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Optimal Double Heat Treatment Process to Improve the Mechanical Properties of Lightweight AlSiCu Alloy (자동차 경량소재 AlSiCu 합금의 기계적 특성을 개선하기 위한 최적의 이중 열처리공정)

  • Park, Sang-Gyu;Kim, Chung-Seok
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.17 no.3
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    • pp.102-108
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    • 2018
  • The objective of this study is to develop the mechanical properties of an AlSiCu aluminum alloy using the two-step solution heat treatment. The microstructure of the gravity casting specimen represents a typical dendrite structure with a secondary dendrite arm spacing (SDAS) of 40 um. In addition to the Al matrix, a large amount of coarsen eutectic Si phase, $Al_2Cu$ intermetallic phase, and Fe-rich phases is generated. The eutectic Si phases are fragmented and globularized with the solution heat treatment. The $Al_2Cu$ intermetallic phase is also resolutionized into the Al matrix. The $2^{nd}$ solution temperature at $525^{\circ}C$ may be an optimal condition to enhance the mechanical properties of the AlSiCu aluminum alloy.

An Explicit Solution of EM Algorithm in Image Deblurring: Image Restoration without EM iterations (영상흐림보정에서 EM 알고리즘의 일반해: 반복과정을 사용하지 않는 영상복원)

  • Kim, Seung-Gu
    • Communications for Statistical Applications and Methods
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    • v.16 no.3
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    • pp.409-419
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    • 2009
  • In this article, an explicit solution of the EM algorithm for the image deburring is presented. To obtain the restore image from the strictly iterative EM algorithm is quite time-consumed and impractical in particular when the underlying observed image is not small and the number of iterations required to converge is large. The explicit solution provides a quite reasonable restore image although it exploits the approximation in the outside of the valid area of image, and also allows to obtain the effective EM solutions without iteration process in real-time in practice by using the discrete finite Fourier transformation.

Effects of Electrolyte Concentration on Electrochemical Properties of Zinc-Air Batteries (전해질 농도에 따른 아연-공기 전지의 전기화학적 특성)

  • Han, Ji Woo;Jo, Yong Nam
    • Korean Journal of Materials Research
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    • v.29 no.12
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    • pp.798-803
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    • 2019
  • The self-discharge behavior of zinc-air batteries is a critical issue induced by corrosion and hydrogen evolution reaction (HER) of zinc anode. The corrosion reaction and HER can be controlled by a gelling agent and concentration of potassium hydroxide (KOH) solution. Various concentrations of KOH solution and polyacrylic acid have been used for gel electrolyte. The electrolyte solution is prepared with different concentrations of KOH (6 M, 7 M, 8 M, 9 M). Among studied materials, the cell assembled with 6 M KOH gel electrolyte exhibits the highest specific discharge capacity and poor capacity retention. Whereas, 9 M KOH gel electrolyte shows high capacity retention. However, a large amount of hydrogen gas is evolved with 9 M KOH solution. In general, the increase in concentration is related to ionic conductivity. At concentrations above 7 M, the viscosity increases and the conductivity decreases. As a result, compared to other studied materials, 7 M KOH gel electrolyte is suitable for Zn-air batteries because of its higher capacity retention (92.00 %) and specific discharge capacity (351.80 mAh/g) after 6 hr storage.

The Effect of Sample Handling on the Rheological Measurement of Regenerated Silk Fibroin Formic Acid Solution using Parallel Plate Geometry

  • Cho, Hee-Jung;Um, In-Chul
    • International Journal of Industrial Entomology and Biomaterials
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    • v.22 no.1
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    • pp.5-10
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    • 2011
  • The effect of sample handling condition on the rheological measurement of regenerated silk fibroin formic acid solution using parallel plate geometry was investigated. In case of loading method, the loading by pouring sample solution resulted in the best reproducibility of rheological measurement. Loading with spoon showed a high variance of viscosity value at low shear rate region ($0.01{\sim}1sec^{-1}$) while loading with syringe exhibited a low reproducibility of viscosity at high shear region ($1{\sim}100sec^{-1}$) with a disappearance of shear thinning phenomenon. It was revealed that the sample loading with small extra amount lead to the most reproducible result. The sample loading with the exact amount for the measuring plate resulted in a lack of reproducibility of high shear viscosity, while the loading with large extra volume produced a limited consistency of low shear viscosity. It was turned out that 3 min. of waiting time before measurement was the optimum condition for reliable result. When the waiting time was less than 1 min., the low shear viscosity was obtained with a lack of consistency. On the other hand, the sample solution started drying when the waiting time increased up to 5 min.

Phosphate Removal from Aqueous Solution according to Activation Methods of Red Mud (알루미늄 제련 폐기물(Red Mud)의 활성화 방법에 따른 수용상의 인산염 제거특성)

  • Kim, I-Tae;Bae, Woo-keun;Kim, Woo-jeong
    • Journal of Korean Society on Water Environment
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    • v.20 no.5
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    • pp.466-472
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    • 2004
  • Red mud is formed as a waste during bauxite refining known as Bayer's process. Its main constituents are iron, aluminium, sodium and silica. The disposal of large quantities of wasted red mud causes a serious ecological problem. In this study, the red mud wasted from the bauxite refinery was studied for phosphate removal from aqueous solution according to activation methods. The influence of heat treatment, and neutralization with sea water and acid treatment level for the optimum conditions for phosphate removal have been determined. Heat treatment combined with acid treatment is most suitable for the removal of phosphate from aqueous solution. The optimal condition was activated with 1 N HCl solution after heating in $600^{\circ}C$ during 4 hours. Acid and heat treatment causes sodalite compounds which hinder the phosphate adsorption to leach out. The adsorption data obtained followed a first-order rate expression and fitted well with the Freundlich Isotherm well.

Synthesis of Nano-Sized Cu Powder by PVA Solution Method and Thermal Characteristics of Sintered Cu Powder Compacts (PVA 용액법을 통한 나노 Cu 분말합성 및 소결체의 열적 특성)

  • Oh, Bok-Hyun;Ma, Chung-Il;Lee, Sang-Jin
    • Korean Journal of Materials Research
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    • v.30 no.2
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    • pp.93-98
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    • 2020
  • Effective control of the heat generated from electronics and semiconductor devices requires a high thermal conductivity and a low thermal expansion coefficient appropriate for devices or modules. A method of reducing the thermal expansion coefficient of Cu has been suggested wherein a ceramic filler having a low thermal expansion coefficient is applied to Cu, which has high thermal conductivity. In this study, using pressureless sintering rather than costly pressure sintering, a polymer solution synthesis method was used to make nano-sized Cu powder for application to Cu matrix with an AlN filler. Due to the low sinterability, the sintered Cu prepared from commercial Cu powder included large pores inside the sintered bodies. A sintered Cu body with Zn, as a liquid phase sintering agent, was prepared by the polymer solution synthesis method for exclusion of pores, which affect thermal conductivity and thermal expansion. The pressureless sintered Cu bodies including Zn showed higher thermal conductivity (180 W/m·K) and lower thermal expansion coefficient (15.8×10-6/℃) than did the monolithic synthesized Cu sintered body.

Investigation of Demixing Phenomena of a Polymer Solution During the Phase Inversion Process

  • Han, Myeong-Jin;D. Bhattacharyya
    • Proceedings of the Membrane Society of Korea Conference
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    • 1995.04a
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    • pp.11-15
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    • 1995
  • Polysulfone (PS) membranes were prepared by the phase inversion process using water or isopropanol as nonsolvent. The Flory-Huggins theory for a ternary system nonsolvent/solvent/polymer is applied to describe the thermodynamic equilibria of the components. The calculated ternary phase equilibria show that demixing of a PS binary solution with n-methylpyrrolidone (NMP) will be fast in a water coagulation bath and will be delayed in an isopropanol bath. The prepared membranes were characterized by SEM, gas adsorption-desorption measurement, and permeability test. The membrane, which is precipitated by fast demixing in a water bath, has nodular structures in the skin region and includes finger-like cavities in the sublayer. The membrane coagulated by isopropanol has a very dense and thick skin structure, which is formed by delayed demixing. The membrane coagulated by isopropanol showed considerably lower pore volume and surface area compared to that observed with water coagulation method. With dimethylformamide (DMF) as solvent and 2-3 wt% of water, the solution can show the liquid-liquid phase separation due to agglomation of the polymer-lean phase from the homogeneous solution. The membranes, which were coagulated near an equilibrium state, show the large (micron size) round pores in the whole membranes. The pores do not contribute the permeation characteristics.

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Optimisation of a novel trailing edge concept for a high lift device

  • Botha, Jason D.M.;Dala, Laurent;Schaber, S.
    • Advances in aircraft and spacecraft science
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    • v.2 no.3
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    • pp.329-343
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    • 2015
  • This study aimed to observe the effect of a novel concept (referred to as the flap extension) implemented on the leading edge of the flap of a three element high lift device. The high lift device, consisting of a flap, main element and slat is designed around an Airbus research profile for sufficient take off and landing performance of a large commercial aircraft. The concept is realised on the profile and numerically optimised to achieve an optimum geometry. Two different optimisation approaches based on Genetic Algorithm optimisations are used: a zero order approach which makes simplifying assumptions to achieve an optimised solution: as well as a direct approach which employs an optimisation in ANSYS DesignXplorer using RANS calculations. Both methods converge to different optimised solutions due to simplifying assumptions. The solution to the zero order optimisation showed a decreased stall angle and decreased maximum lift coefficient against angle of attack due to early stall onset at the flap. The DesignXplorer optimised solution matched that of the baseline solution very closely. The concept was seen to increase lift locally at the flap for both optimisation methods.

Job Shop Scheduling by Tabu Search Combined with Constraint Satisfaction Technique (Tabu Search와 Constraint Satisfaction Technique를 이용한 Job Shop 일정계획)

  • 윤종준;이화기
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.25 no.2
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    • pp.92-101
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    • 2002
  • The Job Shop Scheduling Problem(JSSP) is concerned with schedule of m different machines and n jobs where each job consists of a chain of operations, each of which needs to be processed during an uninterrupted time period of a given length on a given machine. The purpose of this paper is to develop the efficient heuristic method for solving the minimum makespan problem of the large scale job shop scheduling. The proposed heuristic method is based on a Tabu Search(TS) and on a Constraint Satisfaction Technique(CST). In this paper, ILOG libraries is used to embody the job shop model, and a CST is developed for this model to generate the increased solution. Then, TS is employed to overcome the increased search time of CST on the increased problem size md to refine the next-current solution. Also, this paper presents the new way of finding neighbourhood solution using TS. On applying TS, a new way of finding neighbourhood solution is presented. Computational experiments on well known sets of MT and LA problem instances show that, in several cases, our approach yields better results than the other heuristic procedures discussed In literature.

Electrodeposition of Copper on AZ91 Mg Alloy in Cyanide Solution

  • Nguyen, Van Phuong;Park, Min-Sik;Yim, Chang Dong;You, Bong Sun;Moon, Sungmo
    • Journal of the Korean institute of surface engineering
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    • v.49 no.3
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    • pp.238-244
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    • 2016
  • Copper electrodeposition on AZ91 Mg alloy was studied in views of preferential deposition on ${\alpha}$- or ${\beta}$- phases and how to achieve uniform deposition over the entire surface on ${\alpha}$- and ${\beta}$-phases in a cyanide solution. The inhomogeneous microstructure of AZ91 Mg alloy, particularly ${\alpha}$- and ${\beta}$-phases, was found to result in non-uniform deposition of zincate layer, preferential deposition of zincate on ${\beta}$-phases, which leads to non-uniform growth of copper layer during the following electrodeposition process. The preferential depositions of zincate can be attributed to higher cathodic polarizations on the ${\beta}$-phases. Pin-hole defects in the copper electrodeposit were observed at the center of large size ${\beta}$-phase particles which is ascribed to gas bubbles formed at the ${\beta}$-phases. The activation of AZ91 Mg alloy in hydrofluoric acid solution was used to obtain uniform growth of zincate layer on both the ${\alpha}$- and ${\beta}$-phases. By choosing an optimum activation time, a uniform zincate layer was obtained on the AZ91 Mg alloy surface and thereby uniform growth of copper was obtained in a cyanide copper electroplating solution.