• 제목/요약/키워드: limit of detection

검색결과 2,422건 처리시간 0.034초

GC/MS/MS를 이용한 105종의 잔류농약 분석에 관한 연구 (Determination of 105 pesticide residues by GC/MS/MS)

  • 김우성;도정아;이희정;이주영;양승주;이선희
    • 분석과학
    • /
    • 제23권4호
    • /
    • pp.395-404
    • /
    • 2010
  • 레몬과 콩 그리고 채소류에서 105개의 잔류농약을 다종 다성분 분석법으로 GC/MS/MS 분석하였다. 각 시료로부터 acetonitrile로 1차 추출하고 NaCl 15 g을 첨가한 다음 액-액 분배하였으며, Florisil 고체상(SPE) Cartridge로 정제하여 분석하였다. 레몬과 콩에서의 105개 농약의 회수율은 azinphos-methyl, famoxadone, fenamidone, flufenoxuron, triadimefon을 제외한 모든 농약에서 우수한 것으로 나타났는데 레몬에서 71.1~126.0%, 콩에서는 72.5~124.5% 였다. 또한 레몬에서의 검출한계와 정량한계는 각각 0.001~150 ng/mL와 0.004~500 ng/mL으로 확인되었다.

공업용 순 티타늄의 피로거동에서 정류균열에 관한 연구 (A Study on Non-propagating Crack in Fatigue Behavior of Pure Titanium)

  • 김동열;김진학;김민건
    • 대한기계학회논문집A
    • /
    • 제24권4호
    • /
    • pp.1001-1006
    • /
    • 2000
  • To verify the existing theory, non-propagating crack(NPC) does not exist in Ti which fulfills the good conditions for being of NPC, NPC detection in Ti was tried out. Also, the conception of fatigue limit in Ti and a main cause for NPC being were inquired. NPC was detected in both sharp notch root ( $\rho$=0.02mm) and micro pit (diameter = 0.25mm) which held fast to the end under stressing of fatigue limit. Therefore, the existing theory was identified as mistake. But, NPC can not be detected in smooth specimen. This fact would be due to the presumption that NPC is very small or crack does not initiate in smooth specimen. Anyway, the fatigue limit of Ti does not correspond to critical stress of crack initiation but correspond to critical stress of NPC growth. Measurement on the COD of NPC in Ti showed that the crack tip was closed even under the peak stress level at fatigue limit. But, after stress relieving annealing crack tip was opened. Consequently, compressive residual stress which is induced around the crack tip is considered to be the factor causing the NPC being.

고정형 임베디드 감시 카메라 시스템을 위한 다중 배경모델기반 객체검출 (Multiple-Background Model-Based Object Detection for Fixed-Embedded Surveillance System)

  • 박수인;김민영
    • 제어로봇시스템학회논문지
    • /
    • 제21권11호
    • /
    • pp.989-995
    • /
    • 2015
  • Due to the recent increase of the importance and demand of security services, the importance of a surveillance monitor system that makes an automatic security system possible is increasing. As the market for surveillance monitor systems is growing, price competitiveness is becoming important. As a result of this trend, surveillance monitor systems based on an embedded system are widely used. In this paper, an object detection algorithm based on an embedded system for a surveillance monitor system is introduced. To apply the object detection algorithm to the embedded system, the most important issue is the efficient use of resources, such as memory and processors. Therefore, designing an appropriate algorithm considering the limit of resources is required. The proposed algorithm uses two background models; therefore, the embedded system is designed to have two independent processors. One processor checks the sub-background models for if there are any changes with high update frequency, and another processor makes the main background model, which is used for object detection. In this way, a background model will be made with images that have no objects to detect and improve the object detection performance. The object detection algorithm utilizes one-dimensional histogram distribution, which makes the detection faster. The proposed object detection algorithm works fast and accurately even in a low-priced embedded system.

적외선법을 이용한 콘크리트 공동의 적용한계에 관한 기초적 연구 (Fundamental Study on the Limit of Thermographic Survey Applied to Detection of Void in Concrete)

  • 권오현
    • 한국콘크리트학회:학술대회논문집
    • /
    • 한국콘크리트학회 1999년도 봄 학술발표회 논문집(I)
    • /
    • pp.799-806
    • /
    • 1999
  • This study describes the results of experiment and numerical analysis for heating image by thermographic method when the size of void in concrete are changed. By comparing analytical solution by finite element method with measured image by thermography, the relationships between the surface temperature which can be confirmed by this method, the size of void and optimum time for detection of void and the difference of temperature are cleared.

  • PDF

Real-Time Voltammetric Assay of Lead Ion in Biological Cell Systems

  • Ly, Suw-Young
    • Toxicological Research
    • /
    • 제25권4호
    • /
    • pp.231-235
    • /
    • 2009
  • Trace lead detection for cyclic voltammetry (CV) and square-wave (SW) stripping voltammetry was performed using mercury immobilized onto a carbon nanotube electrode (HNPE). Using the characteristics of mercury and the catalytic carbon nanotube structure, a modified technique, the $0.45{\mu}g/l$ detection limit of lead ion was attained. The developed method can be applied to pond water, fish tissue, plant tissue, and in vivo direct assay.

Supervised classification for greenhouse detection by using sharpened SWIR bands of Sentinel-2A satellite imagery

  • Lim, Heechang;Park, Honglyun
    • 한국측량학회지
    • /
    • 제38권5호
    • /
    • pp.435-441
    • /
    • 2020
  • Sentinel-2A satellite imagery provides VNIR (Visible Near InfraRed) and SWIR (ShortWave InfraRed) wavelength bands, and it is known to be effective for land cover classification, cloud detection, and environmental monitoring. Greenhouse is one of the middle classification classes for land cover map provided by the Ministry of Environment of the Republic of Korea. Since greenhouse is a class that has a lot of changes due to natural disasters such as storm and flood damage, there is a limit to updating the greenhouse at a rapid cycle in the land cover map. In the present study, we utilized Sentinel-2A satellite images that provide both VNIR and SWIR bands for the detection of greenhouse. To utilize Sentinel-2A satellite images for the detection of greenhouse, we produced high-resolution SWIR bands applying to the fusion technique performed in two stages and carried out the detection of greenhouse using SVM (Support Vector Machine) supervised classification technique. In order to analyze the applicability of SWIR bands to greenhouse detection, comparative evaluation was performed using the detection results applying only VNIR bands. As a results of quantitative and qualitative evaluation, the result of detection by additionally applying SWIR bands was found to be superior to the result of applying only VNIR bands.

Nanosecond Gated Raman Spectroscopy for Standoff Detection of Hazardous Materials

  • Chung, Jin Hyuk;Cho, Soo Gyeong
    • Bulletin of the Korean Chemical Society
    • /
    • 제35권12호
    • /
    • pp.3547-3552
    • /
    • 2014
  • Laser Raman spectroscopy is one of the most powerful technologies for standoff detection of hazardous materials including explosives. Supported by recent development of laser and sensitive ICCD camera, the technology can identify trace amount of unknown substances in a distance. Using this concept, we built a standoff detection system, in which nanosecond pulse laser and nanosecond gating ICCD technique were delicately devised to avoid the large background noise which suppressed weak Raman signals from the target sample. In standoff detection of explosives which have large kill radius, one of the most important technical issues is the detection distance from the target. Hence, we focused to increase the detection distance up to 54 m by careful optimization of optics and laser settings. The Raman spectra of hazardous materials observed at the distance of 54 m were fully identifiable. We succeeded to detect and identify eleven hazardous materials of liquid or solid particles, which were either explosives or chemical substances used frequently in chemical plants. We also performed experiments to establish the limit of detection (LOD) of HMX at 10 m, which was estimated to be 6 mg.

Sensitive and Enzyme-Free Pseudomonas aeruginosa Detection and Isolation via DNAzyme Cascade Triggered DNA Tweezer

  • Furong Liu;Jingyuan Xu;Lihua Yang
    • Journal of Microbiology and Biotechnology
    • /
    • 제34권9호
    • /
    • pp.1919-1925
    • /
    • 2024
  • Effective isolation and sensitive detection of Pseudomonas aeruginosa (P. aeruginosa) is crucial for the early diagnosis and prognosis of various diseases, such as urinary tract infections. However, efficient isolation and simultaneous detection of P. aeruginosa remains a huge challenge. Herein, we depict a novel fluorescence assay for sensitive, enzyme-free detection of P. aeruginosa by integrating DNAzyme cascade-induced DNA tweezers and magnetic nanoparticles (MNPs)-based separation. The capture probe@MNPs is capable of accurately identifying target bacteria and transporting the bacteria signal to nucleic acid signals. Based on the DNAzyme cascade-induced DNA tweezers, the nucleic acid signals are extensively amplified, endowing the method with a high sensitivity and a low detection limit of 1 cfu/mL. In addition, the method also exhibits a wide detection of six orders of magnitudes. The proposed method could be extended to other bacteria detection by simply changing the aptamer sequence. Taking the merit of the high sensitivity, greatly minimized detection time (less than 1.5 h), enzyme-free characteristics, and stability, the proposed method could be potentially applied to diagnosing and preventing diseases caused by pathogenic bacteria.

Rapid and Sensitive Detection of Hepatitis C Virus in Clinical Blood Samples Using Reverse Transcriptase Polymerase Spiral Reaction

  • Sun, Wenying;Du, Ying;Li, Xingku;Du, Bo
    • Journal of Microbiology and Biotechnology
    • /
    • 제30권3호
    • /
    • pp.459-468
    • /
    • 2020
  • This study established a new polymerase spiral reaction (PSR) that combines with reverse transcription reactions for HCV detection targeting 5'UTR gene. To avoid cross-contamination of aerosols, an isothermal amplification tube (IAT), as a separate containment control, was used to judge the result. After optimizing the RT-PSR reaction system, its effectiveness and specificity were tested against 15 different virus strains which included 8 that were HCV positive and 7 as non-HCV controls. The results showed that the RT-PSR assay effectively detected all 8 HCV strains, and no false positives were found among the 7 non-HCV strains. The detection limit of our RT-PSR assay is comparable to the real-time RT-PCR, but is more sensitive than the RT-LAMP. The established RT-PSR assay was further evaluated for detection of HCV in clinical blood samples, and the resulting 80.25% detection rate demonstrated better or similar effectiveness compared to the RT-LAMP (79.63%) and real-time RT-PCR (80.25%). Overall, the results showed that the RT-PSR assay offers high specificity and sensitivity for HCV detection with great potential for screening HCV in clinical blood samples.

System Capacity Analysis with the Retransmission Limit on ARQ in a Voice/Data DS-CDMA System

  • Lee, Chiho;Gwangzeen Ko;Kim, Kiseon
    • 대한전자공학회:학술대회논문집
    • /
    • 대한전자공학회 2000년도 ITC-CSCC -1
    • /
    • pp.513-516
    • /
    • 2000
  • In this paper, we investigate the effect of the retransmission limit both the system capacity and the average number of retransmissions in a voice/data DS-CDMA system. Basically, we consider the IS-95 type reverse link of the CDMA system, which supports two kinds of services: a general voice and a packetized data service. ARQ is used for the reliable data transmission. Convolutional code is used for FEC and CRC-CCITT code is used for the error detection in ARQ. The result shows that the number of concurrent data users decreases as we reduce the number of the retransmissions. However, at the same time, we can also reduce the average number of retransmissions. Concluding1y, we can select the retransmission limit so as to reduce large amount of' retransmissions with small sacrifice in the system capacity.

  • PDF