• Title/Summary/Keyword: liquid-phase

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Studies on the Deodorization in the Nightsoil Treatment Plant with liquid Phase Catalytic Oxidation Method by Utilization of Fe-EDTA (Fe-EDTA계 액상촉매 산화법에 의한 분뇨처리장 악취제거에 관한 연구)

  • 이인화
    • Journal of Environmental Science International
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    • v.1 no.2
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    • pp.105.1-113
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    • 1992
  • The present study was performed to develop the removal system of the offensive gases, including hydrogen sulfide of acid gas, ammonia or amice of base gas, from the nightsoil treatment plant. In order to remove the offensive gases, the Fe-EDTA system liquid phase catalytic oxidation method with the bubble lift column reactor was employed. From the results obtained, it was confirmed that the offensive gases can be deodorized simultaneously and also hydrogen sulfide of acid gas, ammonia of base gas completely removed at pH 6.45. In addition, as input gases feed rate the efficiency of acid gas did not change but the efficiency of base gases decreased to approximately 90 % at pH 6, 0. From the result of particle size analyzer, it was found that the particle sizes including sulfur and other impurites grew up to $21{\mu}m$ over 72hour reaction time.

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Magnetic Properties of La-doped YIG films prepared by LPE(Liquid Phase Epitaxy). (LPE 성장법으로 성장시킨 La 을 첨가한 YIG 막의 자성특성)

  • 김동영;한진우;김명수;이상석
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • 2000.11a
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    • pp.89-92
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    • 2000
  • Liquid Phase Epitaxy 법을 이용하여 La이 첨가된 YIG(Yitrium Ion Garnet)막을 성장시켰다. X선 회절 분석을 이용하여 La의 첨가량을 변화시키며 제조된 막의 격자상수를 조사한 결과, La의 첨가량이 증가함에 따라 성장된 막의 격자상수도 증가하였으며 Y/La이 20인 경우, 막의 격자상수가 기판으로 사용한 GGG의 격자상수와 일치하였다. VSM(Vibration Sample Magnetometer)를 이용하여 구한 막의 포화자화 값은 La의 첨가량과 관계없이 순수한 YIG의 경우와 같은 값인 1750정도로 거의 일정하였다. FMR(FerroMagnetic Resonance) 측정장치를 이용한 막의 강자성 공명선폭을 측정결과 막의 공명선폭은 La의 첨가량과 관계없이 모든 경우에 순수한 YIG보다 감소하였다. 실험범위내의 La의 첨가에 대해서 기판과의 격자불일치가 순수한 YIG의 경우보다 감소하기 때문이다. La의 첨가량이 많은 조건에서 성장시킨 막은 공명선폭이 크고 두께의 증가에 따라서 선폭이 증가하였으며, YLa가 20과 30일 때 성장시킨 막에서는 공명선폭의 절대값도 작고 두께에 따른 공명선폭의 변화도 관찰되지 않았다.

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Sintering Behavior of 2xxx Series Al alloys with Variation of Sintering Temperature (2xxx Al 합금계 혼합분말의 소결온도에 따른 소결거동)

  • 민경호;김대건;장시영;임태환;김영도
    • Journal of Powder Materials
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    • v.10 no.1
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    • pp.40-45
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    • 2003
  • Sintering behavior of 2xxx series Al alloy was investigated to obtain full densification and sound microstructure. The commercial 2xxx series Al alloy powder. AMB2712, was used as a starting powder. The mixing powder was characterized by using particle size analyzer, SEM and XRD. The optimum compacting pressure was 200 MPa, which was the starting point of the "homogeneous deformation" stage. The powder compacts were sintered at $550~630^{\circ}C$ after burn-off process at $400^{\circ}C$. Swelling phenomenon caused by transient liquid phase sintering was observed below $590^{\circ}C$ of sintering temperature. At $610^{\circ}C$, sintering density was increased by effect of remained liquid phase. Further densification was not observed above $610^{\circ}C$. Therefore, it was determined that the optimum sintering temperature of AMB2712 powder was $610^{\circ}C$.}C$.

Synthesis of Nano-sized Tungsten Carbide - Cobalt Powder by Liquid Phase Method of Tungstate (텅스텐염의 액상법을 통한 초미립 WC-Co 분말의 합성)

  • Kim, Jong-Hoon;Park, Yong-Ho;Ha, Gook-Hyun
    • Journal of Powder Materials
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    • v.18 no.4
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    • pp.332-339
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    • 2011
  • Cemented tungsten carbide has been used in cutting tools and die materials, and is an important industrial material. When the particle size is reduced to ultrafine, the hardness and other mechanical properties are improved remarkably. Ultrafine cemented carbide with high toughness and hardness is now widely used. The objective of this study is synthesis of nanostructured WC-Co powders by liquid phase method of tungstate. The precursor powders were obtained by freezen-drying of aqueous solution of soluble salts, such as ammonium metatungstate, cobalt nitrate. the final compositions were WC-10Co. In the case of liquid phase method, it can be observed synthesis of WC-10Co. The properties of powder produced at various temperature, were estimated from the SEM, BET and C/S analyser.

Possible Strategies for Microstructure Control of Liquid-Phase-Sintered Silicon Carbide Ceramics

  • Chun, Yong-Seong;Kim, Young-Wook
    • Journal of the Korean Ceramic Society
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    • v.42 no.8 s.279
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    • pp.542-547
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    • 2005
  • Keys to the attainment of tailored properties in SiC ceramics are microstructure control and judicious selection of the sintering additives. In this study, three different strategies for controlling microstructure of liquid-phase-sintered SiC ceramics (LPS-SiC) have been suggested: control of the initial $\alpha-SiC$ content in the starting powder, a seeding technique, and a post-sintering heat treatment. The strategies suggested offer substantial flexibility for producing toughened SiC ceramics whereby grain size, grain size distribution, and aspect ratio can be effectively controlled. The present results suggest that the proposed strategies are suitable for the manufacture of toughened SiC ceramics with improved toughness.

LCD with Tunable Viewing Angle by Thermal Modulation of Optical Layer

  • Gwag, Jin-Seog;Lee, You-Jin;Han, In-Young;Yu, Chang-Jae;Kim, Jae-Hoon
    • Journal of Information Display
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    • v.10 no.1
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    • pp.19-23
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    • 2009
  • In this paper, we review the proposed liquid crystal display (LCD) with a tunable viewing angle consisting of a conventional liquid crystal display (LCD) panel and a thermally variable retardation layer (TVRL) characterized by uniformly aligned LC film with transparent indium-tin-oxide electrodes for Joule heating. In the TVRL, nematic phase is transitioned into isotropic by Joule heating. The numerical calculation showed that the intrinsic wide viewing angle was achieved at the isotropic phase of the TVRL by Joule heating, whereas the narrow viewing angle was obtained at the nematic phase of the TVRL. The simulated and experimental results of the proposed LCD show continuous and symmetrical viewing angle characteristics by tuning the retardation of TVRL using Joule heating. The structure of the viewing angle control proposed here is adoptable to all LCD modes with wide viewing angle characteristics.

Suppression of the abnormal grain growth in the sintering of YIG (YIG 소결시 나타나는 비정상입성 장 현상과 그의 억제)

  • 김동영;한진우;전동석;이상석
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07a
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    • pp.466-469
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    • 2002
  • In the sintering of YIG, abnormal grain growth phenomena was observed. This abnormal grain growth is related to the sintering temperature in this experiment. In the sintering below 145$0^{\circ}C$., the sintered body showed narrow size distribution. However, in the sintering at 145$0^{\circ}C$, a few grains grew rapidly with respect to other grains, and bimodal size distribution was appeared. Liquid phase was not observed far from the abnormally grown large grains, but only near the large grains. This means that the abnormal grain growth was caused by the nonuniform distribution of liquid phase which promote the grains growth. This nonuniform distribution of liquid phase was thought to be due to the nonuniform mixing of the starting materials. This abnormal grain growth was suppressed by enhance the compositional uniformity by multiple calcination.

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Trasient Liquid Phase bonding for Power Semiconductor (전력반도체 패키징을 위한 Transient liquid phase 접합 기술)

  • Roh, Myong-Hoon;Nishikawa, Hiroshi;Jung, Jae Pil;Kim, Wonjoong
    • Journal of the Microelectronics and Packaging Society
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    • v.24 no.1
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    • pp.27-34
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    • 2017
  • Recently, a demand in sustainable green technologies is requiring the lead free bonding for high power module packaging due to the environmental pollution. The Transient-liquid phase (TLP) bonding can be a good alternative to a high Pb-bearing soldering. Basically, TLP bonding is known as the combination of soldering and diffusion bonding. Since the low melting temperature material is fully consumed after TLP bonding, the remelting temperature of joint layer becomes higher than the operating temperature of the power module. Also, TLP bonding is cost-effective process than metal nanopaste bonding such as Ag. In this paper, various TLP bonding techniques for power semiconductor were described.

Mechanical Property of Liquid Phase Diffusion Bonded Joint of Rene80/B/Rene80 (Rene 80/B/Rene 80 액상 확산접합부의 기계적 성질)

  • 정재필;강춘식
    • Journal of Welding and Joining
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    • v.13 no.3
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    • pp.125-133
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    • 1995
  • Rene80 superalloy was liquid phase diffusion bonded by using pure boron (B) as an insert material. As a basic study for the possibility of practical application of this bonding method, hardness and high temperature tensile strength of the bonded joint and metallurgical analysis were investigated. As experimental results, hardness of the bonded joint was homogenized after bonding and the tensile strength at 1144K was obtained to 90% of that of base metal. But there were some problems to be improved also, that means the joint was hardened after bonding due to increase of B content and elongation was much lower than that of base metal. Flat area and (Mo, Cr, W) boride, which should be harmful for bonding strength, were observed on the fractured surface of the tensile tested specimen.

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Transient Simulation of Solid/Liquid Two-Phase Flow in a Stirred Tank (교반기 내부의 고체/액체 다상 유동의 비정상상태 해석)

  • Kim, Chi-Gyeom;Yong, Suk-Jin;Won, Chan-Shik;Hur, Nahm-Keon
    • 한국전산유체공학회:학술대회논문집
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    • 2008.03b
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    • pp.236-239
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    • 2008
  • In the present study, a transient glass particle distribution in a stirred solid/liquid mixer was investigated using computational fluid dynamics(CFD). The flow patterns and solid concentaration distriburion in a solid/liquid mixer formed by pitched paddle and baffles were predicted. The numerical results were compared to experimental data from the available literature. Eulerian multi-phase model was used to investigate the influence of the density of solid particle on the same impeller speed. A good agreement was obtained between the experimental data and simulation results.

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