• Title/Summary/Keyword: hot pressed

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X-ray Diffraction Analysis of Residual Stress in Laminated Ceramic

  • Jin, Young-Ho;Chung, Dong-Yoon
    • Journal of the Korean Ceramic Society
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    • v.48 no.5
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    • pp.458-462
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    • 2011
  • The strength of ceramic was improved by lamination by suppressing the propagation of cracks with compressive residual stress in the face layer of the laminate. Hot pressed SiAlON+SiC/SiC/SiAlON+SiC laminate discs were fabricated for tailored residual stress. The residual stress in this laminate was studied by X-ray diffraction (XRD). There was considerable compressive residual stress in the face layer. A Finite Element Analysis (FEA) was performed to support the measured XRD results and to determine the stress field in the laminate. The residual stress measured by XRD had satisfactory agreement with the analytically calculated and FEA values. The measured value by XRD was -385 ${\pm}$ 20 MPa over most of the face layer. The calculated and FEA values were -386 MPa and -371MPa, respectively. FEA also showed significantly modified stresses and the maximum tensile stress near the edge region which are possible crack generators in the presence of flaws or contact damage.

Synthesis and Properties of Ultra-fine (Ti, M1, M2)(CN)-Ni Cermets

  • Kang, Young-Jae;Kang, Shin-Hoo
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.644-645
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    • 2006
  • TiC-and Ti(C,N)-based cermets are excellent in semi-and final finishing of work piece during cutting operations. Typical microstructure of the cermets is a core/rim structure. The undissolved Ti(C,N) cores contribute to their high hardness while the rim phases, (Ti,M1,M2)(C,N)-type solid solutions, play great roles in enhancing the toughness. In this paper, various ultrafine pre-mixed MeC-Ni powders were synthesized and the powders were sintered or hot pressed after mixing in order to control the size and volume fractions of core and rim phases in the system. This paper will present the factors determining the microstructure along with mechanical properties.

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A novel urine-activated microbattery

  • Jin, Bo;Gu, Hal-Bon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.396-397
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    • 2006
  • The novel urine-activated microbatteries have been successfully demonstrated. In this microbattery, a magnesium (Mg) layer and copper chloride (CuCl) in the filter paper are used as the anode and the cathode, respectively. A stack consisting of a Mg layer, CuCl-doped filter paper and a copper (Cu) layer sandwiched between two plastic layers is hot-pressed into the microbatteries at $100^{\circ}C$. The microbatteries can be activated by adding a droplet of human urine. The experimental results show that the microbattery can deliver a maximum voltage of 1.4 V and maximum power of 1.96 mW for the $1\;k{\Omega}$ load resistor.

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A Development of Manufacturing Process of Wooden Footpath Block to Reuse of Wood Waste (목질폐잔재를 재활용한 목질보도블록 제조기술 개발)

  • Park, Hee-Jun
    • Journal of the Korean Wood Science and Technology
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    • v.25 no.3
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    • pp.96-104
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    • 1997
  • The objective of this research project was to develop the wooden footpath block to reuse of wood waste. Some physical and mechanical properties of the wooden block such as water absorption, thickness swelling, modulus of rupture, internal bond, density profile and impact resistance were studied. Water absorption and thickness swelling of the wooden block were greatly reduced when the wooden block was pressed inside the forming device than by conventional hot pressing. Also, Modulus of rupture and internal bond of the wooden block were increased greatly when the pressing was completed inside the forming device. The density profile of the wooden block was improved up to 93.5%, minimum to average density ratio. The wooden block manufactured in this study have excellent physical and mechanical prperties in comparison with existing wood based materials. So, these wooden blocks are applicable to footpth block or other exterior members.

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Physical-Mechanical Properties of Laminated Board Made from Oil Palm Trunk (Elaeis guineensis Jacq.) Waste with Various Lamina Compositions and Densifications

  • PRABUNINGRUM, Dita Sari;MASSIJAYA, Muh Yusram;HADI, Yusuf Sudo;ABDILLAH, Imam Busyra
    • Journal of the Korean Wood Science and Technology
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    • v.48 no.2
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    • pp.196-205
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    • 2020
  • The purpose of this study was to investigate a method for improving the physical and mechanical properties of laminated board made from oil palm trunk (OPT). The effects of pretreating the lamina with heat-pressure and altering the lamina composition of the laminated board were investigated. The outer third of OPT in cross-section had high-density wood, while the underlying third had low to medium density. The hot press was applied to pretreat the lamina that had low to medium density. The lamina were 1.5 cm in thickness, 5 cm in width, and 65 cm in length. The hot press was applied at 2.94 MPa or 4.41 MPa at 150 ℃ for 60 minutes, and the target thickness of the lamina was 1 cm. The three layers of the laminated board samples were bonded with isocyanate adhesive at a glue spread of 300 g/㎡ and cold pressed at 0.98 MPa for 3 h. The laminated board samples were tested according to Japanese Agricultural Standard (JAS) 234-2003. The results showed that the densification of the inner lamina did not significantly affect the physical-mechanical properties of the laminated board produced. However, the laminated board made with high-density laminas for the outer layers fulfilled the JAS 234-2003 standard for the modulus of elasticity and the modulus of rupture.

Characterization of Hot Isostatically Pressed Ni-Based Superalloy IN 713C (열간 등압 성형된 니켈기 초내열 합금 IN 713C 분말 소결체의 특성 평가)

  • Kim, Youngmoo;Kim, Eun-Pyo;Chunga, Seong-Taek;Lee, Seong;Noh, Joon-Woong;Lee, Sung Ho;Kwon, Young-Sam
    • Journal of Powder Materials
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    • v.20 no.4
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    • pp.264-268
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    • 2013
  • Nickel-based superalloy IN 713C powders have been consolidated by hot isostatic pressing (HIPing). The microstructure and mechanical properties of the superalloys were investigated at the HIPing temperature ranging from $1030^{\circ}C$ to $1230^{\circ}C$. When the IN 713C powder was heated above ${\gamma}^{\prime}$ solvus temperature (about $1180^{\circ}C$), the microstructure was composed of the austenitic FCC matrix phase ${\gamma}$ plus a variety of secondary phases, such as ${\gamma}^{\prime}$ precipitates in ${\gamma}$ matrix and MC carbides at grain boundaries. The yield and tensile strengths of HIPed specimens at room temperature were decreased while the elongation and reduction of area were increased as the processing temperature increased. At $700^{\circ}C$, the strength was similar regardless of HIPing temperature; however, the ductility was drastically increased with increasing the temperature. It is considered that these properties compared to those of cast products are originated from the homogeneity of microstructure obtained from a PM process.

Sinterability of Low-Cost 3Y-ZrO2 Powder and Mechanical Properties of the Sintered Body

  • Kim, Min-Sung;Go, Shin-Il;Kim, Jin-Myung;Park, Young-Jo;Kim, Ha-Neul;Ko, Jae-Woong;Jung, Seung-Hwa;Kim, Jae-Yuk;Yun, Jon-Do
    • Journal of the Korean Ceramic Society
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    • v.54 no.4
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    • pp.285-291
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    • 2017
  • This study investigated the effects of grain size and phase constitution on the mechanical properties of $3Y-ZrO_2$ by varying the sintering conditions. The raw powder prepared by a low-cost wet milling using the coarse solid oxide powders was sintered by both pressureless sintering and hot-pressing, respectively. As increasing holding time at $1450^{\circ}C$ for pressureless sintering, it promoted the microstructural coarsening of matrix grains and the phase transformation to tetragonal phase, whereas the bimodal microstructure embedded with abnormal $cubic-ZrO_2$ grains was observed regardless of sintering time. On the other hand, the specimens hot-pressed at $1300^{\circ}C$ for 2 h reached ~ 97% of relative density with homogeneous fine microstructure and mixed phase constitution. It was found that the proportion of untransformed monoclinic zirconia had the most adverse effect on the biaxial strength compared to the impacts of grain size and density. The pressureless sintering of the low-cost powder for prolonged sintering time to 8 h led to a decent combination of mechanical properties ($H_V=13.2GPa$, $K_{IC}=8.16MPa{\cdot}m^{1/2}$, ${\sigma}=981MPa$).

Optical, Mechanical and Tribological Properties of Boronnitride Dispersed Silicon Nitride Ceramics

  • Joshi, Bhupendra;Fu, Zhengyi;Niihara, Koichi;Lee, Soo-Wohn
    • Korean Journal of Materials Research
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    • v.20 no.8
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    • pp.444-449
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    • 2010
  • Transparent ceramics are used in new technology because of their excellent mechanical properties over glasses. Transparent ceramics are nowadays widely used in armor, laser windows, and in high temperature applications. Silicon nitride ceramics have excellent mechanical properties and if transparent silicon nitride is fabricated, it can be widely used. h-BN has a lubricating property and is ductile. Therefore, adding h-BN to silicon nitride ceramics gives a lubricating property and is also machinable. Translucent silicon nitride was fabricated by hot-press sintering (HPS) and 57% transmittance was observed in the near infrared region. A higher wt. % of h-BN in silicon nitride ceramics does not favor transparency. The optical, mechanical, and tribological properties of BN dispersed polycrystalline $Si_3N_4$ ceramics were affected by the density, ${\alpha}:{\beta}$-phase ratio, and content of h-BN in sintered ceramics. The hot pressed samples were prepared from the mixture of $\alpha-Si_3N_4$, AlN, MgO, and h-BN at $1850^{\circ}C$. The composite contained from 0.25 to 2 wt. % BN powder with sintering aids (9% AlN + 3% MgO). A maximum transmittance of 57% was achieved for the 0.25 wt. % BN doped $Si_3N_4$ ceramics. Fracture toughness increased and wear volume and the friction coefficient decreased with an increase in BN content. The properties such as transmittance, density, hardness, and flexural strength decreased with an increase in content of h-BN in silicon nitride ceramics.

Effect of carbon and boron addition on sintering behavior and mechanical properties of hot-pressed SiC (카본 및 보론 첨가가 탄화규소 열간 가압 소결거동 및 기계적 특성에 미치는 영향)

  • Ahn, Jong-Pil;Chae, Jae-Hong;Kim, Kyoung-Hun;Park, Joo-Seok;Kim, Dae-Gean;Kim, Hyoung-Sun
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.18 no.1
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    • pp.15-21
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    • 2008
  • SiC has an excellent resistance to oxidation and corrosion, high temperature strength and good thermal conductivity. However, it is difficult to density because of its highly covalent bonding characteristics. Hot-press sintering process was applied to fabricate fully densified SiC ceramics with carbon and boron addition as a sintering additive. The addition of carbon improved the mechanical properties of SiC because it could induce a fine and homogeneous microstructure by the suppression of abnormal growth of SiC grain. Also, the addition of carbon could control the phase transformation of SiC. The phase transformation of 6H to 4H increased with sintering temperature but the addition of carbon decreased that kind of phase transformation.

Thermoelectric properties of hot pressed polycrystalline $Bi_2Te_3-Bi_2Se_3$ (가압소결된 다결정 $Bi_2Te_3-Bi_2Se_3$ 열전재료의 열전특성)

  • Hwang, C.W.;Hong, I.G.;Paik, D.K.;Choi, S.C.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.4 no.4
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    • pp.363-369
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    • 1994
  • Bimuth telluride base thermoelectrics are prepared by AC current applied hot pressing method. It is possible to minimize the defects arising from the vaporization of Te, thanks to the very short processing time compared to the single crystal growing method. The optimum conditions for the AC applied hot pressing of 95 mol% $Bi_2Te_3-5 mol% Bi_2Se_3$ thermoelectrics are sintering at $400^{\circ}C$, for 2 minutes, under 1500 kgf/$\textrm{cm}^2$, with the particle size of $125 to 250 {\mu}m$, range of powder. The resultant Z value (figure of merit) was $2.2{\times}10^{-3}/K$.

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