• 제목/요약/키워드: hot pressed

검색결과 260건 처리시간 0.021초

PDMS 충진법을 이용하여 형성한 유연열전모듈의 발전특성과 굽힘특성 (Power Generation Properties and Bending Characteristics of a Flexible Thermoelectric Module Fabricated using PDMS Filling Method)

  • 한기선;오태성
    • 마이크로전자및패키징학회지
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    • 제26권4호
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    • pp.119-126
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    • 2019
  • 18쌍의 Bi2Te3계 p-n 가압소결체 열전레그들로 구성되어 있으며 상하부 기판이 없고 내부는 polydimethylsiloxane (PDMS)로 충진되어 있는 유연열전모듈을 형성하고, 이의 발전특성과 굽힘특성을 분석하였다. 유연열전모듈을 팔목에 부착하였을 때 서있는 정적인 상태에서는 2.23 mV의 open circuit 전압과 1.69 ㎼의 최대출력전력이 얻어졌으며, 걸어가는 동적인 상태에서는 3.32 mV의 open circuit 전압과 3.41 ㎼의 최대출력전력이 얻어졌다. 유연열전모듈에 굽힘곡률반경 25 mm로 30,000회까지 반복굽힘 싸이클을 인가하여도 저항변화율이 1% 미만으로 유지되었다.

PDMS로 충진된 신축열전모듈의 신축특성과 발전특성 (Stretchable Characteristics and Power Generation Properties of a Stretchable Thermoelectric Module Filled with PDMS)

  • 한기선;오태성
    • 마이크로전자및패키징학회지
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    • 제26권4호
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    • pp.149-156
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    • 2019
  • 5쌍의 Bi2Te3계 p-n 가압소결체 열전레그들로 구성되어 있으며 상하부 기판이 없고 내부는 polydimethylsiloxane (PDMS)로 충진되어 있는 신축열전모듈을 형성하고, 이의 신축특성과 발전특성을 분석하였다. 신축열전모듈에 변형률 0~0.1 범위의 신축변형 싸이클을 10회 인가하여도 모듈의 integrity가 잘 유지되었으며, 인장변형률이 0.2로 증가시 Cu 전극과 열전레그 사이의 접합부 파단에 의해 모듈이 open 되었다. 신축열전모듈은 열전레그 양단간의 온도차가 2.2 K일 때 4.6 mV의 open circuit 전압을 나타내었으며, 변형률 0~0.1 범위의 인장변형에 의한 open circuit 전압의 변화는 5% 미만이었다. 신축열전모듈은 0.1의 변형률로 인장된 상태에서 레그 양단간 온도차 2.2 K에 의해 18.5 ㎼의 최대발전출력을 나타내었다.

Y2O3가 첨가된 Al2O3-TiC복합 소결체의 치밀화와 기계적 성질 (Sintering and Machanical Properties of Y2O3 Added Al2O3-TiC Composite)

  • 최종선;박상엽;김득중;강석중
    • 한국세라믹학회지
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    • 제26권3호
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    • pp.438-444
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    • 1989
  • The role of TiC and the effect of Y2O3 addition on the densification, microstructure and mechanical properties of Al2O3-TiC composite have been studied. The amount of Y2O3 has been varied from 0 to 2 wt.% while keeping the TiC content at 10, 20 or 30 wt.%. The powder compacts have been sintered at 1,75$0^{\circ}C$ for various times in 1 atm Ar atmosphere and hot isostatically pressed (HIPed) at 1,$600^{\circ}C$ for 0.5h under 1,500atm Ar. Considerable increase in sintered density(over 95%) has been achieved by adding 0.5 wt.% Y2O3 in specimens containing high TiC volume. More addition of Y2O3 does not affect the densification. With increasing the sintering time from 0.5 to 4h, slight increase in density results. The growth of Al2O3 grain has been enhanced by Y2O3 addition ; this tendency is reduced with increasing TiC content because of grain boundary dragging effect of TiC particles. The hardness of specimens increases considerably by an addition of 0.5wt.% Y2O3 owing to the density increase. Further addition of Y2O3 has no effect on hardness. Fracture toughness augments with TiC content by crack deflection around the particles. By adding 0.5wt.% Y2O3, all the specimens can be densified to isolated pore stage and thus can be HIPed to full densification and better mechanical property. In particular, the fracture toughness of Al2O3-30 TiC specimen increases about 50% by HIPing. Fully dense Al2O3-30 TiC with good mechanical properties can be prepared by normal Sintering/HIPing process.

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$Al_2O_3+Y_2O_3 첨가량에 따른 {\beta}-SiC-ZrB_2$계 전도성 복합체의 특성 (The Properties of $\beta-SiC-ZrB_2$ Electroconductive Ceramic Composites with $Al_2O_3+Y_2O_3$Contents)

  • 신용덕;주진영;황철
    • 대한전기학회논문지:전기물성ㆍ응용부문C
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    • 제49권9호
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    • pp.516-522
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    • 2000
  • The mechanical and electrical properties of the hot-pressed and annealed $\beta-SiC-ZrB_2$ electroconductive ceramic composites were investigated as a function of the liquid forming additives of$Al_2O_3+Y_2O_3$ Phase analysis of composites by XRD revealed $\alpha-SiC(6H) ZrB_2\; and YAG(Al_5Y_3O_{12})$ The relative density of composites were increased with increased Al2O3+Y2O3 contents. The Flexural strength showed the highest value of 390.6MPa for composites added with 20wt% Al2O3+Y2O3 additives at room temperature. Owing to crack deflection crack bridging phase transition and YAG of fracture toughness mechanism the fracture toughness showed the highest value of 6.3MPa.m1/2 for composites added with 24wt% Al2O3+Y2O3 additives at room temperature. The resistance temperature coefficient showed the value of$ 2.46\times10^{-3}\;, 2.47\times10^{-3},\; 2.52\times10^{-3}/^{\circ}C$ for composite added with 16, 20, 24wt% Al2O3+Y2O3 additives respectively. The electrical resistivity of the composites was all positive temperature coefficient resistance(PTCR) in the temperature range of $256{\circ}C\; to\; 900^{\circ}C$.

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액장 소결한 $\beta-SiC-TiB_2$계 전도성 복합체의 특성 (The Properties of $\beta-SiC-TiB_2$ Electroconductive Ceramic Composites Densified by Liquid-Phase Sintering)

  • 임승혁;신용덕;송준태
    • 대한전기학회논문지:전기물성ㆍ응용부문C
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    • 제49권9호
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    • pp.510-515
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    • 2000
  • The mechanical and electrical properties of the hot-pressed and annealed $\beta-SiC-TiB_2$ electroconductive ceramic composites were investigated as a function of the liquid forming additives of Al_2O_3+Y_2O_34. The result of phase analysis of composites by XRD revealed $\alpha-SIC(6H)\;TiB_2,\; and YAG(Al5Y3O12) crystal phase. The relative density and the mechanical properties of composites were increased with increasing $Al_2O_3+Y_2O_34 contents because YAG of reaction between $Al_2O_3\; and\; Y_2O_3$ was increased. The Flexural strength showed the highest value of 432.5MPa for composites added with 12wt% $Al_2O_3+Y_2O_34 additives at room temperature. Owing to crack deflection crack bridging phase transition and TAG of fracture toughness mechanism the fracture toughness showed 7.1MPa.m1/2 for composites added with 12wt% $Al_2O_3+Y_2O_34 additives at room temperature. The electrical resistivity and the resistance temperature coefficient showed the lowest of $6.0\times10-4\Omega.cm\; and\; 3.1\times10-3/^{\circ}C4 respectively for composite added with 12wt% \Omega additives at room temperature. The electrical resistivity of the composites was all positive temperature coefficient resistance (PTCR) in the temperature range of $25^{\circ}C\; to\; 700^{\circ}C$.

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ITO/p-InP 태양전지 제작 (The fabrication of ITO/p-InP solar cells)

  • 맹경호;김선태;송복신;문동찬
    • E2M - 전기 전자와 첨단 소재
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    • 제7권3호
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    • pp.243-251
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    • 1994
  • ITO(Indium Tin Oxide) film with thickness of 1500.angs. was prepared by an e-beam evaporator onto a glass and a p-type InP wafer (100) LEC grown Zn-doped p=2.3*10$\^$16/cm$\^$-3/), in which the components of ITO used for evaporation source were hot pressed pellets 1 mole% ln$\_$2/O$\_$3/+9 mole% SnO$\_$2/, and evaporated in O$\_$2/ ambient. The optimum conditions to preparation of ITO thin film were the substrate temperature of 350.deg. C, the injected oxygen pressure of 2*10$\^$-4/ torr, and the evaporation speed of 0.2-0.3.angs./sec, respectively. In these optimum conditions, the resistivity and the carrier concentration were 5.3*10$\^$-3/ .ohm.-cm, 6.5*10$\^$20/cm$\^$-3/, and the transmittance was over 80%. From the results of J-V measurements in ITO/p-InP structure solar cells, the higher pressure of injected oxygen, the more open circuit voltage. The efficiency of ITO/p-InP solar cell without the grid line contact, prepared by the optimum evaporation conditions, was 7.19%. By using the grid line contact, the efficiency, the open circuit voltage, the short circuit current density, the fill factor, the series resistance, and the shunt resistance were 8.5%, 0.47V, 29.48 mAcm$\^$-2/ , 61.35%, 3.ohm., and 26.6k.ohm., respectively.

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$\beta-SIC-ZrB_{2}$복합체의 파괴인성과 전기전도도에 미치는 YAG의 영향 (Effect of YAG on the Fracture Toughness and Electrical Conductivity of $\beta-SIC-ZrB_{2}$ Composites)

  • 신용덕;주진영;윤세원;황철;박미림
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 하계학술대회 논문집
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    • pp.839-842
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    • 2000
  • The mechanical and electrical properties of the hot-pressed and annealed $\beta$-SiC-ZrB$_2$ electroconductive ceramic composites were investigated as function of the liquid forming additives of $Al_2$O$_3$+Y$_2$O$_3$. Phase analysis of composites by XRD revelled $\alpha$ -SiC(6H), ZrB$_2$, and YAG(Al$_{5}$ Y$_3$O$_{12}$ ). Owing to crack deflection, crack bridging, phase transition and YAG of fracture toughness mechanism, the fracture toughness showed the highest value of 6.3MPa.m$^{1}$2/ for composites added with 24wt% $Al_2$O$_3$+Y$_2$O$_3$additives at room temperature. The resistance temperature coefficient respectively showed the value of 2.46$\times$10$^{-3}$ , 2.47$\times$10$^{-3}$ , 2.52$\times$ 10$^{-3}$ $^{\circ}C$ for composite added with 16, 20, 24wt% A1$_2$O$_3$+Y$_2$O$_3$additives. The electircal resistivity of the composites was all positive temperature coefficient resistance(PTCR) in the temperature range of $25^{\circ}C$ to 90$0^{\circ}C$.

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일축인장시험을 통한 투명교정장치용 고분자 소재의 역학적 특성 분석 (Analysis of Mechanical Properties of Polymer Material for Clear Aligner using Uniaxial Tensile Test)

  • 정지영;제태진;전은채
    • 한국기계가공학회지
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    • 제17권5호
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    • pp.64-69
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    • 2018
  • Clear aligners are popular in the field of dental orthodontic treatment because they offer a discreet alternative to braces due to their use of transparent materials. They are formed from flat transparent polymer materials by hot pressed molding. It is necessary to know the mechanical properties of the polymer materials to be able to form the exact shapes of the clear aligners. However, this information is not publicly available. In this study, we present a method to reliably measure the mechanical properties of clear aligner polymer materials and analyze the factors effecting these mechanical properties. First, we surveyed standards related to the mechanical properties of polymer materials to obtain reliable data. Consequently, ISO 527 was selected for use in this study because of the size and thickness of the flat transparent polymer material. The uniaxial tensile tester was constructed and it was verified whether displacement of a crosshead could be regarded as a displacement of gauge-length by optical analysis. Uniaxial tensile tests of three thicknesses from three different companies were performed and each engineering stress-strain curve was measured. Tensile strengths and elastic moduli were obtained by analysis of the stress-strain curves. The tensile strength and elastic modulus of ISO 527 was found to be approximately 50MPa and 2.3GPa, respectively. Both values showed material and thickness dependency.

Modified Densification Process for Increasing Strength Properties of Pine and Gmelina Wood from Community Forests

  • Yunianti, Andi Detti;Tirtayasa P., Kidung;Suhasman, Suhasman;Taskirawati, Ira;Agussalim, Agussalim;Muin, Musrizal
    • Journal of the Korean Wood Science and Technology
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    • 제47권4호
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    • pp.418-424
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    • 2019
  • Densification is a process for improving the strength properties of wood from the felling of young trees, which is a common harvest practice in community forests. A series of experiments was conducted to refine the process with particular regard to the determination of suitable pretreatment and treatment conditions. Samples of pine and gmelina measuring $23cm(L){\times}20cm(W){\times}2cm(T)$ underwent pretreatment through immersion in a 1:1 $CH_3COOH-H_2O_2$ solution at concentrations of 15%, 20%, and 30%. Samples pretreated with the 20% solution showed the greatest improvement in strength; further experiments were conducted to determine the optimum treatment conditions in terms of temperature and duration following immersion. Test samples with the same dimensions as those in the pretreatment experiment were soaked in a 1:1 20% $CH_3COOH-H_2O_2$ solution and warmed in a water bath. The test samples were then individually hot pressed to the target thickness, which was 30% less than the original thickness and held at $150^{\circ}C$ or $170^{\circ}C$ for 15 or 30 minutes. The treated samples were cut for an analysis of their density, recovery of set, and bending strength. Pine and gmelina exhibited the best characteristics after treatment at $150^{\circ}C$ for 30 and 15 minutes, respectively. The results suggest that the modified densification process had increased the bending strength of the wood, but the temperature and duration of treatment must be carefully considered for different wood species.

열간가압소결에 의한 SiC-AIN 고용체의 상 및 미세구조 (Phase and microstructure of hot-pressed SiC-AlN solid solutions)

  • Chang-Sung Lim;Chang-Sam Kim;Deock-Soo Cheong
    • 한국결정성장학회지
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    • 제6권2호
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    • pp.238-246
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    • 1996
  • $\beta$-SiC와 AIN의 혼합분말로부터 열간가압소결에 의하여 고밀도의 SiC-AIN 고용체가 $1870^{\circ}C$에서 $2030^{\circ}C$ 사이의 온도범위에서 제조되어졌다. 온도와 SiC/AIN의 비 및 seed의 존재에 따라 AIN과 $\beta$-SiC(3C) 분말의 반응은 2 H (wurzite) 구조로의 전이를 나타내었다. 결정상들은 SiC-rich 및 AIN-rich 고용체로 구성되었다. $2030^{\circ}C$, 1시간에서 5 wt%의 $\alpha$-SiC seed를 첨가한 50 % AIN/50% SiC의 조성에 대하여 완전한 고용체가 얻어졌으며, 미세구조가 비교적 균일한 2 H상의 결정립 크기를 가지고균일한 성장경향을 나타내었다. SiC-AIN 고용체에 있어서 $\alpha$-SiC seed의 변수가 전이기구 및 결정립의 크기와 모양을 비롯한 결정립 크기의 분포, 조성의 불균일성과 구조적 결함 등에 영향을 미칠 수 있었다.

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