• Applied Microscopy
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• v.48 no.4
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• pp.117-121
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• 2018

The multiple length scale analysis of previously designed Fe-Mn-Al-C based low-density model alloys reveals the difference in ordered ${\kappa}-carbide$, $(Fe,Mn)_3AlC_x$, between Fe-25Mn-16Al-5.2C (at%) alloy and Fe-3Mn-10Al-1.2C (at%) alloy. For the former alloy composition consisting of fully austenite grains, ${\kappa}-carbide$ showed majorly cuboidal and minorly pancake morphology and its chemical composition was not changed through aging for 24 h and 168 h at $600^{\circ}C$. Meanwhile, for the isothermally annealed ferritic alloy system for 1 hr at 500 and $600^{\circ}C$, the dramatic change in the chemical composition of needle-shape ${\kappa}-carbide$, $(Fe,Mn)_3(Fe,Al)C_x$, was found. Here we address that the compositional fluctuations in the vicinity of the carbides are significantly controlled by abutting phase, either austenite or ferrite. Namely, the cooperative ordering of carbon and Al is an important factor contributing to carbide formation in the high-Mn and high-Al alloyed austenitic steel, while the carbon and Mn for the low-Mn and high Al alloyed ferritic steel.

• Nuclear Engineering and Technology
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• v.45 no.7
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• pp.929-940
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• 2013

Environmental fatigue of the metallic components in light water reactors has been the subject of extensive research and regulatory interest in Korea and abroad. Especially, it was one of the key domestic issues for the license renewal of operating reactors and licensing of advanced reactors during the early 2000s. To deal with the environmental fatigue issue domestically, a systematic test program has been initiated and is still underway. The materials tested were SA508 Gr.1a low alloy steels, 316LN stainless steels, cast stainless steels, and an Alloy 690 and 52M weld. Through tests and subsequent analysis, the mechanisms of reduced low cycle fatigue life have been investigated for those alloys. In addition, the effects of temperature, dissolved oxygen level, and dissolved hydrogen level on low cycle fatigue behaviors have been investigated. In this paper, the test results and key analysis results are briefly summarized. Finally, an on-going test program for hot-bending of 347 stainless steel is introduced.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.14 no.2
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• pp.59-68
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• 2018

This study compares true stress-true strain curves obtained by tensile tests of various piping materials with bi-linear stress-strain approximation suggested in the JSME Code Case(CC) Draft, a guideline for piping seismic inelastic response analysis. Based on the comparisons, the reliability of the bi-linear approximation is evaluated. It is found that bi-linear stress-strain curve of TP316 stainless steel is in good agreement with its true stress-true strain curve. However, Bi-linear stress-strain curves of TP304 stainless steel and carbon steels determined by the approximation cannot appropriately estimate their stress-strain behavior. Accordingly new bi-linear approximations for carbon steels and low-alloy steels are proposed. The proposed bi-linear approximations for carbon and low-alloy steels, which include the temperature effect on strength and hardening of material, estimate their stress-strain behavior reasonably well.

• Corrosion Science and Technology
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• v.2 no.2
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• pp.75-81
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• 2003

Chromium, molybdenum. and nitrogen are very important alloying elements in stainless steels and its effect was approved in pitting resistance equivalent (PRE) equations and many experimental results. However, Cr can improve the corrosion resistance, but facilitate the formation of sigma phase. Also. Mo has the same effect in stainless steels. If Cr and Mo are added at high amount to increase the corrosion resistance of stainless steel, corrosion resistance in annealed alloys can be improved, but in case of welding or aging heat treatment. its resistance will be drastically decreased. In this work, increasing Cr and N contents but decreasing Mo than the commercial alloys made the experimental alloys. Typical alloys are 25Cr-4.5Mo-0.43N alloy, 27Cr-4.7Mo-0.4N alloy, 27Cr-5.3Mo-0.25N alloy, 32Cr-2.6Mo-0.36N alloy. After annealing and aging heat treatment, microstructures, anodic polarization test, and pitting corrosion test were performed. Annealed alloys showed $100^{\circ}C$ of CPT and aged alloys showed the different tendency depending upon Cr and Mo contents(SFI)

• Korean Journal of Materials Research
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• v.23 no.9
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• pp.525-530
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• 2013

This study investigated the continuous cooling transformation, microstructure, and mechanical properties of highstrength low-alloy steels containing B and Cu. Continuous cooling transformation diagrams under non-deformed and deformed conditions were constructed by means of dilatometry, metallographic methods, and hardness data. Based on the continuous cooling transformation behaviors, six kinds of steel specimens with different B and Cu contents were fabricated by a thermomechanical control process comprising controlled rolling and accelerated cooling. Then, tensile and Charpy impact tests were conducted to examine the correlation of the microstructure with mechanical properties. Deformation in the austenite region promoted the formation of quasi-polygonal ferrite and granular bainite with a significant increase in transformation start temperatures. The mechanical test results indicate that the B-added steel specimens had higher strength and lower upper-shelf energy than the B-free steel specimens without deterioration in low-temperature toughness because their microstructures were mostly composed of lower bainite and lath martensite with a small amount of degenerate upper bainite. On the other hand, the increase of Cu content from 0.5 wt.% to 1.5 wt.% noticeably increased yield and tensile strengths by 100 MPa without loss of ductility, which may be attributed to the enhanced solid solution hardening and precipitation hardening resulting from veryfine Cu precipitates formed during accelerated cooling.

• Korean Journal of Metals and Materials
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• v.48 no.8
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• pp.749-756
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• 2010

Low carbon steels were oxidized isothermally at 1050 and $1180^{\circ}C$ for 4 hr in air in order to determine the effect of alloying elements Si, S, Cu, Sn, and Ni on oxidation. For oxidation resistance of low carbon steels, the beneficial elements were Si, Cu, and Ni, whereas the harmful elements were S and Sn. The most active alloying element, Si, was scattered inside the oxide scale, at the scale-alloy interface, and as an internal oxide precipitate. The relatively noble elements such as Cu and Ni tended to weakly segregate at the scale-alloy interface. Sulfur and Sn were weakly, uniformly distributed inside the oxide scale. Excessively thick, non-adherent scales containing interconnected pores formed at $1180^{\circ}C$.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.11 no.1
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• pp.33-38
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• 2015

The effects of post weld heat treatment(PWHT) on the mechanical properties of 2.25Cr-1Mo steels were investigated. As the PWHT temperature or holding time increased, the strength of low alloy steels progressively decreased due to softening process. After the conventional PWHT, the strength was larger than the minimum value of materials specification. The Charpy impact energy was hardly affected by the conventional PWHT. The trend of mechanical properties was analyzed in terms of tempering parameter. Most materials replaced from a power plant met the requirements of materials specification except for one heat. Same heat of materials with low impact energy were attributed to the voids formed during casting process.

• Corrosion Science and Technology
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• v.13 no.1
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• pp.1-5
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• 2014

A low carbon steel, Fe-2.25%Cr steel (ASTM T22), and Fe-2.25%Cr-1.6%W steel (ASTM T23) were aluminized by hot dipping into molten Al baths. After hot-dipping, a thin Al-rich topcoat and a thick alloy layer formed on the surface. The topcoat consisted primarily of a thin Al layer that contained a small amount of Fe, whereas the alloy layer consisted of Al-Fe intermetallics such as $Al_5Fe_2$ and AlFe. Cr, Mo, and W in T22 and T23 steels reduced the thickness of the topcoat and the alloy layer, and flattened the reaction front of the aluminized layer, when compared to the low carbon steel.

• Journal of the Korean Society for Heat Treatment
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• v.31 no.1
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• pp.1-5
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• 2018

This work demonstrated the application of an artificial neural network model for predicting the Jominy hardness curve by considering 13 alloying elements in low alloy steels. End-quench Jominy tests were carried out according to ASTM A255 standard method for 1197 samples. The hardness values of Jominy sample were measured at different points from the quenched end. The developed artificial neural network model predicted the Jominy curve with high accuracy ($R^2=0.9969$ for training and $R^2=0.9956$ for verification). In addition, the model was used to investigate the average sensitivity of input variables to hardness change.

• Corrosion Science and Technology
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• v.6 no.4
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• pp.164-169
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• 2007

Hydrogen induced cracking (HIC) was studied phenomenologically and the effect of microstructure on HIC was discussed for the steels having two different levels of nonmetallic inclusions. Steels having different microstructures were produced by thermomechanically controlled processes (TMCP) from two different heats which had the different level of nonmetallic inclusions. Ferrite/pearlite (F/P), ferrite/acicular ferrite (F/AF), ferrite/bainite (F/B) were three representative microstructures for all tested steels. For the steels with higher level of inclusions, permissible inclusion level for HIC not to develop was different according to steelmicrostructure. On the contrary, HIC occurred also at the martensite/austenite (M/A) constituents regardless of steel microstructure when they accumulated to a certain degree. It was proved that M/A constituents were easily embrittled by hydrogen atoms. Steels having F/AF is resistant to HIC at a given actual service condition since they covers a wide range of diffusible hydrogen content without developing HIC.