• 한국분말재료학회지
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• 제19권3호
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• pp.210-214
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• 2012

Mass production-capable $Li_2MnSiO_4$ powder was synthesized for use as cathode material in state-of-the-art lithium-ion batteries. These batteries are main powder sources for high tech-end digital electronic equipments and electric vehicles in the near future and they must possess high specific capacity and durable charge-discharge characteristics. Amorphous silicone was quite superior to crystalline one as starting material to fabricate silicone oxide with high reactivity between precursors of sol-gel type reaction intermediates. The amorphous silicone starting material also has beneficial effect of efficiently controlling secondary phases, most notably $Li_xSiO_x$. Lastly, carbon was coated on $Li_2MnSiO_4$ powders by using sucrose to afford some improved electrical conductivity. The carbon-coated $Li_2MnSiO_4$ cathode material was further characterized using SEM, XRD, and galvanostatic charge/discharge test method for morphological and electrochemical examinations. Coin cell was subject to 1.5-4.8 V at C/20, where 74 mAh/g was observed during primary discharge cycle.

• 한국정밀공학회지
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• 제33권3호
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• pp.235-242
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• 2016

The purpose of this study is an attempt to improve the functionality of a conventional Fused Deposition Modeling (FDM) process using the Automatic Tool Changer (ATC) to perform multimaterial production and post-processing. Hybrid-FDM means a fusion of an Additive Manufacturing process and grinding process using the ATC system. In order to enhance the potentiality of production capacity for multi-material fabrication and surface roughness improvement, two extrusion tools and one grinding tool system are suggested. A pneumatic chuck is attached on a moving platform in the XY axes plane and an extrusion head and grinding head are placed in a docking station, allowing for a quick changeover with each other. Therefore, the manufacturing lead time can be reduced efficiently for the fabrication of a product.

• 한국세라믹학회지
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• 제42권8호
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• pp.532-536
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• 2005

Thermal shock resistance of structural ceramics is a property that is difficult to quantity, and as such is usually expressed in terms of a number of empirical resistance parameters. These are dependant on the conditions imposed, but one method that can be used is the examination of density, Young's modulus and thermal expansion retention after quenching. For high temperature applications, long-annealing thermal durability, cycle thermal stability and residual mechanical properties are very important if these materials are to be used between $1000^{\circ}C$ and $1300^{\circ}C$. In this study, an excellent thermal shock-resistant material based on $Al_2TiO_5-mullite$ composites of various compositions was fabricated by sintering reaction from the individual oxides and adjusting the composition of $Al_2O_3TiO_2/SiO_2$ ratios. The characterization of the damage induced by thermal shock was done by measuring the evolution of the Young's modulus using ultrasonic analysis, density and thermal expansion coefficients.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2009년 추계학술발표대회
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• pp.239-242
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• 2009

Friction stir spot welding (FSSW), developed based on principle of friction stir welding, has been paid attention as a new solid-state spot welding process. Since FSSW can produce high-quality weld in Al alloys more easily than resistance spot welding, this process has been already used for construction of Al components in the automotive industries. Despite the large industrial interests in FSSW, fundamental knowledge on welding phenomena of this process has not been fully understood. In this study, FSSW phenomena, such as the consolidation mechanism, the microstructural evolution and the material flow, were examined in Al alloy 6061. This study clarified that the elliptical zone found in the vicinity of the pin hole on the cross section was characterized by the initially lapped surface of two sheets. Moreover, the following material flow was proposed; capture of the upper material with the threads on the pin surface, spiral flow along the tool rotation, and then release at the tip of the pin.

• 한국해양공학회:학술대회논문집
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• 한국해양공학회 2004년도 학술대회지
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• pp.1-6
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• 2004

This paper shows the study on the design and another applications of the spray-freeze dryer for the production of valuable material powders. Powder production and handling has been an integral part of material extracting processing and pharmaceutical processing because of the wide use of oral dosage forms. There are a few commonly used powder preparation methods including mechanical milling, precipitaion, spray drying, freeze drying, and so on. In general, methods available for preparing inhalation powders are limited due to certain inhalation powder's sensitive nature to the processing environments. This is particularly true for preparing dry powder aerosols where the aerodynamic particle size($<5{\mu}m$) and the size distribution are pivotal. Supercritical fluid antisolvent and spray freeze drying have recently emerged as promising techniques for producing powders for use in microcapsulation. However, the aerosol applications of these powders are yet to be explored. The purpose of this study is to test the feasibility of using spray freeze-dried valuable material powders for aerosolization.

• 소성∙가공
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• 제21권7호
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• pp.412-419
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• 2012

The ingot-breakdown scheme of a tower flange material (low-alloy steel) for offshore wind turbine was investigated using finite element (FE) simulations and experimental analyses. Based on compression test results of the low-alloy steel, a deformation processing map was generated using the superposition approach between the dynamic materials model (DMM) and Ziegler's instability criterion. The deformation processing map allowed determination of the optimum process conditions for the tower flange material. Within the FE simulations of the ingot breakdown process, the Cockcroft-Latham criterion, which considers ductile fracture, was used to predict the possibility of forming defects during the hot working process. In general, the critical value for the ductile fracture of steel is 0.74. During the ingot-breakdown under optimum process conditions, the actual tower flange forgings exhibited a relatively uniform shape without any forming defects.

• 한국재료학회지
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• 제26권5호
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• pp.266-270
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• 2016

Glass-ceramics were developed many years ago and have been applied in many fields such as electronics, chemistry, optics, etc. Much is already known about glass-ceramic technology, but many challenges in glass-ceramic research are still unresolved. Recently, large amounts of slag have steadily increased in the steel industry as by-products. To promote recycling of industrial waste, including steel industry slags, many studies have been performed on the fabrication of basalt-based high-strength glass-ceramics. In this study, we have fabricated such ceramics using various slags to replace high performance cast-basalt, which is currently imported. Glass-ceramic material was prepared in similar chemical compositions with commercial cast-basalt through a pyro process using slags and power plant by-product (Fe-Ni slag, converter slag, dephosphorization slag, Fly ash). The properties of the glass-ceramic material were characterized using DTA, XRD, and FE-SEM; measurements of compressive strength, Vicker's hardness, and abrasion were carefully performed. It is found that the prepared glass-ceramic material showed better performance than that of commercial cast-basalt.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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• pp.493-498
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• 2002

Friction stir welding (FSW) is a relatively new solid-state joining process which can homogenize the heterogeneous microstructure by intensely plastic deformation arising from the rotation of the welding tool. The present study applied the FSW to an A356 aluminum (AI) alloy with the as-cast heterogeneous microstructure in the T6 temper condition, and examined an effect of microstructure on mechanical properties in the weld. The base material consisted of Al matrix with a high density of strengthening precipitates, large eutectic silicon and a lot of porosities. The FSW led to fragment of the eutectic silicon, extinction of the porosities and dissolution of the strengthening precipitates in the Al alloy. The dissolution of strengthening precipitates reduced the hardness of the weld around the weld center and the transverse ultimate tensile strength of the weld. Longitudinal tensile specimen containing only the stir zone showed the roughly same strength as the base material and a much larger elongation. Moreover, Charpy impact tests indicated that the stir zone had remarkably the higher absorbed energy than the base material. The higher mechanical properties of the stir zone were attributed to a homogenization of the as-cast heterogeneous microstructure by FSW.

• 한국세라믹학회지
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• 제41권4호
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• pp.323-327
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• 2004

본 연구는 석회석, 셰일, 전로슬래그, 플라이 애쉬를 사용한 혼합원료에 대해 보통 포틀랜드 시멘트 원료로서 하수슬러지 소각재의 사용에 대해 조사하였다. 이와 관련하여 원료 중 셰일에 대한 하수슬러지의 적정 치환 비율을 확인하였으며, 1,300, 1,350, 1,400, 1,450, 1,50$0^{\circ}C$에서 1시간 혼합원료를 소성하였다. 이후 공기중 급냉을 시행하였으며, XRD, SEM을 통하여 합성된 클링커의 특성을 평가하였다. 또한, 클링커의 미반응 산화칼슘을 측정하여 소성성에 대한 결과를 얻었다.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1999년도 춘계학술대회 논문집
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• pp.712-715
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• 1999

Treeing has a profit to observe processing electrical breakdown because it gives degradation steps of insulation material by optical method. But, reappearance properly of treeing is not so good and precise quantization of tree growth is not so easy because tree Patterns are very complicate. The study on tree growth using image processing is predicted to precision of tree degradation and possible to quality measurement of tree pattern. In this paper, degradation steps are analyzed by image processing, therefore precision and realiability of tree growth are increased. Also, processing of tree degradation is quantized by fractal.