• 한국분말재료학회지
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• 제15권1호
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• pp.1-5
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• 2008

ZnS-$SiO_2$ composite is normally used for sputtering target. In recent years, high sputtering power for higher deposition rate often causes crack formation of the target. Therefore the target material is required that the sintered target material should have high crack resistance, excellent strength and a homogeneous microstructure with high sintered density. In this study, raw ZnS and ZnS-$SiO_2$ powders prepared by a 3-D mixer or high energy ball-milling were successfully densified by spark plasma sintering, the effective densification method of hard-to-sinter materials in a short time. After sintering, the fracture toughness was measured by the indentation fracture (IF) method. Due to the effect of crack deflection by the residual stress occurred by the second phase of fine $SiO_2$, the hardness and fracture toughness reached to 3.031 GPa and $1.014MPa{\cdot}m^{1/2}$, respectively.

• Maxillofacial Plastic and Reconstructive Surgery
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• 제41권
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• pp.54.1-54.3
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• 2019

Background: The presence of septa increases the risk of Schneiderian membrane perforation during sinus lift procedure, and therefore, the chance of graft failure increases. We present a safe method of managing septa and, in particular, overcoming small and palatally located septa. Methods: After the elevation of the flap and the creation of a small bony window positioned anterior to the septum, the Schneiderian membrane is lifted carefully. A thin and narrow osteotome is then placed at the indentation created at the base of the septum, and mobilization of the septum is achieved by gentle malleting. The membrane is again carefully lifted up behind the septum. Results: There was one small membrane perforation case in all 16 cases, and none of these patients showed postoperative complications such as implant failure, infection, or maxillary sinusitis. Conclusions: This technique is useful for overcoming the problem of maxillary sinus septa hindering the sinus floor elevation procedure, leading to fewer complications.

• 한국공간구조학회:학술대회논문집
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• 한국공간구조학회 2008년도 춘계 학술발표회 논문집
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• pp.74-79
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• 2008

본 논문에서는 유한요소법을 이용하여 저속충격을 받는 복합적층판(Graphite/Epoxy)의 충격과도응답을 조사한다. 판의 대처짐을 고려한 von-Karman 이론에 Mindlin의 전단변형 효과와 회전관성 효과를 포함한 비선형 이론을 도입한다. 과도응답의 수렴은 정적만입실험을 통해 얻은 접촉법칙을 사용하며, 다양한 복합적층판의 두께 변화에 따른 접촉력, 변위응답, 변형률 등을 조사하여 비교 분석한다.

• Journal of Mechanical Science and Technology
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• 제15권2호
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• pp.225-231
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• 2001

A mathematical model for the analysis of roll gap phenomena in the strip temper rolling process is described. A new approach to solve the roll indentation and diverging problem in modeling of severe temper rolling cases is obtained by adopting the preliminary displacement principle of two contacted rough bodies to describe the friction behavior in the roll gap. The mechanical peculiarities of the temper rolling process, such as a high friction value with high roughness rolls and a non-circular contact arc, low reduction and non-negligible entry and exit elastic zones as well as central preliminary displacement zone etc., are all taken into account. The deformation of work rolls is calculated with the influence function method and an arbitrary contact are shape is permitted. The strip deformation is modeled by the slab method and the entry and exit elastic deformation zones are included. The preliminary displacement principle is used to determine the boundaries and to calculate the friction of the central preliminary displacement zone. The model is calibrated against the production mill data and installed in the setup computer of a temper rolling mill in POSCO. The validity and precision of the model have been proven through a comparison of the measured roll forces and the predicted ones.

• Macromolecular Research
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• 제14권5호
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• pp.559-564
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• 2006

The improvement of spatial resolution is a fundamental issue in the two-photon, polymerization-based, laser writing. In this study, a voxel tuning method using a radical quencher was proposed to increase the resolution, and the quenching effect according to the amount of radical quencher was experimentally investigated. Employing the proposed method, the lateral resolution of the line patterns was improved almost to 100 nm. However, a shortcoming of the quenching effect was the low mechanical strength of polymerized structures due to their short chain lengths. Nano-indentation tests were conducted to evaluate quantitatively the relationship between mechanical strength and the mixture ratio of the radical quencher into the resins. The elastic modulus was dramatically reduced from an average value of 3.015 to 2.078 GPa when 5 wt% of radical quencher was mixed into the resin. Three-dimensional woodpile structures were fabricated to compare the strength between the resin containing radical quencher and the original resin.

• 한국해양공학회지
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• 제22권3호
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• pp.71-75
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• 2008

This paper illustrates haw $Y_2O_3$ contributes to crack-healing strengths as a function of crack-healing temperature and the additive amount. In investigating mechanical properties, the indentation fracture method is very simple and useful, but careful attention must be paid to the statistical data processing because data may be scattered excessively, especially for brittle materials. To estimate accurate AE signal properties we applied the useful time-frequency method with a discrete wavelet analysis algorithm. In experiments, three kinds of specimens were prepared. After the specimens were indented by a Vickers indentor, they were heat-treated and crack-healed to evaluate bending strength and the AE signal. With higher amounts of the additive powder, as 1, 3, or 5% wt. of $Y_2O_3$, the concentrative tendency of dominant frequency trended toward lower frequency groups. The $Al_2O_3$ ceramic with 3% wt. of $Y_2O_3$ was judged most suitable because it demonstrated superior crack-healing ability and relative concentration on the highest frequency group.

• 대한치과교정학회지
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• 제28권4호
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• pp.641-657
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• 1998

본 연구는 열을 이용한 금속 브라켓의 재생 처리시, 기저부 형태와 브라켓 재생 방법에 따른 전단접착강도 및 브라켓 탈락 양상을 비교하고자 시행되었다. 교정 치료를 위해 발거된 건전한 소구치 252개를 수집하고, Type I, Type II, Type III 스탠다드 브라켓을 각각 재생 방법에 따라 네 군으로 나누어 준비된 소구치에 접착하고, Instron Universal Testing Machine(Model 4466)으로 전단접착강도를 측정하였으며, 브라켓의 탈락 양상을 관찰하고 브라켓 기저부의 주사전자현미경 소견을 관찰하였다. SPSS 통계처 리 프로그램을 이용하여 일원분산분석(oneway ANOVA), Scheffe's multiple range test를 실시하여 다음과 같은 결론을 얻었다. 1. 브라켓 기저부 형태에 따른 전단접착강도는 유의차가 있었으며(p<0.001), 그 크기는 Type III(round indentation, micro-etched base), Typ I(foil-mesh base), Type II(grooved integral base, micro-etched)의 순이었다. 2. 생 방법에 따른 전단접착강도는, Type I, Tpe II 브라켓에서는 Big Jane에 1분간 처리시 우수한 결과를 보였고 (p<0.05), Type III 브라켓에서는 각 군간 유의한 차이를 보이지 않았다(p>0.05). 3. Type I, Type II 브라켓은 기저부-레진 계면에서 가장 높은 빈도로 탈락하였고, Type III 브라켓에서는 레진의 절반 가량이 치면에 잔존하는 탈락 양상이 가장 많았다. 4. 탈락 양상에 따라 탈락시의 전단접착강도가 유의성 있는 차이를 보였는데(p<0.05),브라켓 탈락시 접착제의 절반 가량이 치면에 잔존하는 경우 전단접착강도가 가장 큰 것으로 나타났다. 5. 브라켓 재생 후 기저부에 남아 있는 접착제는 전단접착강도의 감소에 영향을 미치지 않았다.

• 비파괴검사학회지
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• 제33권2호
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• pp.165-172
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• 2013

발전설비 구조물은 기대 수명동안의 안전성을 확보하기 위하여 정해진 규격에 부합하도록 설계하여 건설된다. 하지만 가동 중 다양한 복합 환경에 노출됨에 따라 구조물을 이루고 있는 재료의 열화 현상이 가속화 되어 예상하지 못한 파손이 발생할 수 있기 때문에, 용접부와 같은 구조물의 취약부에 대하여 기계적 물성을 정확하게 측정하는 기술은 안전과 직결되는 필수적인 연구 분야이다. 인장시험 등의 기존의 역학물성 측정 시험법들은 특정 크기의 시편을 요구하고 파괴적인 시험이기 때문에 가동 중 구조물에 적용하는 것이 불가능하였다. 이러한 한계점을 극복하고자 비파괴적이고 간편한 방법으로 다양한 역학물성 평가가 가능한 연속압입시험법이 각광받는 시험법으로서 연구되고 있다. 본 연구에서는 연속압입시험에서 압입자 하부에 발생하는 응력장 해석을 기반으로 하여 인장물성 및 잔류응력을 평가할 수 있는 최신 기법을 소개한다. 또한, 원전 구조물의 취약부로 알려진 용접부에 대하여 실험을 수행하여 산업상에서 연속압입시험이 건전성 평가에 유용하게 적용할 수 있음을 확인하였다.

• 한국진공학회지
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• 제19권5호
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• pp.360-364
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• 2010

나노 소재의 물성을 측정하기 위하여 대부분의 연구 그룹에서는 크게 두 가지 분석 기법인 분광학을 이용한 분석과 나노트라이볼로지를 이용한 분석을 사용하고 있다. 분광학을 이용한 분석에는 NMR (Nuclear Magnetic Resonance), IR (Infrared Spectroscopy), Raman 등이 대표적이라 할 수 있고, 나노트라이볼로지를 이용한 분석에는 AFM (Atomic Force Micro-Scope), EFM (Electrostatic Force Microscope), KFM (Kelvin Force Microscope), Nanoindenter 등의 탐침을 이용한 측정 기법이 대표적이다. Nanoindenter는 물질의 탄성 및 경도를 측정 할 수 있으며 이를 통해 물질의 특성을 연구 하는 데에 사용된다. 그러나 이런 Nanoindenter의 압입 실험에서 압입 조건 등의 통제 변수가 다르면 그 결과 값도 바뀌는 것을 볼 수 있는데 본 실험에서는 이런 압입 조건 중 Load - Hold - Unload force의 속도 및 시간을 변화시켜 물질의 탄성계수와 경도가 어떠한 차이를 가지는지 연구하였다.

• The Journal of Advanced Prosthodontics
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• 제5권1호
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• pp.36-43
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• 2013

PURPOSE. The objective of this study was to compare the fracture toughness ($K_{Ic}$) obtained from the single edge V-notched beam (SEVNB) and the fractographic analysis (FTA) of a glass-infiltrated and a zirconia ceramic. MATERIALS AND METHODS. For each material, ten bar-shaped specimens were prepared for the SEVNB method ($3mm{\times}4mm{\times}25mm$) and the FTA method ($2mm{\times}4mm{\times}25mm$). The starter V-notch was prepared as the fracture initiating flaw for the SEVNB method. A Vickers indentation load of 49 N was used to create a controlled surface flaw on each FTA specimen. All specimens were loaded to fracture using a universal testing machine at a crosshead speed of 0.5-1 mm/min. The independent-samples t-test was used for the statistical analysis of the $K_{Ic}$ values at ${\alpha}$=0.05. RESULTS. The mean $K_{Ic}$ of zirconia ceramic obtained from SEVNB method ($5.4{\pm}1.6\;MPa{\cdot}m^{1/2}$) was comparable to that obtained from FTA method ($6.3{\pm}1.6\;MPa{\cdot}m^{1/2}$). The mean $K_{Ic}$ of glass-infiltrated ceramic obtained from SEVNB method ($4.1{\pm}0.6\;MPa{\cdot}m^{1/2}$) was significantly lower than that obtained from FTA method ($5.1{\pm}0.7\;MPa{\cdot}m^{1/2}$). CONCLUSION. The mean $K_{Ic}$ of the glass-infiltrated and zirconia ceramics obtained from the SEVNB method were lower than those obtained from FTA method even they were not significantly different for the zirconia material. The differences in the $K_{Ic}$ values could be a result of the differences in the characteristics of fracture initiating flaws of these two methods.