• 제목/요약/키워드: lamellar

검색결과 397건 처리시간 0.024초

용사법에 의해 제작된 금속/세라믹 경사기능 재료의 기계적 특성 (Mechanical Properties of Metal/Ceramic FGM made by Thermal Spraying Method)

  • 김영식;남기우;김현수;오명석;김귀식
    • 동력기계공학회지
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    • 제2권3호
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    • pp.41-48
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    • 1998
  • This study was aimed at development of fabrication process of functionally graded materials(FGM), consisting of metal and ceramic by thermal spraying method. NiCrAIY/$Al_2O_3$ FGM were made by using plasma spraying onto the SS400 carbon steel substrate. And mechanical properties such as microhardness, thermal shock resistance and adhesive strength of the coating layer were investigated. Adhesive strength was evaluated by acoustic emission method. It was resulted that NiCrAIY/$Al_2O_3$ FGM made by thermal spraying method showed excellent thermal shock resistance and adhesive strength compared to the other lamellar structures of sprayed coatings and that AE is useful tool to evaluate the defect of thermal sprayed coating layer.

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Cu 첨가에 따른 Nd-Fe-B strip cast의 미세조직과 자기적 특성의 상관관계 (Effect of Cu Content on Microstructural and Magnetic Properties of a Nd-Fe-B Strip Cast)

  • 박송이;김태훈;이성래;김동환;남궁석;장태석
    • 한국분말재료학회지
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    • 제18권1호
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    • pp.24-28
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    • 2011
  • Effect of Cu content on microstructural and magnetic properties of a $(Nd_{26.06},Dy_{6.51})Fe_{bal.}$ $Cu_xB_{0.97}$(wt.%), (x = 0.2, 0.3, 0.4, 0.5) strip-cast was studied. The average inter-lamellar spacing in the free surface and wheel side of the strip cast increased as the Cu content increases. The grain uniformity, the grain alignment, and (00L) texture of the strip cast increased with Cu contents up to 0.4 wt.%. These microstructural changes were attributed to the decrease of the effective cooling rate of the melted alloy caused by the decrease of the melting temperature of resulting from Cu addition. Coercivity and remanence were increased because of the grain alignment and (00L) texture improvement with Cu contents up to 0.4 wt.%.

식물세포(植物細胞)의 Cytolysomes에 관(關)한 전자현미경적(電子顯微鏡的) 연구(硏究) (Electron microscopy of Cytolysomes in plant cells(Glycine max Merr. and Zea mays L.))

  • 김우갑
    • Applied Microscopy
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    • 제4권1호
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    • pp.25-33
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    • 1974
  • Glycine max Merr., Zea mays L.의 엽육세포와 근단세포에서 cytolysome의 기원과 기능에 관하여 추구하였다. Cytolysomes은 원형질막과 세포질의 소포체에서 유래되는데, 원형질막의 함입으로 다소포체인 것과 환상인 다층막성구조로 분화되는 두가지 기본형이 있고, 또 세포질에서는 무과입성 소포체가 세포질의 일부를 분리시키으로서 세포질분리체로 분화된다. 원형질막과 세포질에서 유래된 이들 구조는 각각 막성구조가 증가되면서 액포내로 유리되고 자식성소화과정을 밟아 퇴화되는것 같다.

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주조 및 불연속 석출물 미세조직을 가지는 Mg-Al 합금의 인장 특성 및 열전도도 (Tensile Properties and Thermal Conductivities of Mg-Al alloy with As-Cast and Discontinuous Precipitates Microstructures)

  • 전중환
    • 열처리공학회지
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    • 제33권5호
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    • pp.219-225
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    • 2020
  • The objective of this study was to investigate the tensile properties and thermal conductivities of Mg9.3%Al alloy in as-cast state and heat-treated state consisting of fully discontinuous precipitates (DPs), respectively. The fully DPs microstructure was obtained by solution treatment at 405℃ for 24 h, followed by furnace cooling to RT. The as-cast alloy showed a partially divorced eutectic β(Mg17Al12) phase particles formed along the α-(Mg) cell boundaries. The DPs had various apparent (α+β) interlamellar spacings, which is related to different transformation temperatures during the furnace cooling. The DPs microstructure exhibited better tensile strength than the as-cast one, resulting from the higher value of elongation in response to its more homogeneous microstructure. It is noticeable that the DPs microstructure had 12.4% higher thermal conductivity in average than the as-cast one between RT and 200℃. The XRD analyses revealed that the lower Al concentration in the α-(Mg) matrix may well be responsible for the better thermal conductivity of the DPs microstructure.

급속응고 및 Stone Mill 공정에 의해 제조된 하이브리드 Al2O3-TiC/Al 복합재료의 미세조직 (Microstructure of the Hybrid Al2O3-TiC/Al Composite by Rapid Solidification and Stone Mill Process.)

  • 김택수;이병택;조성석;천병선
    • 한국분말재료학회지
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    • 제10권1호
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    • pp.15-20
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    • 2003
  • Hybrid $A1_2O_3-TiC$ ceramic particle reinforced 6061 and 5083 Al composite powders were prepared by the combination of twin rolling and stone mill crushing process, followed by consolidating processes of cold compaction, degassing and hot extrusion. The composite bar consists of lamellar structure of ceramic particle rich area and matrix area, in which the hybrid was decomposed into each TiC of about $3-4\mutextrm{m}$ and $AI_2O_3$ particles of about $1-2\mutextrm{m}$ in diameter. It also found that fine $Mg_2Si$ precipitates of about 30 nm were embedded in the matrix, which have grains of about 3 $\mutextrm{m}$. Higher UTS was measured at the 5083 composite bar compared to the conventionally fabricated composite, due to again refinement effect by the rapid solidification. No particle was shown to form in the interface between the matrix and reinforcement, whereas carbon was diffused into the matrix.

The study on stabilization of Retinol-Nanoemulsion using Skin Lipid Matrix(SLM)

  • Cho, Joo Hyun;Lim, Choon Bong;Chai, Hee Gil;Eom, Sang Yong;Kim, Jong Heon;Ji, Hong Geun
    • 대한화장품학회:학술대회논문집
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    • 대한화장품학회 2003년도 IFSCC Conference Proceeding Book I
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    • pp.61-72
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    • 2003
  • In cosmetic area, retinol is prominent ingredient for anti-wrinkle but unstable against light, heat, oxygen and so on. Therefore the stabilization of retinol is required. Here, we capsulated doubly retinol in the SLM(Skin Lipid Matrix) that makes three dimensional lamellar structure similar to skin, after formation of primary liposome (retinol-nanoemulsion). First, we make primary liposome from retinol / hydrogenated lecithin / polysorbate20 / caprylic & capric triglyceride / ethanol / and so on, and the mean diameter to 70 nm, using microfluidizer passed three times at 800 Bar, repeatedly. Then we produce DC-liposome (doubly capsulated-liposome) that was encapsulated primary liposome with SLM made of hydrogenated phosphatidyl choline / caprylic & capric triglyceride / 1, 3-butylene glycol / ceramide3 / cholesterol /etc. We measured for color stability against light and heat with chromameter. As a result of this experiment, we observed DC-liposome was more than from 1.5 to 3 times as stable as general liposome. Livability of retinol has improved from 2 to 6 times when we analyzed it by HPLC. Also, penetration effect of DC-liposome has improved.

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한국산 Incabates (Acari: Oribatida)속의 1 신종 (A New Species of the Genus Incabates Hammer (Acari: Oribatida) from Jeju, Korea)

  • 최성식;김태흥
    • 한국응용곤충학회지
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    • 제41권3호
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    • pp.171-175
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    • 2002
  • 이 논문은 날개응에의 소매응애과(Haplozetidae)에 속하는 신종 제주소매응애(신칭: Incabates barbatus sp.nov.)를 기재한 것이다. 이 신종은 일본에서 기록된 1. major와 매우 닳았으나, 1. major는 가슴등판센털(머리끝털; ro, 지게털, la)과 감각털의 머리가 매끈한 반면 신종은 머리끝털(ro)과 지게털(la)의 중간부분 바깥쪽에 거치들이 나 있고, 감각기 머리 표면에 작은 돌기가 나 있어 거칠다. Incabates속에는 현재까지 신종을 포함하여 모두 9종이 기록되었는데, 이들에 대한 검색표를 작성하였다.

A Molecular Dynamics Simulation on the Self-assembly of ABC Triblock Copolymers.3. Effects of Block Composition in Asymmetric Triblock Copolymers

  • Ko, Min-Jae;Kim, Seung-Hyun;Jo, Won-Ho
    • Fibers and Polymers
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    • 제4권1호
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    • pp.15-19
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    • 2003
  • The self-assembly of asymmetric ABC triblock copolymers in the ordered structure is investigated using an isothermal-isobaric molecular dynamics simulation. Unlike symmetric A BC triblock copolymers, more fascinating mophologies are observed in asymmetric ones because of a larger difference of incompatibility between the components. Various modes of self-assembly in assymmetric ABC triblock copolymers are also observed depending on the block composition. When the composition of block A Is changed from 0.125: to 0.25 at the same $f_B$ : 0.25, the morphological transition from the “cylinder in cylinder” to “cylinders at cylinder” structure is observed in the simulation. In the case of ABC triblocks with $f_B$=0.5, a lamellar-type structure is changed to a cylinder-type structure with increasing the length of block A. When the midblock length increases further to $f_B$=0.625, the “spheres on cylinder” structure is observed in both the $A_{10}$$B_{50}$$C_{20}$ and $A_{20}$$B_{50}$$C_{10}$ triblocks. From these results, the phase diagram of ABC triblock copolymers can be constructed.

Synthesis, Structure, and Thermal Property of Poly(trimethylene terephthalate- co-trimethylene 2,6-naphthalate) Copolymers

  • Jeong, Young-Gyu;Jo, Won-Ho;Lee, Sang-Cheol
    • Fibers and Polymers
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    • 제5권3호
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    • pp.245-251
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    • 2004
  • Poly(trimethylene terephthalate-co-trimethylene 2,6-naphthalate)s (P(TT-co-TN)s) with various copolymer composition were synthesized, and their chain structure, thermal property and crystalline structure were investigated by using $^1$H-NMR spectroscopy, differential scanning calorimetry (DSC) and wide-angle X-ray diffraction (WAXD), respectively. It was found from sequence analysis that all the P(TT-co-TN) copolymers synthesized have a statistical random distribution of TT and TN units. It was also observed from DSC thermograms that the glass transition temperature increases linearly with increasing the TN comonomer content, whereas the melting temperature of copolymer decreases with increasing the corresponding comonomer content in respective PTT- and PTN-based copolymer, showing pseudo-eutectic melting behavior. All the samples melt-crystallized isothermally except for P(TT-co-66 mol % TN) exhibit multiple melting endotherms and clear X-ray diffraction patterns. The multiple melting behavior originates from the dual lamellar population and/or the melting-recrystallization-remelting. The X-ray diffraction patterns are largely divided into two classes depending on the copolymer composition, i.e., PTT and PTN $\beta$-form diffraction patterns, without exhibiting cocrystallization.

Study on High-Temperature Oxidation Behaviors of Plasma-Sprayed TiB2-Co Composite Coatings

  • Fadavi, Milad;Baboukani, Amin Rabiei;Edris, Hossein;Salehi, Mahdi
    • 한국세라믹학회지
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    • 제55권2호
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    • pp.178-184
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    • 2018
  • In the present study, $TiB_2-Co$ composite coatings were thermally sprayed onto the surface of a 304 stainless steel substrate using an atmospheric plasma spray (APS). The phase analysis of the powders and plasma-sprayed coatings was performed using X-ray diffractometry analysis. The microstructures of the coatings were studied by a scanning electron microscope (SEM). The average particle size and flowability of the feedstocks were also measured. Both $TiB_2-32Co$ and $TiB_2-45Co$ (wt.%) coatings possessed typical dense lamellar structures and high-quality adhesion to the substrate. The oxidation behaviors of the coatings were studied at $900^{\circ}C$ in an atmospheric environment. In addition, the cross-sectional images of the oxidized coatings were analyzed by SEM. A thin and well-adhered layer was formed on the surface of both $TiB_2-Co$ coatings, confirming satisfactory high-temperature oxidation resistance. The kinetic curves corresponding to the isothermal oxidation of the coatings illustrated a short transient stage from rapid to slow oxidation during the early portion of the oxidation experiment.