill at $150^{\circ}C$ and organic substanced like a packing material was decomposed at$ 300^{\circ}C$. More than 99.9% of mercury contained in the battery was distiled and separated at about $250^{\circ}C$ and 20 torr with 8 hours' reaction time. The dissolution tests of the residue after distillation showed that mercury concentration in the solution were lower than 5 ppb and this values satisfied the environ-mental condition. Also as the furnace heating rate was above $15^{\circ}C$/min, it was found that the spent battery was destroyed because of increased pressure in the battery inside.

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Evaluation of the Basic Properties of Concrete with Types of Cellulose Fibers (셀룰로오스 섬유 종류에 따른 콘크리트의 기초 물성 평가에 관한 연구)

  • Park, Yong-Kyu;Lee, Joo-Hun;Jeon, In-Ki;Kim, Hyun-Woo;Yoon, Ki-Woon
    • Journal of the Korea Institute of Building Construction
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    • v.11 no.5
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    • pp.419-425
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    • 2011
  • Topping concrete that is not reinforced with rebar to prevent poor tensile performance is vulnerable to cracking. In this study, jute, which is known to be an excellent natural fiber material for strengthening concrete performance, was compared with other cellulose fibers in terms of its capacity to reduce the cracking of concrete. As a result, it was found that compared with concrete using other fibers, concrete using jute fiber showed more than a 50 % reduction of plastic shrinkage crack resistance with the contents of 0.9 kg/$m^3$ and 1.2 kg/$m^3$ for. For impact strength tests, the final destruction of WF and PULP fibers took up to 5 times the number of falls, while jute has 10-18 circuitry, showing excellent ductility properties.

Development of Fatigue Model for Asphalt Black Base by Accelerated Pavement Testing (포장가속시험을 이용한 아스팔트 안정처리층의 피로모형 개발)

  • Yeo, In-Soo;Suh, Young-Chan;Mun, Sung-Ho
    • International Journal of Highway Engineering
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    • v.9 no.4
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    • pp.11-20
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    • 2007
  • This thesis develops a fatigue model for the asphalt black base using the APT(Accelerated Pavement Testing) and analyzes the correlation of the APT analysis result with results of previous laboratory tests. For the APT testing, aggregate of the maximum grain size of 25mm(BB-3) was used as the material for the asphalt black base. The result of the APT revealed that the variable of the fatigue model, i.e. the maximum tensile stress on the bottom part of the pavement, increased as the number of loading increased while the modulus of elasticity for the pavement layer decreased gradually. The tensile strain was obtained from a strain gauge, and it was used to derive the values of $k_1=1.29{\times}10^{-6}$ and $k_2=3.02$ from the basic equation of the asphalt fatigue model, $N_f=k_1(\frac{1}{\epsilon})^{k_2}$. The fatigue life predicted from the asphalt fatigue model was greater than that obtained from laboratory experiments, given the same tensile strain. Additionally, a theory to estimate the remaining life of the pavement was developed using FWD, a non-destructive experiment.

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A Study on the Optimization of Curing Technology for Improving Properties of Concrete Pavement (콘크리트 포장의 내구성 향상을 위한 양생제 시공기술 최적화 연구)

  • Park, KwonJea;Ryu, SungWoo;Kim, HyungBae;Joo, YoungMin;Cho, Yoon-Ho
    • International Journal of Highway Engineering
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    • v.15 no.5
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    • pp.11-20
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    • 2013
  • PURPOSES : This study is to suggest time to spray curing compound, the amount of curing compound, and the number of times to spray curing compound based on indoor tests. METHODS : Based on the literature review, two methods are used in this study, One is test for water retention of concrete curing material and the other is test for abrasion resistance of concrete surfaces by the rotating-cutter method. Through those methods, curing compound was evaluated. RESULTS : The result of the laboratory experiment for time to spray curing compound indicates that 30 minutes after placing concrete is optimal. For the amount of curing compound, $0.5{\ell}/m^2$ is the minimum quantity for both concretes. Through test of the number of times to spray curing compound, method to spray the whole amount of curing compound in twice is more efficient than it to spray the whole amount at a time. Also, method of separately 30-50 minutes spray is better than method of separately 10-30 minutes spray. CONCLUSIONS : From the testing results, it can be proposed that optimum time to curing compound is $30{\pm}15$ minutes, $0.5{\ell}/m^2$ is efficient for spraying the whole amount of curing compound at a time, and $0.4{\ell}/m^2$ is the best for spraying the whole amount of curing compound in twice, which sprays it in 20 minutes after 30 minutes from placing concrete.

Adhesion Prevention with Guardix® (Sodium Hyaluronate) After Flexor Tendon Repair in Rabbits (토끼 모델에서 굴근 인대 봉합 후 가딕스®의 유착 방지 효과)

  • Kim, Hark Young;Chang, Hak;Minn, Kyung Won
    • Archives of Plastic Surgery
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    • v.36 no.5
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    • pp.543-547
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    • 2009
  • Purpose: Adhesion is the most common and troublesome complication after repair of flexor tendon injury. Recently, use of sodium hyaluronate derivatives for adhesion prevention is increasing. A commercial product, Guardix$^{(R)}$, sodium hyaluronate(NaHe) combined with carboxymethylcellulose(CMC) has been newly developed as a preventive material for adhesion. We have investigated its effect in rabbits. Methods: Twenty seven male New Zealand white rabbits were operated under ketamine anesthesia. After tendon repair in zone II of the hind paw, Guardix$^{(R)}$(experimental group) or normal saline(control group) was administered. Biomechanical tests were performed to estimate adhesion formation at 2, 4, 8, and 12 weeks after the operation. Maximum tensile load to flex the distal interphalangeal joint 50 degree from its resting state(MTL50) was measured, depicting the amount of adhesion formed. Subsequently, breaking strength was assessed. Results: There were no postoperative complications such as infection, wound dehiscence, or hematoma. MTL50 was significantly lower in the experimental group than in the control group at 4, 8, 12 weeks (p<0.05). Mean value of MTL50 was 6.64N in the experimental group and 28.53N in the control group at 12 weeks after surgery. There were no significant differences in breaking strength. Conclusion: Our results indicate that Guardix$^{(R)}$ is helpful in reducing adhesion formation and does not interfere with normal healing processes of the tendon.

Shear Performance of PUR Adhesive in Cross Laminating of Red Pine

  • Kim, Hyung-Kun;Oh, Jung-Kwon;Jeong, Gi-Young;Yeo, Hwan-Myeong;Lee, Jun-Jae
    • Journal of the Korean Wood Science and Technology
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    • v.41 no.2
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    • pp.158-163
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    • 2013
  • Cross laminated timber (CLT) has been an rising issue as a promising building material replacing steel-concrete in mid story rise construction. But, there was no specific standard for CLT because it had been developed in industrial section. Recently, new draft for requirements of CLT was proposed by EN which suggested to evaluate the performance of adhesive in CLT by the same method as glulam. But, it has been reported that shear performance of cross laminated timber is governed by rolling shear. Therefore, block shear tests were carried out to compare parallel to grain laminating and cross laminating using commercial one component PUR (Poly urethane resin). The result showed that the current glulam standard for evaluating bonding performance is not appropriate for CLT. Beacause shear strength of cross laminating decreased to 1/3 of parallel to grain laminating and this strength was representing shear performance of wood itself not the bond. However, cross laminating showed no significant effect on wood failure. Thus, wood failure can be used as a requirement of CLT bonding. Based on the results, cross laminating effect should be included when evaluating adhesive performance of CLT correctly and should be considered as an important factor.

Tribology Characteristics in 300 μm of Hexagonal Array Dimple Pattern

  • Choi, H. J.;Hermanto, A. S.;Kwon, S. H.;Kwon, S. G.;Park, J. M.;Kim, J. S.;Chung, S. W.;Chae, Y. H.;Choi, W. S.
    • Tribology and Lubricants
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    • v.31 no.6
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    • pp.308-315
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    • 2015
  • In the tribological performance of materials, a textured surface reduces the friction coefficient and wear. This study investigates the effects of a pattern of 300 µm dimples in a hexagonal array on the tribological characteristics. Previous studies investigated 200 µm dimples by using a similar material and method. There are three frictional conditions based on the Stribeck curve: boundary friction, mixed friction, and fluid friction. In this experiment, we investigated the frictional characteristics by conducting frictional tests at sliding speeds ranging from 9.6 rpm to 143.3 rpm and a normal load ranging from 13.6 N to 92 N. We used a photolithography method to create dimples for surface texturing. We used five specimens with different dimple densities 10%, 15%, 20%, 25%, and 30% in this study. The dimple density on the surface area is one of the important factors affecting the friction characteristics. The duty number graph indicates a fully developed fluid friction regime. Fluid friction occurs at a velocity of 28.7-143.3 rpm. We observed the best performance at a dimple density of 10% and a dimple diameter of 300 µm in the hexagonal array, the lowest friction coefficient at 0.0037 with 9.6 rpm 9.6N load, and the maximum friction coefficient at 0.0267 with 143.3 rpm 92N load.

Adhesion Characteristics between Mold and Thermoplastic Polymer Film in Thermal Nanoimprint Lithography (열 나노임프린트 리소그래피에서의 몰드와 열가소성 폴리머 필름 사이의 응착 특성)

  • Kim, Kwang-Seop;Kang, Ji-Hoon;Kim, Kyung-Woong
    • Tribology and Lubricants
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    • v.24 no.5
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    • pp.255-263
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    • 2008
  • Adhesion tests were conducted to investigate the adhesion characteristics between mold and thermoplastic polymer film. Coating of anti-sticking layer (ASL), a kind of polymer material, imprint pressure, and separation velocity were considered as the process conditions. A piece of fused silica without patterns on its surface was used as a mold and the thermoplastic polymer films were made on Si substrate by spin-coating the commercial polymer solution such as mr-I PMMA and mr-I 7020. The ASL was derived from (1H, 1H, 2H, 2H - perfluorooctyl) trichlorosilane($F_{13}$-OTS) and coated on the fused silica mold in vapor phase. The pull-off force was measured in various process conditions and the surfaces of the mold and the polymer film were observed after separation. It was found that the adhesion characteristics between the mold and the thermoplastic polymer film and the release performance of ASL were changed according to the process conditions. The ASL was effective to reduce the pull-off force and the damage of polymer film. In cases of the mold coated with ASL, the pull-off force did not depend on imprint pressure and separation velocity.

Fatigue Fracture Characteristics by Corrosion Degradation of 12Cr Alloy Steel (12Cr합금강의 부식열화에 의한 피로파괴 특성)

  • Jo, Seon-Yeong;Kim, Cheol-Han;Bae, Dong-Ho
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.25 no.6
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    • pp.996-1003
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    • 2001
  • In order to investigate the fatigue fracture characteristics by corrosion degradation of 12Cr alloy steel, both the fatigue characteristics in air of them artificially degraded during long period and the corrosion fatigue characteristics were experimentally evaluated in various environments which were determined from electro-chemical polarization tests. And also, their fracture mechanisms were analyzed and compared, fractographyically. From their results, the fracture mechanical characteristics of it artificially degraded during long period in the distilled water, 3.5 wt.% NaCl solution and 12.7wt.%(1M) Na$_2$SO$_4$solution of 25, 60 and 90$\^{C}$ did not show distinguishable difference comparing with non-corroded one in regardless of temperature and degradation period. It means that degradation of the material by just surface corrosion does not remarkably affect to fatigue crack growth. On the other hand, the crack growth rates by corrosion fatigue increased due to activity increase of corrosive factors such as OH(sub)-,Cl(sup)- and SO$_4$(sup)- at the crack tip with temperature increase. Therefore, the crack growth rates by corrosion fatigue were more faster than that in air of the artificially degraded specimen due to the such difference of crack growth mechanism.