• Title/Summary/Keyword: interfacial energy

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Effects of Sizing Treatment of Carbon Fibers on Mechanical Interfacial Properties of Nylon 6 Matrix Composites (탄소섬유의 사이징처리가 탄소섬유/나일론6 복합재료의 기계적 계면 특성에 미치는 영향)

  • Park, Soo-Jin;Choi, Woong-Ki;Kim, Byung-Joo;Min, Byung-Gak;Bae, Kyong-Min
    • Elastomers and Composites
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    • v.45 no.1
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    • pp.2-6
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    • 2010
  • The sizing treatments of PAN-based carbon fiber surfaces were carried out in order to improve the interfacial adhesion in the carbon fibers/nylon6 composite system. The parameter to characterize the wetting performance and surface free energy of the sized fibers were determined by a contact angle method. The mechanical interfacial properties of the composites were investigated using critical stress intensity factor ($K_{IC}$). The cross-section morphologies of sized CFs/nylon6composites were observed by SEM. As the experimental results, it was observed that silane-based sizing treated carbon fibers showed higher surface free energies than other sizing treatments. In particular, the KIC of the sizing-treated carbon fibers reinforced composites showed higher values than those of untreated carbon fibers-reinforced composites. This result indicated that the increase in the surface free energy of the fibers leads to the improvement of the mechanical interfacial properties of carbon fibers/nylon6 composites.

Effect of BOE Wet Etching on Interfacial Characteristics of Cu-Cu Pattern Direct Bonds for 3D-IC Integrations (3차원 소자 적층을 위한 BOE 습식 식각에 따른 Cu-Cu 패턴 접합 특성 평가)

  • Park, Jong-Myeong;Kim, Su-Hyeong;Kim, Sarah Eun-Kyung;Park, Young-Bae
    • Journal of Welding and Joining
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    • v.30 no.3
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    • pp.26-31
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    • 2012
  • Three-dimensional integrated circuit (3D IC) technology has become increasingly important due to the demand for high system performance and functionality. We have evaluated the effect of Buffered oxide etch (BOE) on the interfacial bonding strength of Cu-Cu pattern direct bonding. X-ray photoelectron spectroscopy (XPS) analysis of Cu surface revealed that Cu surface oxide layer was partially removed by BOE 2min. Two 8-inch Cu pattern wafers were bonded at $400^{\circ}C$ via the thermo-compression method. The interfacial adhesion energy of Cu-Cu bonding was quantitatively measured by the four-point bending method. After BOE 2min wet etching, the measured interfacial adhesion energies of pattern density for 0.06, 0.09, and 0.23 were $4.52J/m^2$, $5.06J/m^2$ and $3.42J/m^2$, respectively, which were lower than $5J/m^2$. Therefore, the effective removal of Cu surface oxide is critical to have reliable bonding quality of Cu pattern direct bonds.

Failure characteristics of combined coal-rock with different interfacial angles

  • Zhao, Tong-Bin;Guo, Wei-Yao;Lu, Cai-Ping;Zhao, Guang-Ming
    • Geomechanics and Engineering
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    • v.11 no.3
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    • pp.345-359
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    • 2016
  • In order to investigate the influence of the interfacial angel on failure characteristics and mechanism of combined coal-rock mass, 35 uniaxial/biaxial compressive simulation tests with 5 different interfacial angels of combined coal-rock samples were conducted by PFC2D software. The following conclusions are drawn: (1) The compressive strength and cohesion decrease with the increase of interfacial angle, which is defined as the angle between structure plane and the exterior normal of maximum principal plane, while the changes of elastic modulus and internal friction angle are not obvious; (2) The impact energy index $K_E$ decreases with the increase of interfacial angle, and the slip failure of the interface can be predicted based on whether the number of acoustic emission (AE) hits has multiple peaks or not; (3) There are four typical failure patterns for combined coal-rock samples including I (V-shaped shear failure of coal), II (single-fracture shear failure of coal), III (shear failure of rock and coal), and IV (slip rupture of interface); and (4) A positive correlation between interfacial angle and interface effect is shown obviously, and the interfacial angle can be divided into weak-influencing scope ($0-15^{\circ}$), moderate-influencing scope ($15-45^{\circ}$), and strong-influencing scope (> $45^{\circ}$), respectively. However, the confining pressure has a certain constraint effect on the interface effect.

Optimum Conditions for Improvement of Mechanical and Interfacial Properties of Thermal Treated Pine/CFRP Composites (열처리된 Pine/탄소섬유 복합재료의 기계적 및 계면물성 향상을 위한 최적 조건)

  • Shin, Pyeong-Su;Kim, Jong-Hyun;Park, Ha-Seung;Baek, Yeong-Min;Kwon, Dong-Jun;Park, Joung-Man
    • Composites Research
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    • v.30 no.4
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    • pp.241-246
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    • 2017
  • The brittle nature in most FRP composites is accompanying other forms of energy absorption mechanisms such as fibre-matrix interface debonding and ply delamination. It could play an important role on the energy absorption capability of composite structures. To solve the brittle nature, the adhesion between pines and composites was studied. Thermal treated pines were attached on carbon fiber reinforced polymer (CFRP) by epoxy adhesives. To find the optimum condition of thermal treatment for pine, two different thermal treatments at 160 and $200^{\circ}C$ were compared to the neat case. To evaluate mechanical and interfacial properties of pines and pine/CFRP composites, tensile, lap shear and Izod test were carried out. The bonding force of pine grains was measured by tensile test at transverse direction and the elastic wave from fracture of pines was analyzed. The mechanical, interfacial properties and bonding force at $160^{\circ}C$ treated pine were highest due to the reinforced effect of pine. However, excessive thermal treatment resulted in the degradation of hemicellulose and leads to the deterioration in mechanical and interfacial properties.

Interfacial Wave Characteristics for Countercurrent Stratified Air-Water Flow in a Horizontal Pipe

  • Chung, Heung-June;Chun, Se-Young;Chung, Moon-Ki;No, Hee-Cheon
    • Nuclear Engineering and Technology
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    • v.28 no.4
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    • pp.379-389
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    • 1996
  • To experimentally investigate the several wave patterns for the horizontal countercurrent stratified air-water flow, a series of systematic experimental studies have been performed. The experiments are carried out in a horizontal pipe with 4m in length and 102mm in inner diameter. The oater and air superficial velocities vary from 0.0004 to 0.0204 and from 0 to 6m/s, respectively. The instantaneous water thickness is measured by parallel-wire conductance probes, and the wave field is recorded by high speed video camera. Also, to evaluate the wave effect on interfacial friction factor, the pressure drop is measured. Statistical data anal)sis is accomplished in order to obtain the fundamental wave parameters such as un amplitude, length and velocity, and spatial growth factor. By using these statistical parameters, the wave regime boundaries can be verified.

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Analysis of Flame Generated Turbulence for a Turbulent Premixed Flame with Zone Conditional Averaging (영역분할조건평균법을 이용한 난류예혼합화염내 난류운동에너지 생성에 관한 연구)

  • Im, Yong Hoon;Huh, Kang Yul
    • Journal of the Korean Society of Combustion
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    • v.8 no.4
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    • pp.15-23
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    • 2003
  • The zone conditional two-fluid equations are derived and validated against DNS database of a premixed turbulent flame. The conditional statistics of major flow variables are investigated to understand the mechanism of flame generated turbulence. The flow field in burned zone shows substantially increased turbulent kinetic energy, which is highly anisotropic due to reaction kinematics across thin f1amelets. The transverse component may be larger than the axial component for a distributed pdf of the flamelet orientation angle, while the opposite occurs due to redistribution of turbulent kinetic energy and flamelet orientation normal to the flow at the end of a flame brush. The major source or sink terms of turbulent kinetic energy are the interfacial transfer by the mean reaction rate and the work terms by fluctuating pressure and velocity on a flame surface. Ad hoc modeling of some interfacial terms may be required for further application of the two-fluid model in turbulent combustion simulations.

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Suppression of interfacial crack for foam core sandwich panel with crack arrester

  • Hirose, Y.;Hojo, M.;Fujiyoshi, A.;Matsubara, G.
    • Advanced Composite Materials
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    • v.16 no.1
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    • pp.11-30
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    • 2007
  • Since delamination often propagates at the interfacial layer between a surface skin and a foam core, a crack arrester is proposed for the suppression of the delamination. The arrester has a semi-cylindrical shape and is arranged in the foam core and is attached to the surface skin. Here, energy release rates and complex stress intensity factors are calculated using finite element analysis. Effects of the arrester size and its elastic moduli on the crack suppressing capability are investigated. Considerable reductions of the energy release rates at the crack tip are achieved as the crack tip approached the leading edge of the crack arrester. Thus, this new concept of a crack arrester may become a promising device to suppress crack initiation and propagation of the foam core sandwich panels.

A Study on the Improvement of Stress Field Analysis in a Domain Composed of Dissimilar Materials

  • Song, Kee-Nam;Lee, Jin-Seok
    • Nuclear Engineering and Technology
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    • v.30 no.3
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    • pp.202-211
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    • 1998
  • Interfacial stresses at two-material interfaces and initial displacement field over the entire domain are obtained by modifying the potential energy functional with a penalty function, which enforces continuity of the stresses at the interface of two materials. Based on the initial displacement field and interfacial stresses, a new methodology to generate a continuous stress field over the entire domain has been proposed by combining the modified projection method of stress-smoothing and Loubignac's iterative method of improving the displacement field. Stress analysis is carried out on two examples made of dissimilar materials : one is a two-material cantilever composed of highly dissimilar materials and the other is a zirconium-lined cladding tube made of slightly dissimilar materials. Results of the analysis show that the proposed method provides an improved continuous stress field over the entire domain, and accurately predicts the nodal stresses at the interface, while the conventional displacement-based finite element method produces significant stress discontinuities at the interface. In addition, the total strain energy evaluated from the improved continuous stress field converges to the exact value in a few iterations.

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