• Title/Summary/Keyword: liquid recovery

Search Result 775, Processing Time 0.028 seconds

Fine Structure and Physical Properties of Cotton Fibers and their Fabrics Treated with Liquid Ammonia, NaOH, and NaOH/Liquid Ammonia (액체암모니아, 수산화나트륨, 수산화나트륨/액체암모니아 처리한 면의 미세구조 및 물성)

  • 배소영;이문철;김홍성;이영희;김경환
    • Textile Coloration and Finishing
    • /
    • v.6 no.2
    • /
    • pp.47-54
    • /
    • 1994
  • Cotton fiber, NaOH-mercerized cotton fiber, cotton fabric, and NaOH-mercerized cotton fabric have been treated by liquid ammonia at -33.4$^{\circ}C$. The fine structures, bending properties, tensile strengthes, shrinkages for laundering, and wrinkle recoveries were studied. The treatment of cottons with liquid ammonia brought about the transition of crystal lattice ; transforming cellulose I crystal of original cotton to cellulose I and III crystal, and cellulose II crystal of mercerized cotton to cellulose II and III crystals. The degree of crystallinities were decreased in the order of liquid ammonia>NaOH/liquid ammonia>NaOH-treated cotton. However moisture regain and water absorbency for liquid ammonia-treated cotton were lower than that of NaOH-treated cotton because of a difference in swelling actions of the agents. It seems caused by intermicrofibrillar pores produced in swelling processes. The bending rigidity and bending hysteresis were decreased remarkly by liquid ammonia treatment. Therefore softness and dimensional stability were improved. The liquid amminia and NaOH/liquid ammonia-treated cottons moreover show excellent properties in tensile strength, anti-shrinkage for laundering, and wrinkle recovery.

  • PDF

Effects of Reaction Conditions on the Performance of Catalytic Pyrolysis of LDPE in a Semi-Batch Reactor (LDPE 반회분식 촉매열분해에서 조업조건이 반응 특성에 미치는 영향)

  • Na, Jeong-Geol;Leem, Chel-Hyen;Choi, Hwi-Kyoung;Chung, Soo-Hyun
    • 한국신재생에너지학회:학술대회논문집
    • /
    • 2006.11a
    • /
    • pp.79-82
    • /
    • 2006
  • Fueled by ballooning oil prices, waste plastics are now regarded as being cheap and abundant renewable sources, removing their stigma of dirty wastes Catalytic pryolysis of plastics in liquid phase allows recovery of light fuel oil as well as green treatment of polymerics wastes, and therefore significant efforts have been devoted to this research field. In this study, catalytic Pyrolysis of LDPE was carl ied out in semi-batch reactor which equipped a unit of separation and recirculation. The effect of react ion conditions were examined by analyzing liquid oil yield and carbon number distribution of products

  • PDF

A Study on the Recovery of Acetonitrile in the Process of Manufacturing Acrylonitrile (아크릴로니트릴 제조공정에서 아세토니트릴 회수에 관한 연구)

  • 박동원;최성욱;김영일
    • Resources Recycling
    • /
    • v.8 no.3
    • /
    • pp.31-36
    • /
    • 1999
  • In the process of manufacturing acrylonitrile, azeotrope of water-acetonitrile is formed as by-product. To1uene-ethylacetate mixture was selected as solvent to determine the liquid-liquid equilibria for to1uene(l)-water(2)-acetomtrile(3)-ethyjacetate(4) system. The experimental he-line data were correlated with the UNIFAC model. The distribution and selectivity for quaternary system was also studied.

  • PDF

A Study on the Simulation of Toluene Recovery Process using Sulfolane as a Solvent (Sulfolane 용매를 이용한 톨루엔 회수공정의 모사에 관한 연구)

  • Cho, Jungho
    • Korean Chemical Engineering Research
    • /
    • v.44 no.2
    • /
    • pp.129-135
    • /
    • 2006
  • In this study, computer modeling and simulation works were performed to obtain nearly pure toluene product from toluene containing non-aromatic compounds using sulfolane as a solvent through an extractive distillation process. NRTL liquid activity coefficient model was adopted for phase equilibrium calculations and Aspen Plus release 12.1, a commercial process simulator, was used to simulate the extractive distillation process. In this study, it was concluded that the toluene product with a purity of 99.8 percent by weight and a recovery of 99.65 percent was obtained through an extractive distillation process.

Effects of Gas Injection on the Recovery of Copper Powder from Industrial Waste Water in Fluidized - Bed Electrolytic Reactors (유동층 전극반응기에서 기체의 유입이 산업폐수로부터 동입자의 회수에 미치는 영향)

  • Song, Pyung-Seob;Son, Sung-Mo;Kang, Yong;Kim, Seung-Jai;Kim, Sang Done
    • Applied Chemistry for Engineering
    • /
    • v.16 no.4
    • /
    • pp.485-490
    • /
    • 2005
  • Effects of gas injectino on the copper recovery form industrial waste water in a fluidized-bed electrolytic reactor were investigated. Effects of gas injection on the individual phase holdup and efficiency of copper recovery for given operating variables such as liquid and gas velocity (0.1~0.4 cm/s), current density ($2.0{\sim}3.5A/dm^2$) and amount of fluidized solid particles (1.0~4.0 wt%) were examined. The solid particle, whose diameter and swelling density were 0.5 mm and $1100kg/m^3$, respectively, was made of polystylene and divinyl benzene. It was found that the holdup of gas and solid phases increased, but that of the liquid phase decreased with increasing velocity of gas injected into the reactor. With increasing gas and/or liquid velocity and increasing amount of fluidized particles is not needed, the rate of copper recovery increased to a maximum value of and subsequently decreased. The recovery rate of copper increased almost linearly with increasing current density in accordance with Faraday's law.

A New Analytical Method for Erythromycin in Fish by Liquid Chromatography/Tandem Mass Spectrometry

  • Park, Mi-Jung;Park, Mi-Seon;Lee, Tae-Seek;Shin, Il-Shik
    • Food Science and Biotechnology
    • /
    • v.17 no.3
    • /
    • pp.508-513
    • /
    • 2008
  • Erythromycin has been used to treat Streptococosis, Edwardsiel1osis, Vibriosis, Bacterial enteritis in the cultured fish. In this study, a rapid and effective erythromycin analysis method with new sample treatment protocol and liquid chromatography/tandem mass spectrometry (LC/MS/MS) system for fish products was developed. For the erythromycin extraction from fish muscle, the solvent mixture composed of 0.2% meta-phosphoric acid and methanol (6:4) showed good recovery rate, and the optimum extraction solvent volume was 20 mL. Erythromycin detection using LC/MS/MS were carried out under electro spray ionization (ESI) positive condition and erythromycin mass value 576.2 and 157.9. And the detection limit of the established method was 0.005 mg/kg in fish products. The recovery rate of the developed method applied to the fish species were as following, olive flounder, $87.6{\pm}5.0%$; black rockfish, $87.2{\pm}6.4%$; eel, $85.2{\pm}4.8%$; and rainbow trout, $86.0{\pm}6.2%$. In the established method in this study, the correlation of coefficient values ($R^2$) of erythromycin calibration curve (n=11) was 0.9998.

Simultaneous Determination of Cysteamine and Cystamine in Cosmetics by Ion-Pairing Reversed-Phase High-Performance Liquid Chromatography

  • Kim, Yejin;Na, Dong Hee
    • Toxicological Research
    • /
    • v.35 no.2
    • /
    • pp.161-165
    • /
    • 2019
  • Cysteamine has been used in cosmetics as an antioxidant, a hair straightening agent, and a hair waving agent. However, recent studies indicate that cysteamine can act as an allergen to hairdressers. The objective of this study was to develop and validate a simple and effective reversed-phase high-performance liquid chromatography (RP-HPLC) method for the measurement of cysteamine and its dimer, cystamine. Sodium 1-heptanesulfonate (NaHpSO) was used as an ion-pairing agent to improve chromatographic performance. Separation was performed on a Gemini C18 column ($250mm{\times}4.6mm$, $5{\mu}m$ particle size) using a mobile phase composed of 85:15 (v/v) 4 mM NaHpSO in 0.1% phosphoric acid:acetonitrile. UV absorbance was monitored at 215 nm. The RP-HPLC method developed in this study was validated for specificity, linearity, limit of detection, limit of quantitation, precision, accuracy, and recovery. Cysteamine and cystamine were chromatographically resolved from other reducing agents such as thioglycolic acid and cysteine. Extraction using water and chloroform resulted in the recovery for cysteamine and cystamine ranging from 100.2-102.7% and 90.6-98.7%, respectively. This validated RP-HPLC method would be useful for quality control and monitoring of cysteamine and cystamine in cosmetics.

Analysis of Cleaning Sponge Ball Recovery Performance According to Vortex Promoter Design Parameters in CTCS for Power Plant (발전소용 CTCS 내 Vortex Promoter 설계 변수에 따른 세척용 스폰지 볼 회수성능 분석)

  • Dawoon Jung;Seungyul Lee;Dongsun Kim;Hyunkyu Suh
    • Journal of ILASS-Korea
    • /
    • v.28 no.3
    • /
    • pp.126-133
    • /
    • 2023
  • This study analyzes the flow characteristics and sponge ball recovery performance in a ball strainer according to vortex promoter design variables through flow-particle analysis based on actual experiments to derive a method for improving the recovery rate of cleaning sponge balls of CTCS applied to existing power plants. Based on the ball strainer in CTCS used in the power plant, the experiment was conducted by changing the design factor of the improved shape. In addition, flow and particle analysis were performed under the same conditions as the experiment to numerically the flow characteristics and recovery rate in the ball strainer according to the design factor of the vortex promoter. As a result of the study, it was confirmed that the recovery performance was improved by about 3% by changing the design height of the Vortex promoter. And when comparing the difference between maximum and minimum recovery rate, it was found that the effect on the recovery performance increased slightly according to the distance condition compared to the vortex promoter design height condition.

Developing Liquid Cooling Garments to Alleviate Heat Strain of Workers in Summer and Exploring Effective Cooling Temperature and Body Regions (여름철 작업자들의 고체온증 예방을 위한 액체냉각복 개발 및 효과적인 냉각온도와 인체 냉각부위 탐색)

  • Jung, Jae-Yeon;Kang, Juho;Seol, Seonhong;Lee, Joo-Young
    • Fashion & Textile Research Journal
    • /
    • v.22 no.2
    • /
    • pp.250-260
    • /
    • 2020
  • The purpose of the present study was to explore the most effective body region and cooling temperature to alleviate heat strain of workers in hot environments. We developed liquid cooling hood, vest, sleeves and socks and applied the water temperatures of 10, 15, 20, and 25℃ through the liquid cooling garments in a hot and humid environment (33℃ air temperature and 70% RH air humidity). A healthy young male participated in a total of 16 experimental trials (four cooling garments × four cooling temperatures) with the following protocol: 10-min rest, 40-min exercise on a treadmill and 10-min recovery. The results showed that rectal temperature, mean skin temperature, and ratings of perceived exertion during exercise; heart rate and diastolic blood pressure during recovery; and total sweat rate were lower for the vest condition than other garment conditions(p < .05). However, there was no differences in mean skin temperature among the four cooling garments when we compared the values converted by covering area(%BSA). When we classified the results by cooling temperature, there were no consistent differences in thermoregulatory and cardiovascular responses among the four temperatures, but 25℃ water temperature was evaluated as being the most ineffective cooling temperature in terms of subjective responses. In conclusion, the results indicated that wearing cooling vest with < 20℃ cooling temperature can alleviate heat strain of workers in hot and humid environments. If the peripheral body regions are cooled with liquid cooling garments, larger cooling area with lower cooling temperature than 10℃ would be effective to reduce heat strain of workers. Further studies with a vaild number of subjects are required.

Indirect Bacterial Effect Enhanced Less Recovery of Neonicotinoids by Improved Activities of White-Rot Fungus Phlebia brevispora

  • Harry-Asobara, Joy L.;Kamei, Ichiro
    • Journal of Microbiology and Biotechnology
    • /
    • v.29 no.5
    • /
    • pp.809-812
    • /
    • 2019
  • Bacterial strains that improve mycelial morphology and growth of white-rot fungi in liquid medium could enhance the impact of white-rot fungi towards lesser recovery of neonicotinoids when cocultured. This was demonstrated by the recovery of clothianidin and acetamiprid from cocultures of the white-rot fungus Phlebia brevispora strains with two mycelial-growth-promoting bacteria, Enterobacter sp. TN3W-14 and Pseudomonas sp. TN3W-8. Clothianidin recovery from cocultures of white-rot fungi and bacteria was over 40% lower than that from axenic microbial cultures and mixed-bacterial cultures. About 20% less acetamiprid was equally recovered from both TMIC33929+TN3W-14 cocultures and mixed-bacterial cultures than from axenic fungal and bacterial cultures.