• Title/Summary/Keyword: lab report

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Incorporation of Graphitic Porous Carbon for Synthesis of Composite Carbon Aerogel with Enhanced Electrochemical Performance

  • Singh, Ashish;Kohli, D.K.;Singh, Rashmi;Bhartiya, Sushmita;Singh, M.K.;Karnal, A.K.
    • Journal of Electrochemical Science and Technology
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    • v.12 no.2
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    • pp.204-211
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    • 2021
  • We report, synthesis of high surface area composite carbon aerogel using additive based polymerization technique by incorporating graphitic porous carbon as additive. This additive was separately prepared using sol-gel polymerization of resorcinol-furfuraldehyde in iso-propyl alcohol medium at much above the routine gelation temperature to yield porous carbon (CA-IPA) having graphitic layered morphology. CA-IPA exhibited a unique combination of meso-pore dominated surface area (~ 700 m2/g) and good conductivity of ~ 300 S/m. The composite carbon aerogel (CCA) was synthesized by traditional aqueous medium based resorcinol-formaldehyde gelation with CA-IPA as additive. The presence of CA-IPA favored enhanced meso-porosity as well as contributed to improvement in bulk conductivity. Based on the surface area characteristics, CCA-8 composition having 8% additive was found to be optimum. It showed specific surface area of ~ 2056 m2/g, mesopore area of 827 m2/g and electrical conductivity of 180 S/m. The electrode formed with CCA-8 showed improved electrochemical behavior, with specific capacitance of 148 F/g & ESR < 1 Ω, making it a better choice as super capacitor for energy storage applications.

Study on Perception of Science High School Students about Composing Laboratory Reports by Grade (과학 고등학교 학생들의 실험 보고서 작성에 대한 학년별 인식 조사 연구)

  • Song, Shin-Cheol;Shim, Kew-Cheol
    • Journal of Science Education
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    • v.36 no.2
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    • pp.303-312
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    • 2012
  • This study was to find science high school students' perception about composing laboratory reports by grade. The instrument to survey the perception of them consisted of the perception about making a lab report, and the effect of compositing laboratory reports on the scientific concept understanding and the scientific inquiry ability. Subjects were 260 students of four science high schools in Seoul metropolitan city and Kyounggi province. Most of science high school students had a little positive perception about compositing lab reports, but they had very positive perception about the effects of it on the scientific concept understanding and scientific inquiry ability. There was the significant difference between grades, because the 10th grade students showed more positive perception toward compositing lab reports than the 11th graders(p<.05). The results suggested that different educational approaches and teaching strategies be needed for science high school students considering grades.

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Development of Multi-Frequency Impedance Measurement System for Acupuncture Points and Preliminary Report of Measurement Results (Multi-frequency 자극 방식을 이용한 생체 전기 임피던스 측정 시스템 설계 및 경혈의 전기적 특이성에 대한 고찰)

  • Kim, Soo-Byeong;Lee, Na-Ra;Lee, Seung-Wook;Choi, Jun-Young;Lee, Yong-Heum
    • Korean Journal of Acupuncture
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    • v.29 no.1
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    • pp.71-81
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    • 2012
  • Objectives : The purpose of this paper was to suggest new diagnostic method that was to supersede the estimation of electrical properties at acupoints. Thus, we developed the multi- frequencies bioelectrical impedance measurement system so as to analyze the state of bio-ions in body fluid as body compositions, not skin impedance at acupoint. Methods : At low frequency, the current does not penetrate the cell membrane and at high frequency, the current passes through both intracellular and extracellular fluid because of the decreas of cell membrane impedance. To confirm the reflection of composition in extracellular fluid or intracellular fluid of segment such as acupoint, the system was developed to detect the acupoint potential between adjacent two points in the area of LU3, LU4 and LU9 using 5,50 and 200KHz. Results : The detected acupoint potential has been decreased according to elevation of frequency. As a result of correlation of left/right identical acupoint, we observed a high correlation of three types of acupoint potential at multi-frequencies. Moreover, we observed the low correlation at 5KHz, and that was a significant factor to be considered as unbalanced relationship of identical acupoints. Conclusions : On the basis of meridian theoretical point of view, we may infer the acupoint's physiological composition using the multi-frequencies bioelectrical impedance measurement system.

Effects of Various Post-Treatments of Carbon Nanotube Films for Reliable Field Emission

  • Han, Jae-Hee;Lee, Su-Hong;Berdinsky, Alexander S.;Yoo, Ji-Beom;Park, Chong-Yun;Choi, Jin-Ju;Jung, Tae-Won;Han, In-Taek;Kim, Jong-Min
    • 한국정보디스플레이학회:학술대회논문집
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    • 2005.07b
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    • pp.1462-1465
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    • 2005
  • In this report, the FE characteristics of carbon nanotubes (CNTs) treated using both thermal annealing and mechanical coatings on the as-grown CNTs system atically studied. It was found that in the high temperature annealed samples, CNTs were attacked at its root during annealing due to a small amount of oxygen, and were pulled out of the substrate in places after FE measurements because of the contact resistance. However, for the mechanically coated samples both with spin on glass (SOG) and polymethyl methacrylate (PMMA), CNTs were found to be nearly intact after FE measurements and showed reliable FE characteristics over repeatable voltage scan. The reliability of CNTs during FE could be owing to the strong adhesion of CNTs to the substrate both by SOG and PMMA coatings.

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Stemness and Proliferation of Murine Skin-Derived Precursor Cells under Hypoxic Environment

  • Kim, Hyewon;Park, Sangkyu;Roh, Sangho
    • International Journal of Oral Biology
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    • v.41 no.2
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    • pp.69-74
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    • 2016
  • Skin-derived precursors (SKPs) have potential to differentiate to various cell types including osteoblasts, adipocytes and neurons. SKPs are a candidate for cell-based therapy since they are easily accessible and have multipotency. Most mammalian cells are exposed to a low oxygen environment with 1 to 5% $O_2$ concentration in vivo, while 21% $O_2$ concentration is common in in vitro culture. The difference between in vitro and in vivo $O_2$ concentration may affect to the behavior of cultured cells. In this report, we investigated the effect of hypoxic condition on stemness and proliferation of SKPs. The results indicated that SKPs exposed to hypoxic condition for 5 days showed no change in proliferation. In terms of mRNA expression, hypoxia maintained expression of stemness markers; whereas, oncogenes, such as Klf4 and c-Myc, were downregulated, and the expression of Nestin, related to cancer migration, was also downregulated. Thus, SKPs cultured in hypoxia may reduce the risk of cancer in SKP cell-based therapy.

Study on the structure and morphology of vacuum-evaporated pentacene as a function of the evaporation condition

  • Chang, Jae-Won;Kim, Hoon;Kim, Jai-Kyeong;Lee, Yun-Hi;Oh, Myung-Hwan;Jang, Jin;Ju, Byeong-Kwon
    • 한국정보디스플레이학회:학술대회논문집
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    • 2002.08a
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    • pp.754-758
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    • 2002
  • In order to reach the high quality of organic thin films such as high mobility for device applications, it is strongly desirable to study the growth properties of pentacene film as a function of evaporation condition. Here, we report the structure and morphology of thermal evaporated pentacene thin film by AFM, SEM, and XRD as a function of the evaporation rate and substrate temperature. These results play a key role in determining the electric performance of organic thin film transistor devices.

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Production of Recombinant Humanized Anti-HBsAg Fab Fragment from Pichia pastoris by Fermentation

  • Deng, Ning;Xiang, Junjian;Zhang, Qing;Xiong, Sheng;Chen, Wenyin;Rao, Guirong;Wang, Xunzhang
    • BMB Reports
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    • v.38 no.3
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    • pp.294-299
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    • 2005
  • In this report, we describe the high-yield secretory expression of the recombinant human anti-HBsAg Fab fragment from Pichia pastoris that was achieved by co-integration of the genes encoding the heavy and light chains (both under the control of alcohol oxidase promoter) into the genome of the yeast cells. The fed-batch fermentations were carried out in a 5 L scale. Both chains of the Fab were successfully expressed upon methanol induction. The absorbance ($OD_{600}$) of the broth can reach 350~500 at the end of fed-batch phase. After the induction, the expression level of the recombinant Fab (soluble) reached 420~458 mg/L. The recombinant Fab fragment was purified from the crude culture supernatant by ion exchange chromatography and the purity of the recombinant Fab fragment was over 95%. The affinity activities of the crude fermentation supernatant and the purified Fab were analyzed by indirect ELISA, which showed that the purified recombinant Fab fragment had high affinity activity with hepatitis B surface antigen.

Selective doping of Li-rich layered oxide cathode materials for high-stability rechargeable Li-ion batteries

  • Han, Dongwook;Park, Kwangjin;Park, Jun-Ho;Yun, Dong-Jin;Son, You-Hwan
    • Journal of Industrial and Engineering Chemistry
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    • v.68
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    • pp.180-186
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    • 2018
  • We report the discovery of Li-rich $Li_{1+x}[(Ni_{0.225}Co_{0.15}Mn_{0.625})_{1-y}V_y]O_2$ as a cathode material for rechargeable lithium-ion batteries in which a small amount of tetravalent vanadium ($V^{4+}$) is selectively and completely incorporated into the manganese sites in the lattice structure. The unwanted oxidation of vanadium to form a $V_2O_5-like$ secondary phase during high-temperature crystallization is prevented by uniformly dispersing the vanadium ions in coprecipitated $[(Ni_{0.225}Co_{0.15}Mn_{0.625})_{1-y}V_y](OH)_2$ particles. Upon doping with $V^{4+}$ ions, the initial discharge capacity (>$275mA\;h\;g^{-1}$), capacity retention, and voltage decay characteristics of the Li-rich layered oxides are improved significantly in comparison with those of the conventional undoped counterpart.

Esthetic Rehabilitation of Anterior Dentition by All Ceramic Crowns Using IPS e.max CAD : A Case of Tetracycline Discoloration (전치부 전부도재관을 이용한 테트라싸이클린 착색의 심미보철 회복 증례 (IPS e.max CAD 블록의 이용))

  • Kim, Jae-Hong;Cho, Young-kyu;Kim, Hae-Young
    • Journal of dental hygiene science
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    • v.11 no.4
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    • pp.299-303
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    • 2011
  • The purpose of this case report was to present an example of an esthetic and functional rehabilitation of anterior teeth with tetracycline discoloration and minor morphological abnormality of a 39-year old female. A chairside computer-aided design/computer-aided manufacturing (CAD/CAM) system with CEREC AC was applied for the prosthetic procedure and all ceramic crowns made with lithum disilicate (IPS e.max CAD) restored the esthetic and functional features of sixteen anterior teeth successfully.

Decolorization of methyl red by selected bacteria in industrial waste sludge

  • Yim, Dae-Woo;Lee, Kang-Min
    • 한국생물공학회:학술대회논문집
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    • 2003.10a
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    • pp.398-401
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    • 2003
  • Azo dyes are aromatic compounds characterized by one or more azo bonds $(R_l-N=N-R_2)$. More than 800,000 tons of dyes are produced annually worldwide, of which 60-70% are azo dyes. During manufacturing, an estimated 10-15% is released into the environment. Aside from their negative aesthetic effects, certain azo dyes have been shown to be toxic and, in some cases, these compounds are carcinogenic and mutagenic. To establish biological wastewater treatment of azo dye, it is essential to discover azo dye-degrading microorganisms. In this report, sludge-contaminated with dyes were gathered through wastewater outlets from the industrial regions. The following to separation of bacteria within them, bacteria which decolorize methyl red, a azo dye, were selected and destined.

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