• Title/Summary/Keyword: indenter test

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Analysis of Material Deformation Behavior in Nanoindentation Process by using 3D Finite Element Analysis and its Experimental Verification (3차원 유한요소해석을 이용한 나노인덴테이션 공정에서의 소재거동해석 및 실험적 검증)

  • 이정우;윤성원;강충길
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.1174-1177
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    • 2003
  • In this study, to achieve the optimal conditions for mechanical hyper-fine pattern fabrication process, deformation behavior of the materials during indentation was studied with numerical method by ABAQUS S/W. Polymer (PMMA) and brittle materials (Si, Pyrex glass) were used as specimens, and forming conditions to reduce the elastic recover and pile-up was proposed. The indenter was modeled a 3D rigid surface. Minimum mesh sizes of specimens are 1-10nm. Comparison between the experimental data and numerical result demonstrated that the finite element approach is capable of reproducing the loading-unloading behavior of a nanoindentation test. The result of the investigation will be applied to the fabrication of the hyper-fine pattern.

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A Berkovich Indentation Technique Based on 3D FEA solutions for Material Property Evaluation (3차원 유한요소해에 기초한 Berkovich 압입 물성평가법)

  • Kim, Min-Soo;Hyun, Hong-Chul;Lee, Kyoung-Yoon;Lee, Hyung-Yil
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1-6
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    • 2008
  • Due to the self-similarity of Berkovich and conical indenters, different materials may show the same loaddepth curve for single indentation. In this study, we first compare the load-depth characteristics of conical and Berkovich indenters via finite element method. We also analyze the variation of load-depth curves with angle of Berkovich indenter, indentation parameters, and material properties. With numerical regressions of obtained data, we then propose dual-Berkovich indentation formulae for material property evaluation. The proposed approach provides the values of elastic modulus, yield strength and strain-hardening exponent and corresponding stress-strain curve with an average error of less than 3%. The method is valid for any elastic indenters made of tungsten carbide and diamond for instance.

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A Study on Elastic-Plastic Deformation and 3-D FEA for the Berkovich Nano-Indentation (베르코비치 나노인덴테이션에 대한 3차원 유한요소해석과 탄소성 변형에 관한 연구)

  • Yang Hyeon-Yun;Kim Ji-Soo;Yun Jon-Do;Cho Sang-Bong
    • Journal of the Korean Society for Precision Engineering
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    • v.22 no.10 s.175
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    • pp.167-173
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    • 2005
  • The Berkovich nano-indentation is an indentation test method analyzing mechanical properties of materials such as hardness and elastic modulus. The length scale of the penetration is measured in nanometers. Therefore, this method becomes widely useful for analyzing the mechanical property of thin film which can not be measured before. In this paper, comparing two results of the load-displacement curve obtained by the Berkovich nano-indentation and the 3-D finite element analysis, it was confirmed that the 3-D finite element analysis is useful. The phenomenon of pile-up and sink-in due to material properties was discussed by the finite element analysis.

In-field Evaluation of Structural Strength and Reliability Using Advanced Indentation System (Advanced Indentation System을 이용한 현장에서의 구조강도 건전성 평가)

  • Choi, Yeol;Son, Dong-Il;Jang, Jae-Il;Kwon, Dong-Il
    • Proceedings of the KSR Conference
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    • 2001.05a
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    • pp.230-237
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    • 2001
  • For the structural integrity of large and complex structures such as railway vehicle, the in-field diagnosis of mechanical properties of the structures is needed, and especially, the mechanical characteristics of the weldment must be carefully evaluated. But, conventional standard testing methods having destructive procedures are not applicable to in-field assessment of mechanical property variations within weldment because they needs the limitations of specimen size and geometry. In this paper, to overcome this problems, the advanced indentation technique (AIS) is introduced for simple and non-destructive/in-field testing of weldment of industrial structures. This test measures indentation load-depth curve during indentation and analyzes the mechanical properties related to deformation and fracture. First of all, flow properties such as yield strength, tensile strength and work hardening index can be evaluated through the analysis of the deformation behavior beneath the spherical indenter. Additionally, case studies of advanced indentation techniques are introduced.

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Acoustic Emission and Indentation Fracture Method for the Engineering Ceramics (세라미스 파괴인성평가에 있어서 IF법과 AE)

  • 김부안;문창권
    • Journal of Ocean Engineering and Technology
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    • v.15 no.2
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    • pp.61-65
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    • 2001
  • The fracture toughness of ceramics can be measure by such various methods as DT (double torsion), CN (chevron notch) etc. But, the application of these methods to the engineering ceramics is very difficult because of its very high hardness. So, IF (indentation fracture) method is generally used for the evaluation of fracture toughness of ceramics. The Median crack induced by the sharp Vickers indenter was compared with the detected AE (acoustic emission) signal. On the silicon nitride ceramics, the AE test results agree fairly well with the median crack occurance and growth process. But, on the alumina, very many complicated crack signals were detected besides median crack. It can be considered that the IF methods must be used in limited engineering ceramics materials.

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Estimation of Interfacial Adhesion through the Micromechanical Analysis of Failure Mechanisms in DLC Film

  • Jeong, Jeung-Hyun;Park, Hae-Seok;Ahn, Jeong-Hoon;Dongil Kwon
    • The Korean Journal of Ceramics
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    • v.3 no.2
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    • pp.73-81
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    • 1997
  • In this paper, it is intended to present more reproducible and quantitative method for adhesion assemssement. In scratch test, micromechanical analysis on the stress state beneath the indenter was carried out considering the additional blister field. The interface adhesion was quantified as work of adhesion through Griffith energy approach on the basis of the analyzed stress state. The work of adhesion for DLC film/WC-Co substrate calculated through the proposed analysis shows the identical value regardless of distinctly different critical loads measured with the change of film thickness and scratching speed. On the other hand, uniaxial loading was imposed on DCL film/Al substrate, developing the transverse film cracks perpendicular to loading direction. Since this film cracking behavior depends on the relative magnitude of adhesion strength to film fracture strength, the quantification of adhesion strength was given a trial through the micromechanical analysis of adhesion-dependence of film cracking patterns. The interface shear strength can be quantified from the measurement of strain $\varepsilon$s and crack spacing $\lambda$ at the cessation of film cracking.

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Development of Evaluation Technology of Mechanical Properties Using Continuous Indentation Method (연속압입시험법을 이용한 소재의 기계적 물성 평가기술 연구)

  • Lee, Jeong-Hwan;Ok, Myoung-Ryul;Lee, Yun-Hee;Ahn, Jeong-Hoon;Kwon, Dong-Il
    • Proceedings of the KIEE Conference
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    • 1997.11a
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    • pp.703-708
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    • 1997
  • Continuous indentation test is a very powerful method to monitor the materials reliability since it is very simple, easy and almost non-destructive. It can provide material properties such as elastic modulus, yield strength, work-hardening exponent, etc., than the conventional hardness test. In our study, the true stress-strain curve is derived from the indentation load-depth curve. For this, average indentation strain is defined and the flow stress is obtained from the analysis of the indentation stress field. The residual stress is analyzed from the variation of the indentation behavior with the applied residual stress. And the estimation of fracture characteristic is tried by considering the conventional fracture toughness modeling and the stress/strain state under the spherical indenter.

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A study on Creep of Plate PMMA in Thermal-Nanoindentation Process for Hyperfine pit structure Fabrication (극미세 점 구조체 제작을 위한 열간나노압입 공정에서의 평판형 PMMA의 크립현상에 관한 연구)

  • Lee, E.K.;Jung, Y.N.;Kang, C.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.05a
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    • pp.273-276
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    • 2008
  • Thermoplastic resin takes place stress relaxation and creep according to temperature and time. In room temperature, time dependent deformation (TDD) of polymer was carried out at previous study. In this study, it evaluates time dependent deformation to relate temperature. Nanoscale indents can be used as cells for molecular electronics and drug delivery, slots for integration into nanodevices, and defects for tailoring the structure and properties. Therefore, it is important to control pattern depth for change of indent depth by creep when using Nanoindenter. For evaluating TDD at high temperature, it is occurred thermal-nanoindentation test by changing hold time at maximum load. Temperature is putted at $90^{\circ}C$, hold time at maximum loads are putted at 1, 10, 50, 100, 200, 300 and 500s.

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Plating of Cu layer with the aid of organic film on Si-wafer (유기박막을 이용한 Si기판상의 구리피복층 형성에 관한 연구)

  • Park Ji-hwan;Park So-yeon;Lee Jong-kwon;Song Tae-hwa;Ryoo Kun-kul;Lee Yoon-bae;Lee Mi-Young
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.5 no.5
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    • pp.458-461
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    • 2004
  • In order to improve the adhesion properties of copper, MPS(3-mercaptopropyltrimethoxysilane) organic film were employed. The plasma pretreatment in pure He or $He/O_{2}$ mixed gas environment greatly increased adhesion force. Adhesion force was measured by scratch test with nano indenter. Microstructures and surface roughness were observed with scanning electron microscope(SEM). The characteristics of MPS layer for pretreatment were studied with flourier transform infrared spectroscope(FT-IR) and contact angle tester. The heighest adhesion was achieved in the specimen pretreated with mixed plasma and NPS coating, which was 56mN. Other specimen showed lower value by $20{\%}$ to $30{\%}$. The roughness of substrate was not affected by the bonding strength of copper plating.

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Impact response of ultra-high performance fiber-reinforced concrete filled square double-skin steel tubular columns

  • Li, Jie;Wang, Weiqiang;Wu, Chengqing;Liu, Zhongxian;Wu, Pengtao
    • Steel and Composite Structures
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    • v.42 no.3
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    • pp.325-351
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    • 2022
  • This paper studies the lateral impact behavior of ultra-high performance fiber-reinforced concrete (UHPFRC) filled double-skin steel tubular (UHPFRCFDST) columns. The impact force, midspan deflection, and strain histories were recorded. Based on the test results, the influences of drop height, axial load, concrete type, and steel tube wall thickness on the impact resistance of UHPFRCFDST members were analyzed. LS-DYNA software was used to establish a finite element (FE) model of UHPFRC filled steel tubular members. The failure modes and histories of impact force and midspan deflection of specimens were obtained. The simulation results were compared to the test results, which demonstrated the accuracy of the finite element analysis (FEA) model. Finally, the effects of the steel tube thickness, impact energy, type of concrete and impact indenter shape, and void ratio on the lateral impact performances of the UHPFRCFDST columns were analyzed.