• Journal of the Korean Society of Safety
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• v.30 no.4
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• pp.8-13
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• 2015

The magnetic shape memory alloys have recently received a lot of attention due to the considerable progress achieved in understanding the particular importance and the development of the factors. Among these alloys, the ferromagnetic Co-Ni- alloys have been concerned specially because of the thermoelastic character of the fcc (g) - bct (a) martensitic transformation which exhibits under the action of the temperature (shape memory effect), the stress (superelasticity) and the magnetic field (magnetoelasticity). The morphological, the crystallographical, and the thermal characteristics of thermally induced martensite in Co-35.3Ni-11.3Al(wt.%) and Co-28.1Ni-47.4Fe-3.3Ti (wt.%) alloy have been investigated by the scanning electron microscope (SEM), the X-ray Diffraction (XRD), and the differential scanning calorimeter (DSC).

• Laser Solutions
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• v.2 no.2
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• pp.27-33
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• 1999

Electron beam was applied on the low carbon steel in order to fabricate Metal/Metal GBM(Graded Boundary Material). Ni sheet was placed on the steel substrate. The electron beam was irradiated on the surface and produced a homogeous alloyed layer. Sequential repetition of electron beam treatments for 4 times resulted in 8mm thick graded layer. To determine each layers property, optical microscopy, XRD, microhardness tester and EDS were used. The residual stress was measured by the low angle x-ray diffraction method. The graded boundary layer was stepwise profile, but Ni content incresed up to 80 wt% and Fe content decreased 20 wt% near surface. Each layers microstructure and hardness varied by different Fe/Ni composition. The compressive residual stress was induced by martensite transformation in the 1st and End layers and the shrinkage cracks were formed in graded layer by rapid cooling.

• Korean Journal of Materials Research
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• v.10 no.9
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• pp.642-647
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• 2000

Nanocrystalline NiAl alloy containing 36at.%Al was synthesized by mechanical alloying (MA). Synthesized powder was sintered by a pulse electric current sintering (PECS) facility. Effecting parameters on the phase transformation were discussed in terms of cooling rate and time spent on heat treatment. The behavior of phase transformation for sintered parts was examined by differential scanning calorimetry (DSC) and X-ray diffraction (XRD) method. Microstructure was observed by scanning electron microscopy (SEM). Martensitic lattice parameter and volume fraction was calculated by direct comparison method in X-ray diffraction analysis.

• Corrosion Science and Technology
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• v.17 no.3
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• pp.129-137
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• 2018

The resistance to corrosion of additive manufactured (3D printing) Ti-6Al-4V alloys was investigated using micro-electrochemical tests. In terms of corrosion resistance, the acicular martensitic ${\alpha}^{\prime}$ phase in such additive manufactured Ti-6Al-4V was the focus of attention, and its behavior was distinct from that of conventional subtractive manufactured Ti-6Al-4V. To order to identify ${\alpha}^{\prime}$ phase, XRD tests were performed and micro Vickers hardness was measured for different grains (bright and dark grains) in the additive manufactured Ti-6Al-4V alloy. Micro-electrochemical tests were performed to measure corrosion resistance of bright and dark grains in the additive manufactured Ti-6Al-4V alloy with specially designed electrochemical micro-droplet cell. Critical pitting temperature (CPT) measurement was performed to evaluate the resistance to pitting corrosion of additive manufactured Ti-6Al-4V alloys with different volumes of ${\alpha}^{\prime}$ phase and subtractive manufactured Ti-6Al-4V alloy. The dark grains of the laminated Ti-6Al-4V alloy distributed broader than the bright grains measured with low microhardness. The dark grains of the Ti-6Al-4V alloy, which was rich in martensite ${\alpha}^{\prime}$, had lower general corrosion and pitting resistance than bright grains. As the fraction of martensite ${\alpha}^{\prime}$ phase increased, the resistance to the pitting corrosion decreased.

• Journal of the Korean Society for Heat Treatment
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• v.36 no.5
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• pp.303-310
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• 2023

β titanium alloys are widely used in aerospace industry due to their excellent specific strength and corrosion resistance. In particular, mechanical properties of metastable β titanium can efficiently be controlled by various deformation mechanisms such as slip, twinning, and SIM (Stress-Induced Martensite Transformation), making it an ideal material for many industrial applications. In this study, Ti-5Mo-xFe (x=1, 2, 4 wt%) alloy was designed by adding a relatively inexpensive β element to ensure price competitiveness. Additionally, microstructural analysis was conducted using OM, SEM, and XRD, while mechanical properties were evaluated through hardness and compression tests to consider the deformation mechanisms based on the Fe content. SIMT occurred in all three alloys and was influenced by the presence of β_m (metastable beta) and beta stability. As the Fe content decreased, the α'' phase increased due to SIMT occurring within the β_m phase, resulting in softening. Conversely, as the Fe content increased, the strength of the alloy increased due to a reduction in α'' formation and the contributions of solid solution strengthening and grain strengthening. Moreover, unlike the other alloys, shear bands were observed only in the fracture of the Ti-5Mo-4Fe alloy, which was attributed to differences in texture and microstructure.

• Laser Solutions
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• v.7 no.2
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• pp.1-10
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• 2004

This work was attempted to join SCP sheet and STS304 sheet by using Nd:YAC laser beam. SCP sheet has good formability and low cost, while STS304 has excellent corrosion resistance and mechanical properties in high temp. In this experiment, butt joint type was used to develop the tailored blank welding for dissimilar steel. Sheets which have different thermal properties. Computer simulation was conducted to obtain the off-set position for efficient welding by considering laser power, scanning speed, focal length and basic properties. The result showed that the optimum thermal distribution was obtained when the laser beam was irradiated at $0.05{\sim}0.1$ mm off-set toward the SCP sheet side. The experiment was conducted based on the result of computer simulation to show the same optimum conditions. Optimum conditions were 3KW in laser beam power, 6m/min in scanning speed, -0.5mm in focal position, 0.1mm off-set toward SCP. Microhardness test, tensile test, bulge test, optical microscopy, EDS, and XRD were performed to observe the microstructure around fusion zone and to evaluate the mechanical properties of optimum conditions, The weld zone had high microhardness values by the formation of the martensitic structure. Tensile test measured the strength of welded region by vertical to strain direction and the elongation of welded region by parallel to strain direction. Bulge test showed $52\%$ formability of the original materials. Bead shape, grain size, and martensitic structure were observed by the optical microscopy in the weld zone. Detailed results of EDS, XRD confirmed that the welded region was connected of martensitic structure.

• Laser Solutions
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• v.1 no.1
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• pp.4-10
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• 1998

A basic research for tailored blank welding between mild steel and Zn-coated steel was carried out with $CO_2$ laser beam. The materials used in this work were low carbon steel sheet with a thickness of 1.2mm and Zn-coated steel sheet with the same thickness and 6.3$\mu$m Zn coating. Experiments were carried out by applying the Taguchi method in order to obtain optimized conditions for the application of tailored blank laser welding method in practical manufacturing process. Optical microscopy, XRD, SEM and TEM analysis were performed to observe microstructures and to determine the solidification mode of welded zone. Also mechanical properties were measured by microhardness test tensile test and Erichsen test in order to evaluate the formability of welded specimen. There was no trapped Zn in the fusion zone, and the phases in this region consisted of polygonal ferrite, quasi-polygonal ferrite, banitic ferrite and martensite. The elongation value of welded specimen was more than 80% of that value in the substrate and LDH value was more than 90% of that value in the substrate metal.

• Laser Solutions
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• v.2 no.3
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• pp.42-51
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• 1999

This research was conducted as a fundamental study to apply tailored blank welding technique into automotive production process. The materials used in this study were 2.0mm thickness low carbon steel sheets and 1.2mm Zn-coated low carbon steel sheets. To ensure the reproducibility and to consider various factors, experiments were. conducted by applying Taguchi experimental method with 6 factors. Every welding process was repeated 3 times to offset the effect of uncontrolled factors. Elongation and LDH(Limited Dome Height)were measured to evaluate formability of specimens and Optical microscopy, XRD, SEM, and EDS analysis were performed to observe the microstructures and to determine the solidification mode in the weld. The elongation of specimen welded with optimum condition was 83% of base metal, and LDH was 84% of base metal. In case of laser treated specimen where Zn coating was removed, elongation was 85% of base metal, and LDH was 85% of base metal. In fusion zone, phases were consisted of quasi-polygonal ferrite, banitic ferrite, and martensite.

• Journal of the Korean Society for Precision Engineering
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• v.24 no.4 s.193
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• pp.57-67
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• 2007

Laser surface hardening technologies have been used to improve characteristics of wear and to enhance the fatigue resistance fur mold parts. The objective of this research work is to investigate the influence of the process parameters, such as power of laser and defocused spot position, on the characteristics of laser surface hardening for the case of SKD61 steel. CW Nd:YAG laser is selected as the heat source. The optical lens with the elliptical profile is designed to obtain a wide surface hardening area with a uniform hardness. From the results of the experiments, it has been shown that the maximum average hardness is approximatly 780 Hv when the power, focal position and the travel of laser are 1,095 W, 0mm and 0.3 m/min, respectively. In samples treated with lower scanning speeds, some small carbide particles appear in the interdendritic regions. This region contains fine martensite and carbide in proportions which depend on the local thermal cycle.

• Korean Journal of Metals and Materials
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• v.46 no.11
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• pp.713-724
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• 2008

The need to lower the weights of automotive vehicle and to improve the safety of cars has resulted in the development of high strength steels such as TRIP(Transformation Induced Plasticity) and DP (Dual Phase) steel. It is well known that the higher strength of steel shows the poorer press formability. Among the high strength steels, DP steel shows several good characteristics such as low yield ratio, high initial n value, high elongation, high bake hardenability and anti-aging property. However, there's a certain limit in application of DP steels to the automotive panel parts because their poor deep drawbility caused by martensite. In this study, the effect of alloying elements on the deep drawability and recrystallization texture in TS 440MPa grade DP steel with 0.015~0.02% carbon has been investigated on the base of SEM, TEM, XRD and EBSD analysis.