• Title/Summary/Keyword: high-s milling

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Ethanol Fermentation of Raw Cassava Starch (II) (캇사바전분의 무증자당화에 의한 에타놀발효에 관한 연구(I I))

  • Bae, Moo;Lee, Jae-Moon
    • Microbiology and Biotechnology Letters
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    • v.12 no.4
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    • pp.261-264
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    • 1984
  • The optimal condition of the ethanol fermentation from raw cassava starch by simultaneous saccharification - fermentation (SSF) was studied using glucoamylase from Aspergillus sp. and a yeast strain. The rate and yield of ethanol production were optimum at pH 3.6 with shaking. The fine milling treatment was effective for both saccharification and SSF of raw cassava starch. The presaccharification at 6$0^{\circ}C$ for 1 hr before SSF increased the rate and yield of ethanol production, as well. To increase the ethanol concentration after fermentation the substrate concentration could be increased up to 2195 without the problem of viscosity. The use of high concentration ethanol tolerant yeast strains and high substrate concentration produced ethanol higher than 10%(W/V) after fermentation for 5 days.

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The LaserFIB: new application opportunities combining a high-performance FIB-SEM with femtosecond laser processing in an integrated second chamber

  • Ben Tordoff;Cheryl Hartfield;Andrew J. Holwell;Stephan Hiller;Marcus Kaestner;Stephen Kelly;Jaehan Lee;Sascha Muller;Fabian Perez-Willard;Tobias Volkenandt;Robin White;Thomas Rodgers
    • Applied Microscopy
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    • v.50
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    • pp.24.1-24.11
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    • 2020
  • The development of the femtosecond laser (fs laser) with its ability to provide extremely rapid athermal ablation of materials has initiated a renaissance in materials science. Sample milling rates for the fs laser are orders of magnitude greater than that of traditional focused ion beam (FIB) sources currently used. In combination with minimal surface post-processing requirements, this technology is proving to be a game changer for materials research. The development of a femtosecond laser attached to a focused ion beam scanning electron microscope (LaserFIB) enables numerous new capabilities, including access to deeply buried structures as well as the production of extremely large trenches, cross sections, pillars and TEM H-bars, all while preserving microstructure and avoiding or reducing FIB polishing. Several high impact applications are now possible due to this technology in the fields of crystallography, electronics, mechanical engineering, battery research and materials sample preparation. This review article summarizes the current opportunities for this new technology focusing on the materials science megatrends of engineering materials, energy materials and electronics.

A Study on Hydrodynamic Stiffness Characteristics of Air Bearing for High Speed Spindle

  • Lee, J.Y.;Lee, D.W.;Seong, S.H.;Lee, Y.C.
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.10b
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    • pp.115-116
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    • 2002
  • This study was carried out as one of efforts to overcome difficulties in air bearing design due to low stiffness and low damping. Hydrodynamic effects on hydrodynamic stiffness of a fluid film in a high speed air bearing with tow-row air sources are investigated. The hydrodynamic effects by the high speed over DN 1,000,000 and eccentricity of a proceeding which are not considered in conventional design of an air bearing need to be reconsidered. The hydrodynamic effects, which dominantly influence on the load capacity of air bearing, are caused mainly by proceeding speed, eccentricity, and the source positions. The two-row source arrangement in the air bearing produces quite unique hydrodynamic effects with respect to pressure distribution of the air film. Optimal arrangement of the two-row sources improves performance of an air bearing in film reaction force and loading capacity of high speed spindles. This study compares the pressure distribution by numerical simulation as a function of eccentricity of proceeding and the source positions. The air source position 1/7L form one end of an air bearing was found to be superior to source position of 1/4L. The dynamic stiffness were obtained using a two-dimensional cutting method which can directly measure the cutting reaction forces and the displacements of the spindle in two directions using a tool dynamometer and transducer sensors. Heat generation in the air film can not be negligible over the speed of DN 2,000,000. In order to analysis effects of heat generation on the characteristics of air bearing, high cooling bearing spindle and low cooling bearing spindle were tested and compared. Characteristics of the frequency response of shaft and motion of run out errors were different for the spindle. The test results show that, in the case of low cooling bearing spindle, the stiffness became smaller due to heat generation. The results, which were obtained for high speed region, may be used as a design information for spindle which can be applied to precision devices such as ultra precision grinding and ultra high speed milling.

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Improvement of the Magnetic Properties of (Nd, Dy)-Fe-B Sintered Magnets by Modification of HD and Annealing Processes (HD 처리 및 열처리공정 개선에 의한 (Nd, Dy)-Fe-B 소결자석의 자기특성 향상)

  • NamKung, S.;Lee, Y.H.;Kim, M.K.;Jang, T.S.
    • Journal of Powder Materials
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    • v.17 no.5
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    • pp.359-364
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    • 2010
  • In an attempt to optimize the magnetic properties of (Nd, Dy)-Fe-B sintered magnets, hydrogenation and post-sintering heat treatment processes were investigated at various hydrogenation temperatures and heat treatment temperatures. The coercivity of (Nd, Dy)-Fe-B sintered magnets hydrogenated at $400^{\circ}C$ increased to about 1.2 kOe without any detrimental effect on the remanence. Moreover, the coercivity of the magnets was enhanced further by a consecutive $2^{nd}$ and $3^{rd}$ step heat treatment. These results eventually leaded to the reduction of the Dy content in a high coercive (> 30 kOe) (Nd, Dy)-Fe-B sintered magnets, as much as 10%.

A Study on Nuclear Legacy Site Management according to International Management Guidance (국제 관리 지침에 따른 레거시 부지 관리에 대한 연구)

  • Chang, Sunyoung
    • Journal of the Korean Society of Radiology
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    • v.16 no.2
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    • pp.185-194
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    • 2022
  • The decommission of nuclear legacy sites, which have been contaminated by previous activities such as uranium mining & milling as well as nuclear tests, has started to gain global attention. Within the Korean peninsula, Republic of Korea(ROK)has had experience in dismantling research reactors. For the Democratic People's Republic of Korea(DPRK), the possibility of nuclear activities being implemented and operations records being managed without consideration of the latest nuclear safety regulations are high. Hence, the chances of DPRK's sites remaining as nuclear legacy is also high. This study investigates approaches and considerations that needs to be taken in account in the event of a nuclear legacy site occurrence, reviewing its international cases for the solution of the legacy sites. The regulation, process of optimization, and stakeholder engagement for a nuclear legacy site should be considered in such an event. Developing legacy site response plans can be used to prevent future legacy site occurrences.

Characterization and synthesis of aqueous pink-red ceramic ink for digital inkjet printing (잉크젯 프린팅용 pink-red 수계 무기잉크의 제조 및 특성평가)

  • Lee, Won-Jun;Hwang, Hae-Jin;Han, Kyu-Sung;Cho, Woo-Suk;Kim, Jin-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.25 no.1
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    • pp.20-26
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    • 2015
  • Ceramic ink-jet printing technology in art tiles, decorated tablewares and other porcelain products has many advantages of fast and precision printing of various images with high efficiency and low cost. For the application to ink-jet printing, ceramic ink requires a stable dispersibility with nano-sized pigments. In this paper, characteristics of pink-red aqueous ceramic ink for ink-jet printing was demonstrated. $CaCr_{0.1}Sn_{0.8}SiO_5$ pigment was synthesized using solid state reaction and deagglomerated using attrition milling. The aqueous ceramic ink contains 10 wt% of the obtained $CaCr_{0.1}Sn_{0.8}SiO_5$ nanopigment with 0.4 wt% of sodium dodecyl sulfate (SDS) as a dispersion agent. Viscosity of $CaCr_{0.1}Sn_{0.8}SiO_5$ aqueous ceramic ink was adjusted using 0.18 wt% of polyvinyl alcohol (PVA) for a suitable jetting from the nozzle. The prepared pink-red ceramic ink showed a good jetting property with formation of a single sphere-shaped droplet after $180{\mu}s$ without a tail and satellite droplet.

A Study on the Removal of CFRP Machining Defects by Various Tool Geometries (공구 형상에 따른 CFRP의 가공결함 제거에 관한 연구)

  • Park, Ki Moon;Ko, Tae Jo;Yu, Zhen;Kumaran S, Thirumalai
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.16 no.4
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    • pp.16-23
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    • 2017
  • CFRP(Carbon Fiber Reinforced Plastics) has many industrial applications due to its low weight and high strength properties. Due to its superior properties, for example, excellent resistance to fatigue wear, corrosion, and breakage from fatigue, it has been widely applicable to aircraft, automotive, and medical industries and so on. The main machining for CFRP is drilling, and route milling. In case of drilling, the machining defects such as the delamination of each layer, uncut fiber, resin burning, spalling, and exit burrs are inevitable. The issue to remove such kind of defects is necessary to make CFRP parts successful. From this point of view, this paper investigates the removal effectiveness of machining defects existing at exit region with different type of tool geometries. Consequently, based on the experiments, the tool geometry is most impact factor to remove uncut fiber or resin.

Structural and Magnetic Properties of Mechanochemically Prepared Li Ferrite Nanoparticles

  • Haddadi, M.;Mozaffari, M.;Amighian, J.
    • Journal of Magnetics
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    • v.22 no.2
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    • pp.169-174
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    • 2017
  • In this work, lithium ferrite ($Li_{0.5}Fe_{2.5}O_4$) nanoparticles were prepared via mechanochemical processing and subsequent heat treatment at a relatively low ($600^{\circ}C$) calcining temperature. The raw materials used were high purity $Fe_2O_3$ and $Li_2CO_3$ that were milled for between 2 and 20 h. The milled powders were then calcined at temperatures of 500 and $600^{\circ}C$ for 5 h in air. XRD results show that optimum conditions to obtain single phase lithium ferrite nanoparticles with a mean crystallite size of about 23 nm, using Scherrer's formula, are 10 h milling and calcination at $600^{\circ}C$. Saturation magnetization and coercivity of the single phase Li ferrite nanoparticles are 44.6 emu/g and 100 Oe respectively, which are both smaller than those of the bulk Li ferrite. The Curie temperature of the single sample was determined by a Faraday balance, which is $578^{\circ}C$ and smaller than that of bulk Li ferrite.

A Study on Acoustic Signal Characterization for Al and Steel Machining by Audio Deep Learning (오디오 딥러닝을 활용한 Al, Steel 소재의 절삭 깊이에 따른 오디오 판별)

  • Kim, Tae-won;Lee, Young Min;Choi, Hae-Woon
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.20 no.7
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    • pp.72-79
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    • 2021
  • This study reports on the experiment of using deep learning algorithms to determine the machining process of aluminium and steel. A face cutting milling tool was used for machining and the cutting speed was set between 3 and 4 mm/s. Both materials were machined with a depth to 0.5mm and 1.0mm. To demonstrate the developed deep learning algorithm, simulation experiments were performed using the VGGish algorithm in MATLAB toobox. Downcutting was used to cut aluminum and steel as a machining process for high quality and precise learning. As a result of learning algorithms using audio data, 61%-99% accuracy was obtained in four categories: Al 0.5mm, Al 1.0mm, Steel 0.5mm and Steel 1.0mm. Audio discrimination using deep learning is derived as a probabilistic result.

Synthesis Behavior of Ti-50.0 ~ 66.7at%Si Powders by In situ Thermal Analysis during Mechanical Alloying (기계적 합금화과정에서의 in situ 열분석에 의한 Ti-50.0~66.7at%Si 분말의 합성거동)

  • Byun Chang Sop;Lee Sang Ho;Lee Wonhee;Hyun Chang Yong;Kim Dong Kwan
    • Korean Journal of Materials Research
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    • v.14 no.5
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    • pp.310-314
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    • 2004
  • Mechanical alloying (MA) of Ti-50.0~66.7at%Si powders was carried out in a high-energy ball mill, and in situ thermal analysis was also made during MA. In order to classify the synthesis behavior of the powders with respect to at%Si, the synthesis behavior during MA was investigated by in situ thermal analysis and X-ray diffraction (XRD). In situ thermal analysis curves and XRD patterns of Ti-50.0~59.6at%Si powders showed that there were exothermic peaks during MA, indicating TiSi, $TiS_2$, and $Ti_{5}$ $Si_4$ phase formation by a rapid exothermic reaction of self-propagating high-temperature synthesis (SHS). Those of Ti-59.8~66.7 at%Si powders, however, showed that there were no peaks during MA, indicating any Ti silicide was not synthesised until MA 240 min. For Ti-50.0~59.6at%Si powders, the critical milling times for SHS increased from 34.5 min to 89.5 min and the temperature rise, $\Delta$T (=peak temperature-onset temperature) decreased form $26.2^{\circ}C$ to $17.1^{\circ}C$ as at%Si increased. The critical composition of Si for SHS reaction was found to be 59.6at% and the critical value of the negative heat of formation of Ti-59.6at%Si to be -1.48 kJ/g.