• Title/Summary/Keyword: material homogeneity

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Measurement of Heavy Metals Using Portable XRF in Children's Playing Goods (Portable XRF를 이용한 어린이 야외 놀이용품의 중금속 측정)

  • Kim, Hyung-Jin;Baek, Young Man;Jung, Kyung Hoon;Hong, Suk Youn;Heo, Hwa Jin;Seong, Jin Uk;Park, Je Chul
    • Journal of Environmental Science International
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    • v.22 no.4
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    • pp.471-479
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    • 2013
  • The present study was conducted to judge the applicability of field quality control by children's goods manufacturers by assessing the contents of heavy metals such as Pb and Cd in outdoor play goods for children through measurement using Portable XRF and comparing the results through detailed analyses using ICP. Heavy metal contents of 711 part samples of 505 products were measured using XRF. According to the results, the ratio of products that exceeded the Pb and Cd content standards specified under the Quality Management and Safety Control of Industrial Products Act were 2.4% and 2.6%. Many products certified for self-regulated safety exceeded the standards and thus it was considered that harmful chemical material centered safety management systems would be necessary. Detailed ICP analyses of some products were compared and the results showed deviations of 0.9~80.8% from XRF results. The reasons for this are deviations in the characteristics of measured cross sections and the homogeneity of samples resulting from sample preparation methods, etc. Therefore, it is considered that field quality control will be applicable if measuring methods are efficiently established based on product characteristics and calibration curve preparation methods are established through quality control.

The study on Development and characteristic of ultrasound biopsy training phantom of breast (유방 초음파 팬텀의 제작과 특성에 관한 연구)

  • Ma, Sang-Chull;Kong, Young-Kun;Ahn, Young-Man
    • Journal of radiological science and technology
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    • v.26 no.3
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    • pp.19-24
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    • 2003
  • We carried out studies on development and characteristic of ultrasound brast training biopsy phantom. the major finding were of follow ; (1) C type TMM was shown good homogeneity, brightness and attenuation as like human soft tissue. (2) $TiO_2$ 4.10%w/v TMM was shown good homogeneous echo texture and propagated speed as like the human Tissue. (3) $TiO_2$ type TMM was appeared lower brightness and higher penetration rate than C type TMM. Therefor, Breast TM phantom and target material TMM will be useful $TiO_2$ 4.10 %w/v TMM and C 2.09 %w/v TMM.

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Comparative Analysis of the Weight Functions for the Reconstruction of a Gamma-ray CT based on the EM Technique (EM기반의 감마 CT 영상복원을 위한 가중치 함수 비교분석)

  • Lee, Na-Young;Jung, Sung-Hee;Kim, Jong-Bum;Kim, Jin-Sup;Kim, Jae-Ho
    • Journal of the Korean Society for Nondestructive Testing
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    • v.27 no.5
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    • pp.449-458
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    • 2007
  • In this paper, we reconstructed the cross-sectional images of two phantoms simulating a petrochemical process from gamma radiation measurements. Three different weight functions for EM image reconstruction algorithm were built and compared with histograms representing the variance of the homogeneity of the phantom material, The radiation source, $^{137}Cs$, collimated by a lead with 5 mm diameter aperture and the measurement was made with a lead shielded 1inch NaI detector. As a result, the method taking into account the beam area in each pixel for a weight function showed the best resolution among the three methods.

Applying a Forced Censoring Technique with Accelerated Modeling for Improving Estimation of Extremely Small Percentiles of Strengths

  • Chen Weiwei;Leon Ramon V.;Young Timothy M.;Guess Frank M.
    • International Journal of Reliability and Applications
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    • v.7 no.1
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    • pp.27-39
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    • 2006
  • Many real world cases in material failure analysis do not follow perfectly the normal distribution. Forcing of the normality assumption may lead to inaccurate predictions and poor product quality. We examine the failure process of the internal bond (IB or tensile strength) of medium density fiberboard (MDF). We propose a forced censoring technique that closer fits the lower tails of strength distributions and better estimates extremely smaller percentiles, which may be valuable to continuous quality improvement initiatives. Further analyses are performed to build an accelerated common-shaped Weibull model for different product types using the $JMP^{(R)}$ Survival and Reliability platform. In this paper, a forced censoring technique is implemented for the first time as a software module, using $JMP^{(R)}$ Scripting Language (JSL) to expedite data processing, which is crucial for real-time manufacturing settings. Also, we use JSL to automate the task of fitting an accelerated Weibull model and testing model homogeneity in the shape parameter. Finally, a package script is written to readily provide field engineers customized reporting for model visualization, parameter estimation, and percentile forecasting. Our approach may be more accurate for product conformance evaluation, plus help reduce the cost of destructive testing and data management due to reduced frequency of testing. It may also be valuable for preventing field failure and improved product safety even when destructive testing is not reduced by yielding higher precision intervals at the same confidence level.

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Flow Measurement in Bubbly and Slug Flow Regimes Using The Electromagnetic Flowmeter Developed (전자기유량계를 이용한 기포 및 슬러그 유동 측정방법 연구)

  • Cha, Jae-Eun;Ahn, Yeh-Chan;Seo, Kyung-Woo;Kim, Moo-Hwan
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.26 no.11
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    • pp.1559-1569
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    • 2002
  • In order to investigate the characteristics of electromagnetic flowmeter in two -phase flow, an AC electromagnetic flowmeter was designed and manufactured. In various flow conditions, the signals and noises from the flowmeter were obtained and analyzed by comparison with the observed flow patterns with a high speed CCD camera. The experiment with the void simulators in which rod shaped non-conducting material was used was carried out to investigate the effect of the bubble position and the void fraction on the flowmeter. Based on the results from the void simulator, two -phase flow experiments encompassed from bubbly to slug flow regime were conducted. The simple relation $\Delta$ $U_{TP}$ = $\Delta$ $U_{SP}$ (l-$\alpha$) was verified with measurements of the potential difference and the void fraction. Due to the lack of homogeneity in a rent two -phase flow, the discrepancy between the relation and the present measurement was slightly increased with void fraction and also liquid volumetric flux jf. Whereas there is no difference in the shape of the raw signal between single-phase flow and bubbly flow, the signal amplitude for bubbly flow is higher than that for single -phase flow at the same water flow rate, since the passage area of the water flow is reduced. In the case of slug flow, the phase and the amplitude of the flowmeter output show dramatically the flow characteristics around each slug bubble and the position of a slug bubble itself. Therefore, the electromagnetic flowmeter shows a good possibility of being useful for identifying the flow regimes.ul for identifying the flow regimes.

A Study on the Types of Social Networks of Housewives in Urban Nuclear Families (가족의 사회관계망 유형화 연구 - 도시 핵가족 주부를 중심으로 -)

  • 원효종;옥선화
    • Journal of Families and Better Life
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    • v.20 no.4
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    • pp.149-164
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    • 2002
  • The purpose of this study was to identify the types of social networks of urban housewives according to different network composition patterns and to analyze the structural and functional characteristics of identified types. The data used in this study were collected from 589 full-time housewives residing in Taejeon city. The major findings are as follows: 1) The social networks of housewives in urban nuclear families were classified into eight types: the kin network, the non-kin network, the kin-centered network, the friend-centered network, the neighbor-centered network, the associate-centered network, the parallel network, and the decentralized network. 2) The structual characteristics (size, density, homogeneity, duration, proximity, frequency, closeness, direction) varied according to the type. The kin network type and the non-kin network type showed extreme degrees in network characteristics. The parallel network type and the decentralized network type showed an average level of network characteristics. The kin-, friend-, neighbor-, and the associate-centered types showed network characteristics of an intermediate level between the single-category types and the decentralized type. 3) The average levels of function of social network types were different in only two(service support, interference) of the six function areas(emotional support, service support, material support, information support, social companionship support, interference). The average level of service support by the non-kin network type was higher than other types. The average level of interference by the kin-centered network type was higher than other types, and that of the neighbor-centered network type was lower than other types. On the other hand, the total amount of function performance of social network types was different in all function areas. The total amount of social support given by the decentralized network type was greater than the other types. The total amount of interference given by the non-kin network type was smaller than the other types.

Effect of Melt-Spinning Process on Hydrogen Storage Properties of Mass-Produced Ti0.85Zr0.13(Fex-V)0.56Mn1.47Ni0.05 Alloy (대량용해 Ti0.85Zr0.13(Fex-V)0.56Mn1.47Ni0.05 수소저장합금의 용융방사공정을 통한 수소저장특성)

  • Kim, Jinho;Han, Kyusung
    • Journal of Hydrogen and New Energy
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    • v.24 no.5
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    • pp.367-372
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    • 2013
  • Hydrogen storage as a metal hydride is the most promising alternative because of its relatively large hydrogen storage capacities near room temperature. TiMn2-based C14 Laves phases alloys are one of the promising hydrogen storage materials with easy activation, good hydriding-dehydriding kinetics, high hydrogen storage capacity and relatively low cost. In this work, multi-component, hyper-stoichiometric $Ti_{0.85}Zr_{0.13}(Fe_x-V)_{0.56}Mn_{1.47}Ni_{0.05}$ C14 Laves phase alloys were prepared by a vacuum induction melting for a hydrogen storage tank. Since pure vanadium (V) is quite expensive, the substitution of the V element in these alloys has been tried and some interesting results were achieved by replacing V by commercial ferrovanadium (FeV) raw material. In addition, the melt-spinning process, which was applied to the manufacturing of some of these alloys, could make the plateau slopes much flatter, which resulted in the increase of reversible hydrogen storage capacity. The improvement of sloping properties of melt-spun $Ti_{0.85}Zr_{0.13}(Fe_x-V)_{0.56}Mn_{1.47}Ni_{0.05}$ alloys was mainly attributed to the homogeneity of chemical composition.

Manufacturing of GFRP Sheet Using Plain Weaving Method (평직직조방법을 적용한 GFRP Sheet 제조에 관한 연구)

  • Kim, in Woo;Kim, Hyoung Seok;Lee, Jung Hoon;Lee, Dong Gi
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.38 no.8
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    • pp.849-855
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    • 2014
  • The GFRP composite is used for hot press flow molding of automotive components, and the different flow rates of fiber and plastic are likely to induce fiber orientation and inhomogeneity in the material. However, very limited systematic research studies are available on composite materials with superior flow homogeneity and optimized fiber orientation. The inhomogeneity and fiber orientation issues of GFRP composites have still not been resolved through research. The plain weaving method applied to the GFRP prepreg can improve its recyclability, inhomogeneity, fiber flow, structural stability, fiber deformation, surface smoothness, degree of impregnation, and other mechanical properties. The need for more detailed and thorough studies is evidenced.

Detecting Incipient Caries Using Front-illuminated Infrared Light Scattering Imaging

  • Kim, Ji-Young;Ro, Jung-Hoon;Jeon, Gye-Rok;Kim, Jin-Bom;Ye, Soo-Young
    • Transactions on Electrical and Electronic Materials
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    • v.13 no.6
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    • pp.310-316
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    • 2012
  • A new method for early caries diagnosis was proposed and tested through a home-made optical examination system that used quantitative light fluorescence (QLF) and digital imaging fiber optic transillumination (FOTI) (DIFOTI), with light sources across a wide spectral range, from 350 nm to 1,000 nm. The front-illuminated infrared light scattering image (FIR) showed similar diagnostic abilities to that of DIFOTI. The FIR method was invented based on the observation that caries lesions lose the high transmittance and low scattering properties of benign enamel tissue. There are various methods for the early diagnosis of caries, such as visual examination, exploration, X-ray radiography, QLF, FOTI, and infrared fluorescence (diagnodent). Among them, methods based on optical properties are regarded as having the most potential. A comparative study was performed between the FOTI, QLF, diagnodent, optical coherence tomography, and FIR scattering image methods, using 20 extracted teeth samples with early caries. A scale of lesion measurement based on optical image contrast was proposed. The statistical analysis showed a significant correlation between the DIFOTI and FIR methods (r = 0.35, p < 0.05). However, the QLF and diagnodent methods showed little association with FIR images, as they have different detection principles as compared with FIR. Tomographic images obtained by OCT, using 1,330 nm super luminescent LED as a gold standard of tooth structure, verified that the FOTI and FIR results correctly represented the lack of homogeneity in dental tissue. The newly proposed FIR method attained similar diagnostic results to those of FOTI, but with an easier approach.

Thermodynamic Prediction of SiC Deposition in C3H8-SiCl4-H2 System (C3H8-SiCl4-H2 시스템에서의 탄화 실리콘 증착에 대한 열역학적인 해석)

  • Kim, Jun-Woo;Jeong, Seong-Min;Kim, Hyung-Tae;Kim, Kyung-Ja;Lee, Jong-Heun;Choi, Kyoon
    • Journal of the Korean Ceramic Society
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    • v.48 no.3
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    • pp.236-240
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    • 2011
  • In order to deposit a homogeneous and uniform ${\beta}$-SiC films by chemical vapor deposition, we demonstrated the phase stability of ${\beta}$-SiC over graphite and silicon via computational thermodynamic calculation considering pressure, temperature and gas composition as variables. The ${\beta}$-SiC predominant region over other solid phases like carbon and silicon was changed gradually and consistently with temperature and pressure. Practically these maps provide necessary conditions for homogeneous ${\beta}$-SiC deposition of single phase. With the thermodynamic analyses, the CVD apparatus for uniform coating was modeled and simulated with computational fluid dynamics to obtain temperature and flow distribution in the CVD chamber. It gave an inspiration for the uniform temperature distribution and low local flow velocity over the deposition chamber. These calculation and model simulation could provide milestones for improving the thickness uniformity and phase homogeneity.