• Title/Summary/Keyword: in situ monitoring

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In situ reduction of gold nanoparticles in PDMS matrices and applications for large strain sensing

  • Ryu, Donghyeon;Loh, Kenneth J.;Ireland, Robert;Karimzada, Mohammad;Yaghmaie, Frank;Gusman, Andrea M.
    • Smart Structures and Systems
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    • v.8 no.5
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    • pp.471-486
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    • 2011
  • Various types of strain sensors have been developed and widely used in the field for monitoring the mechanical deformation of structures. However, conventional strain sensors are not suited for measuring large strains associated with impact damage and local crack propagation. In addition, strain sensors are resistive-type transducers, which mean that the sensors require an external electrical or power source. In this study, a gold nanoparticle (GNP)-based polymer composite is proposed for large strain sensing. Fabrication of the composites relies on a novel and simple in situ GNP reduction technique that is performed directly within the elastomeric poly(dimethyl siloxane) (PDMS) matrix. First, the reducing and stabilizing capacities of PDMS constituents and mixtures are evaluated via visual observation, ultraviolet-visible (UV-Vis) spectroscopy, and transmission electron microscopy. The large strain sensing capacity of the GNP-PDMS thin film is then validated by correlating changes in thin film optical properties (e.g., maximum UV-Vis light absorption) with applied tensile strains. Also, the composite's strain sensing performance (e.g., sensitivity and sensing range) is also characterized with respect to gold chloride concentrations within the PDMS mixture.

Use of In-Situ Optical Emission Spectroscopy for Leak Fault Detection and Classification in Plasma Etching

  • Lee, Ho Jae;Seo, Dong-Sun;May, Gary S.;Hong, Sang Jeen
    • JSTS:Journal of Semiconductor Technology and Science
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    • v.13 no.4
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    • pp.395-401
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    • 2013
  • In-situ optical emission spectroscopy (OES) is employed for leak detection in plasma etching system. A misprocessing is reported for significantly reduced silicon etch rate with chlorine gas, and OES is used as a supplementary sensor to analyze the gas phase species that reside in the process chamber. Potential cause of misprocessing reaches to chamber O-ring wear out, MFC leaks, and/or leak at gas delivery line, and experiments are performed to funnel down the potential of the cause. While monitoring the plasma chemistry of the process chamber using OES, the emission trace for nitrogen species is observed at the chlorine gas supply. No trace of nitrogen species is found in other than chlorine gas supply, and we found that the amount of chlorine gas is slightly fluctuating. We successfully found the root cause of the reported misprocessing which may jeopardize the quality of thin film processing. Based on a quantitative analysis of the amount of nitrogen observed in the chamber, we conclude that the source of the leak is the fitting of the chlorine mass flow controller with the amount of around 2-5 sccm.

대수층에서의 자연표류 실험을 통한 염화지방족 탄화수소화합물 오염 지하수의 생물학적 복원 타당성 연구

  • Kim Jin-Uk;Ha Cheol-Yun;Kim Nam-Hui;Hong Gwang-Pyo;Gwon Su-Yeol;An Yeong-Ho;Ha Jun-Su;Park Hu-Won;Kim Yeong
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2005.04a
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    • pp.127-130
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    • 2005
  • The feasibility of stimulating in situ aerobic cometabolic activity of indigenous microorganisms was investigated in a trichloroethene(TCE)-contaminated aquifer, A series of single-well natural drift tests (SWNDT) was conducted by injecting site groundwater amended with a bromide tracer and combinations of toluene, oxygen, nitrate, ethylene and TCE into an existing monitoring well and by sampling the same well over time. Transformation of ethylene, a surrogate of overall TCE transformation activity, was also observed, and its transformation results in the production of ethylene oxide, suggesting that some tolune-oxidizing microorganisms stimulated may express a monooxygenase enzymes. Also in situ transformation of TCE was confirmed by dilution-adjusted data analysis developed in this study. These results indicate that, in this environment, toluene and oxygen additions stimulated the growth and aerobic cometabolic activity of indigenous microorganisms expressing monooxygenase enzymes and that these are responsible for observed toluene utilization and cometabolism of ethylene and TCE. The simple, low-cost field test method provides an effective method for conducting rapid field assessments and pilot testing of aerobic cometabolism of TCE, which has previously hindered application of this technology to groundwater remediation.

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Stability Analysis of Large Slope Based on In-Situ Monitoring and Numerical Analysis (대절토사면의 현장계측 및 수치해석을 통한 사면 안정성 분석 사례)

  • Kim, Byung-Chul;Hwang, Ji-Hoon;Won, Ji-Hyun;Choi, Mun-Kyu;Kwon, Oh-Sung;Song, Chi-Yong
    • Proceedings of the Korean Geotechical Society Conference
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    • 2005.10a
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    • pp.629-638
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    • 2005
  • 본 연구대상 사면은 연장이 300m이고 최대 사면높이가 80m에 달하는 대절토 사면으로 서 총 11 소단으로 이루어져 있으며, 전 사면에 걸쳐 Soil Nail 공법으로 보강이 되어있다. 사면 상단부에 설치된 2개의 경사계를 이용하여 주기적으로 사면의 수평방향 변위 계측을 실시하던 중, 사면 하부의 소단 굴착과정에서 상대적으로 급격한 사변경사 방향의 수평변위가 발생한 것을 확인하였다. 본 연구에서는 사면의 수평방향 변위 계측결과 분석 및 대상 사면에 대한 수치해석을 통하여 사면의 안정성 여부를 판단하고자 하였으며, 굴착단계별 수평방향 변위량 및 변위 양상을 분석함으로써 급격히 증가한 변위의 원인을 파악하였다. 수치해석을 통해 나타난 사면 굴착 단계에 따른 사면 토체의 소성영역을 도시한 결과, 사면 전체에 걸쳐 대규모 파괴면이 나타났으며 파괴활동면이 Soil Nail 로 보강된 영역의 바깥쪽에 위치하여 사면 안정성 확보를 위한 대책방안이 수립되어야 할 것으로 판단되었다. 또한 보다 자세한 원인 규명을 위한 확인 시추조사를 실시하여 하부 지층 특성을 파악하였으며, 하부에 풍화가 심하고 절리 및 균열이 심한 파쇄구간이 분포하고 있음이 확인되었다. 연구 대상 사면의 변위 계측 결과, 수치해석 결과, 확인 시추 조사 결과 및 예상되는 사면 활동의 규모 등을 고려할 때 사변의 안정성 확보를 위한 대책방안이 수립되어야 하며, 본 사면은 억지말뚝과 Ahchor 공법 적용이 가장 적절할 것으로 판단되었다.

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Towards a Machine Learning Approach for Monitoring Urban Morphology - Focused on a Boston Case Study - (도시 형태 변화 모니터링을 위한 머신러닝 기법의 가능성 - 보스톤 사례연구를 중심으로 -)

  • Hwang, Jie-Eun
    • Design Convergence Study
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    • v.16 no.5
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    • pp.125-140
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    • 2017
  • This study explores potential capability of a machine learning approach for monitoring urban morphology based on an evident case study. The case study conveys year 2006 investigations on interpreting urban morphology of Boston Main Streets by applying a machine learning approach. From the lesson of the precedent study, in 2016, another field research and interview was conducted to compare changes in urban situation, data commons culture, and technology innovation during the decade. This paper describes open possibilities to advance urban monitoring for morphological changes. Most of all, a multi-participatory data platform enables managing urban data system in real time. Second, collaboration with machines with artificial intelligence can intervene the framework of the urban management system as well as transform it through new demands of innovative industries. Recently, urban regeneration became a dominant urban planning strategy in Korean, therefore, urban monitoring is on demand. It is timely important to correspond to in-situ problems based on empirical research.

Conductivity Measurements of Submarine Sediments

  • Park, Chan-Hong;Lee, Seung-Hee;Shon, Ho-Woong
    • Journal of the korean society of oceanography
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    • v.36 no.1
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    • pp.1-8
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    • 2001
  • An in-situ four-electrode contact resistivity probe system was designed, and field-tested in submarine sediments. Seismic survey was also performed to support and compare the results of electric survey. The probe was designed to be driven to selected depths below the seafloor using a Vibracore system. The four insulated electrodes were, spaced equidistant across the wedge, were extended beyond the probe tip to minimize effects of sediment disturbance by the wedge insertion. In-situ measurements of resistivity were recorded on board by precision electronic equipment consisting of signal generators and processors, and by temperature-monitoring systems. Overall limits of Uncertainty at respective depths below the seafloor are up to ${\pm}$10 of the measured values. Best estimates of conductivity are considered to be ${\pm}$3 percent of the reported values. Resistivity measurements were made at six sites in carbonate sediments to a maximum depth of penetration of about 5 m. Average values of conductivity range between 0.88 and 1.21 mho/m. The results show the seabed is composed of alternating layers of relatively high-conductivity material (0.8 to 1.4 mho/m) in thicknesses of more or less one meter and layers about 30 cm thick having relatively low conductivities (0.4 to 0.8 mho/m).

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Condition assessment of bridge pier using constrained minimum variance unbiased estimator

  • Tamuly, Pranjal;Chakraborty, Arunasis;Das, Sandip
    • Structural Monitoring and Maintenance
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    • v.7 no.4
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    • pp.319-344
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    • 2020
  • Inverse analysis of non-linear reinforced concrete bridge pier using recursive Gaussian filtering for in-situ condition assessment is the main theme of this work. For this purpose, minimum variance unbiased estimation using unscented sigma points is adopted here. The uniqueness of this inverse analysis lies in its approach for strain based updating of engineering demand parameters, where appropriate bound and constrained conditions are introduced to ensure numerical stability and convergence. In this analysis, seismic input is also identified, which is an added advantage for the structures having no dedicated sensors for earthquake measurement. First, the proposed strategy is tested with a simulated example whose hysteretic properties are obtained from the slow-cyclic test of a frame to investigate its efficiency and accuracy. Finally, the experimental test data of a full-scale bridge pier is used to study its in-situ condition in terms of Park & Ang damage index. Overall the study shows the ability of the augmented minimum variance unbiased estimation based recursive time-marching algorithm for non-linear system identification with the aim to estimate the engineering damage parameters that are the fundamental information necessary for any future decision making for retrofitting/rehabilitation.

Assessments of the GEMS NO2 Products Using Ground-Based Pandora and In-Situ Instruments over Busan, South Korea

  • Serin Kim;Ukkyo Jeong;Hanlim Lee;Yeonjin Jung;Jae Hwan Kim
    • Korean Journal of Remote Sensing
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    • v.40 no.1
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    • pp.1-8
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    • 2024
  • Busan is the 6th largest port city in the world, where nitrogen dioxide (NO2) emissions from transportation and port industries are significant. This study aims to assess the NO2 products of the Geostationary Environment Monitoring Spectrometer (GEMS) over Busan using ground-based instruments (i.e., surface in-situ network and Pandora). The GEMS vertical column densities of NO2 showed reasonable consistency in the spatiotemporal variations, comparable to the previous studies. The GEMS data showed a consistent seasonal trend of NO2 with the Korea Ministry of Environment network and Pandora in 2022, which is higher in winter and lower in summer. These agreements prove the capability of the GEMS data to monitor the air quality in Busan. The correlation coefficient and the mean bias error between the GEMS and Pandora NO2 over Busan in 2022 were 0.53 and 0.023 DU, respectively. The GEMS NO2 data were also positively correlated with the ground-based in-situ network with a correlation coefficient of 0.42. However, due to the significant spatiotemporal variabilities of the NO2, the GEMS footprint size can hardly resolve small-scale variabilities such as the emissions from the road and point sources. In addition, relative biases of the GEMS NO2 retrievals to the Pandora data showed seasonal variabilities, which is attributable to the air mass factor estimation of the GEMS. Further studies with more measurement locations for longer periods of data can better contribute to assessing the GEMS NO2 data. Reliable GEMS data can further help us understand the Asian air quality with the diurnal variabilities.

Virtual Metrology for predicting $SiO_2$ Etch Rate Using Optical Emission Spectroscopy Data

  • Kim, Boom-Soo;Kang, Tae-Yoon;Chun, Sang-Hyun;Son, Seung-Nam;Hong, Sang-Jeen
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.464-464
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    • 2010
  • A few years ago, for maintaining high stability and production yield of production equipment in a semiconductor fab, on-line monitoring of wafers is required, so that semiconductor manufacturers are investigating a software based process controlling scheme known as virtual metrology (VM). As semiconductor technology develops, the cost of fabrication tool/facility has reached its budget limit, and reducing metrology cost can obviously help to keep semiconductor manufacturing cost. By virtue of prediction, VM enables wafer-level control (or even down to site level), reduces within-lot variability, and increases process capability, $C_{pk}$. In this research, we have practiced VM on $SiO_2$ etch rate with optical emission spectroscopy(OES) data acquired in-situ while the process parameters are simultaneously correlated. To build process model of $SiO_2$ via, we first performed a series of etch runs according to the statistically designed experiment, called design of experiments (DOE). OES data are automatically logged with etch rate, and some OES spectra that correlated with $SiO_2$ etch rate is selected. Once the feature of OES data is selected, the preprocessed OES spectra is then used for in-situ sensor based VM modeling. ICP-RIE using 葰.56MHz, manufactured by Plasmart, Ltd. is employed in this experiment, and single fiber-optic attached for in-situ OES data acquisition. Before applying statistical feature selection, empirical feature selection of OES data is initially performed in order not to fall in a statistical misleading, which causes from random noise or large variation of insignificantly correlated responses with process itself. The accuracy of the proposed VM is still need to be developed in order to successfully replace the existing metrology, but it is no doubt that VM can support engineering decision of "go or not go" in the consecutive processing step.

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Design, Optimization and Verification of 16S rRNA Oligonucleotide Probes of Fluorescence in-situ Hybridization for Targeting Clostridium spp. and Clostridium kluyveri

  • Hu, Lintao;Huang, Jun;Li, Hui;Jin, Yao;Wu, Chongde;Zhou, Rongqing
    • Journal of Microbiology and Biotechnology
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    • v.28 no.11
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    • pp.1823-1833
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    • 2018
  • Fluorescence in-situ hybridization (FISH) is a common and popular method used to investigate microbial communities in natural and engineered environments. In this study, two specific 16S rRNA-targeted oligonucleotide probes, CLZ and KCLZ, were designed and verified to quantify the genus Clostridium and the species Clostridium kluyveri. The optimal concentration of hybridization buffer solution for both probes was 30% (w/v). The specificity of the designed probes was high due to the use of pellets from pure reference strains. Feasibility was tested using samples of Chinese liquor from the famed Luzhou manufacturing cellar. The effectiveness of detecting target cells appears to vary widely in different environments. In pit mud, the detection effectiveness of the target cell by probes CLZ and KCLZ was 49.11% and 32.14%, respectively. Quantitative analysis by FISH technique of microbes in pit mud and fermented grains showed consistency with the results detected by qPCR and PCR-DGGE techniques, which showed that the probes CLZ and KCLZ were suitable to analyze the biomass of Clostridium spp. and C. kluyveri during liquor fermentation. Therefore, this study provides a method for quantitative analysis of Clostridium spp. and C. kluyveri and monitoring their community dynamics in microecosystems.