• Title/Summary/Keyword: homogenous

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Hydrothermal Synthesis of 6mol% Yttria Stabilized Cubic ZrO2 Nano Powders (이트리아 안정화 지르코니아 나노 분말 합성)

  • Lee, Jae-Hoon;Bae, Sung-Hwan
    • Korean Journal of Materials Research
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    • v.27 no.8
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    • pp.445-450
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    • 2017
  • YSZ (Yttria-stabilized zirconia) is a ceramic material that is used for electronic and structural materials due to its excellent mechanical properties and specific electrical characteristics according to the Yttrium addition. Hydrothermal synthesis has several advantages such as fine particle size, uniform crystalline phase, fast reaction time, low process temperature and good dispersion condition. In order to synthesize YSZ nanoparticles with high crystallinity, hydrothermal synthesis was performed at various concentrations of NaOH. The hydrothermal process was held at a low temperature ($100^{\circ}C$), with a short process time (2,4,8 hours); the acidity or alkalinity of solution was controlled in a range of pH 2~12 by addition of NaOH. The optimum condition was found to be pH 12, at which high solubility levels of Y(OH) and Zr(OH) were reported. The synthesized nano powder showed high crystallinity and homogenous composition, and uniform particle size of about 10 nm.

A Strategy for Homogeneous Current Distribution in Direct Methanol Fuel Cells through Spatial Variation of Catalyst Loading

  • Park, Sang-Min;Kim, Sang-Kyung;Peck, Dong-Hyun;Jung, Doo-Hwan
    • Journal of Electrochemical Science and Technology
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    • v.8 no.4
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    • pp.331-337
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    • 2017
  • A simple strategy is proposed herein for attaining uniform current distribution in direct methanol fuel cells by varying the catalyst loading over the electrode. In order to use the same total catalyst amount for a serpentine flow field, three spatial variation types of catalyst loading were selected: enhancing the cathode catalyst loading (i) near the cathode outlet, (ii) near the cathode inlet, and (iii) near the lateral areas. These variations in catalyst loading are shown to improve the homogeneity of the current distribution, particularly at lower currents and lower air-flow rates. Among these three variations, increased loading near the lateral areas was shown to contribute most to achieving a homogenous current distribution. The mechanism underlying each catalyst loading variation method is different; very high catalyst-loading is shown to decrease the homogeneity of the distribution, which may be caused by water management in the thick catalyst layer thereof.

Waveguide Applicator System for Head and Neck Hyperthermia Treatment

  • Fiser, Ondrej;Merunka, Ilja;Vrba, Jan
    • Journal of Electrical Engineering and Technology
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    • v.11 no.6
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    • pp.1744-1753
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    • 2016
  • The main purpose of this article is a complex hyperthermia applicator system design for treatment of head and neck region. The applicator system is composed of four waveguides with a stripline horn aperture and circular water bolus. The specific absorption rate (SAR) and temperature distribution from this applicator in various numerical phantom models was investigated. For used targets, the treatment planning based on the optimization process made through the SEMCAD X software is added to show the steering possibilities of SAR and thereby temperature distribution. Using treatment planning software, we proved that the SAR and temperature distribution can be effectively controlled (by amplitude and phase changing) improving the SAR and temperature target coverage approximately by 20 %. For the proposed applicator system analysis and quantitative evaluation of two parameters 25 % iso-SAR and $41^{\circ}C$ iso-temperature contours in the treatment area with the respect to sensitive structures in treatment area were defined. To verify our simulation results, the real measurement of reflectivity coefficient as well as the temperature distribution in a homogenous phantom were performed.

Application of magnesium to improve uniform distribution of precipitated minerals in 1-m column specimens

  • Putra, Heriansyah;Yasuhara, Hideaki;Kinoshita, Naoki;Hirata, Akira
    • Geomechanics and Engineering
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    • v.12 no.5
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    • pp.803-813
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    • 2017
  • This study discussed the possible optimization of enzyme-mediated calcite precipitation (EMCP) as a soil-improvement technique. Magnesium chloride was added to the injection solution to delay the reaction rate and to improve the homogenous distribution of precipitated minerals within soil sample. Soil specimens were prepared in 1-m PVC cylinders and treated with the obtained solutions composed of urease, urea, calcium, and magnesium chloride, and the mineral distribution within the sand specimens was examined. The effects of the precipitated minerals on the mechanical and hydraulic properties were evaluated by unconfined compressive strength (UCS) and permeability tests, respectively. The addition of magnesium was found to be effective in delaying the reaction rate by more than one hour. The uniform distribution of the precipitated minerals within a 1-m sand column was obtained when 0.1 mol/L and 0.4 mol/L of magnesium and calcium, respectively, were injected. The strength increased gradually as the mineral content was further increased. The permeability test results showed that the hydraulic conductivity was approximately constant in the presence of a 6% mineral mass. Thus, it was revealed that it is possible to control the strength of treated sand by adjusting the amount of precipitated minerals.

Synthesis and Characterization of Fe-containing AC/TiO2 Composites and Their Photodegradation Effect for the Piggery Waste

  • Oh, Won-Chun
    • Environmental Engineering Research
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    • v.13 no.2
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    • pp.85-92
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    • 2008
  • In this present study, we have synthesized Fe-containing AC(activated carbon)/$TiO_2$ composites with titanium (VI) n-butoxide (TNB) as a titanium source to Fe treated AC through an impregnation method. The result of the textural surface properties demonstrates that there is a slight decrease in the BET surface area of composite samples with an increase of the amount of Fe treated. The surface properties of scanning electron microscope (SEM) presented a characterization of a porous texture on the Fe-containing AC/$TiO_2$ composites and homogenous compositions for Fe and titanium dioxide distributed on the sample surfaces. Fe compound peaks and a titanium dioxide structure were observed in the X-ray diffraction patterns for the Fe-containing AC/$TiO_2$ composites. The results of chemical elemental composition for the Fe-containing AC/$TiO_2$ composites showed that most of the spectra for these samples gave stronger peaks for C, O, treated Fe components and Ti metal than that of any other elements. From the photo degradation results for the piggery waste, the Fe-containing AC/$TiO_2$ composites showed an excellent degradation activity for the chemical oxygen demand (COD) due to a photocatalysis of the supported $TiO_2$, radical reaction by Fe species and the adsorptivity and absorptivity of porous carbon.

The Population Genetic Structure of the Oyster Crassostera gigas (Bivalvia:Ostreidae) from Gamak Bay in Korea (가막산 참굴의 집단 구조 분석)

  • Cho, Eun-Seob;Jeong, Hee-Dong
    • Journal of Life Science
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    • v.18 no.7
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    • pp.1015-1018
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    • 2008
  • To analyze the population genetic structure of the oyster Crassostrea gigas Thunberg, 34 specimens werecollected from Gamak bay in March, 2007. Total genomic DNA was extracted from each sample and PCR was performed to identify haplotypes of oyster by using HCO2918 and LCO1491 primers. Four kinds of haplotypes (CR1, CR2, CR3, and CR4) were identified. Among these group, CR3 showed the highest relative frequency at 73% than any other of haplotypes. On the basis of hierarchical genetic structure, the population of Gamak showed a higher genetic relationship with Namhae, but the genetic distance between southern and western coasts was negative and no statistical significance was found (p>0.05). Consequently, the oyster from Korea coast is determined to be both homogenous and large.

Surgical Treatment of a Plunging Ranula using the Intraoral and Submandibular Approach (구강 내 접근과 하악하 절개를 통한 몰입성 하마종의 수술적 치료)

  • Kim, Jung Hong;Eun, Seok Chan;Baek, Rong Min
    • Archives of Craniofacial Surgery
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    • v.11 no.2
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    • pp.111-115
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    • 2010
  • Purpose: A plunging ranula is relatively uncommon and represents a mucus escape reaction occurring from a disruption of the sublingual salivary gland. It is a common condition found in young adults, even though the reported age range is 2 - 61 years. We report our experience of a complete excision of a plunging ranula via the intraoral and submandibular approach. Methods: A 23-year-old man had a large protruding mass in the right submandibular area. Initially, the protruding mass appeared bilaterally but the left side disappeared spontaneously. The MRI findings revealed a homogenous fluid attenuation mass in the submandibular space, suggesting a ranula. The sublingual gland was extirpated through the intraoral approach and the ranula excised totally via the submandibular approach. Results: The patient had an uneventful postoperative course without infection, paralysis and tongue sensory changes, etc. The pathology findings were characteristic of a pseudocyst without a lining epithelium or endothelium but with a vascular fibro-conective tissue wall filled with mucinous fluid. No recurrence was observed on the submandibular area during the 8 month follow-up period. Conclusion: The combined intraoral approach and submandibular approach is an effective and highly recommended method for sublingual gland extirpation and complete excision of a plunging ranula.

CYTOMORPHOLOGICAL STUDIES ON THE GIANT CELL LESIONS (거대 세포출현 병소부에 관한 세포학적 연구)

  • Lim, Chang-Youn;Chun, Dong-Jin;Park, Jae-Ho;Choi, Poo-Pyoung
    • The Journal of the Korean dental association
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    • v.9 no.4
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    • pp.191-194
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    • 1971
  • The authors have studied cytomorphologically on the gian cells appearing in the giant cell lesions which had been collected from the biopsies at the department of oral pathology, college of dentistry, Seoul National University. The results are as follows: 1. We can classify two types of giant cells and large sized giant cells which have foamy, large nuclei and prominent nucleoli, and small sized giant cells which have small, round and homogenous stained cytoplasm. 2. We can not see the phagocytosed materials, only can see the foamy microvacuoles in the cytoplasm of giant cells. 3. We can not see the mitotic figures, nore fused figures in giant cells. 4. Osteoclasts in the periphery of bone tissue reveal large and pale stained with H-E stain, giant cells on the granulation tissue and chronic inflammatory tissue reveal deeply stained with hematoxylin and prominent nuclei, but smaller than osteoclasts.

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Cytologic Features of Secretory Meningioma in Squash Preparation -A Case Report- (분비성 수막종의 입착도말 소견 -1예 보고-)

  • Kim, Se-Hoon;Lee, Kwang-Gil;Kim, Tai-Seung
    • The Korean Journal of Cytopathology
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    • v.15 no.1
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    • pp.52-55
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    • 2004
  • Secretory meningioma is a distinct subtype of meningioma. We describe the cytologic features of a secretory meningioma on squash preparations, in comparision with other cytologic mimickers. A 54-year-old woman presented with hearing loss, vertigo, tinnitus, and headache for seven years. A brain MRI study revealed a 4.5cm sized mass in the cerebellopontine angle, which showed homogenous signal intensity in T2-weighted image. The intraoperative squash smear showed some well-defined, thin rimmed intracytoplasmic inclusions, containing a finely granular eosinophilic core among less cohesive meningiomatous cells. Histologic sections revealed a meningothelial meningioma with scattered inclusions, with periodic acid-Schiff, carcinoembryonic antigen, and cytokeratin positivity. Identification of characteristic intracytoplasmic inclusions is helpful for diagnosing secretory meningiomas. On squash preparations, differential diagnoses included tumors with inclusions or cytoplasmic vacuolizations, such as metastatic mammary infiltrating ductal carcinoma, gastric adenocarcinoma, hepatocellular carcinoma, and clear cell ependymoma, oligodendroglioma, hemangioblastoma, chordoma, and other variants of meningiomas (clear cell, xanthomatous, microcytic, and chordoid variants). In addition, the possibilities of glioma with eosinophilic granular body, and metastatic tumors from mammary infiltrating ductal carcinoma, gastric adenocarcinoma, and hepatocellular carcinoma in meningioma should be considered.

Morphological Studies on the Epithelium of the Foregut of the Nymph and the Adult in the Grasshopper, Oxya sinuosa (우리벼메뚜기 유충과 성충의 전장 점막상피에 관한 형태학적 연구)

  • Lee, Hyeung-Sik;Lee, Jae-Hyun
    • Applied Microscopy
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    • v.20 no.2
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    • pp.12-22
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    • 1990
  • The morphological characteristics and changes of the foregut in the grasshopper (Oxya sinuosa Mistshenko) have been studied with the special reference to the developmental stage. In light microscope level, the epithelia are seen the cuboidal shape in the 5th instar nymph and the adult. A number of pigment granules are appeared in the cuboidal epithelium of the 5th instar nymph, however the pigment granules were a few in the adult. Indistinct or undifferentiated folds of the epithelial layer were appeared in the 5th instar nymph, whereas the well-developed folds were in the adult. The well-developed muscular layers are seen in the 5th instar nymph, however in the adult the muscular layers are appeared thin or a few layer except the crop. In electron microscope level, in the foregut epithelium, a few round or oval shaped mitochondria, well-developed rER, Golgi complex, lysosome and a number of vacuoles were appeared in the cytoplasm. Two types of pigment granules, electron dense or homogenous and low electron dense or lamellar profiles, are seen in the esophageal epithelium. The crystalline profiles and plasma membrane infoldings were also appeared. In the foregut epithelium of the 5th instar nymph, however the cell organelles were generally undifferentiated and in the crop two types of pigment granules as the adult esophageal epithelium were also found.

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