• Title/Summary/Keyword: high-Tc

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Fabrication of Superconducting Precursor for Electric Power Transmission (전력전송용 초전도 전구체의 합성)

  • Lee, Sang-Heon;Lee, Young-Hie
    • Proceedings of the KIEE Conference
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    • 2005.11a
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    • pp.77-78
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    • 2005
  • A high Tc superconducting with a nominal composition of $Bi_{2}Sr_{2}Ca_{2}Cu_{3}O_{Y}$ was prepared by the citarte method. The solid precursor produced by the dehydration of the gel at $120^{\circ}C$ for 12h is not in the amorphous state as expected but in a crystalline state. X-ray diffraction peaks of nearly the same angular position as the peaks of high Tc phase were observed in the precursor. After pyrolysis at $400^{\circ}C$ and calcination at $840^{\circ}C$ for 4h, the (001)peak of the high Tc phase was cleary observed. Experimental results suggest that the intermediate phase formed before the formation of the superconducting phase may be the most important factro in determining whether it is easy to form the high Tc phase or not, because the nucleation barriers of the two superconducting phase may be altered by the variation of the crystal structures of those intermediate phase.

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Investigation of Properties and Fabrication of the High Tc Superconducting Motor (고온초전도 모타의 제작과 특성 고찰)

  • Sohn, M.H.;Ha, D.W.;Jeong, D.Y.;Ryu, K.S.;Yun, M.S.
    • Proceedings of the KIEE Conference
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    • 1990.07a
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    • pp.254-256
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    • 1990
  • We fabricated a high Tc superconducting motor named the "Meissner Motor" using Y system high Tc superconductors, which rotates with the repulsive force caused by the Meissner effect. And, we derived the optimal rotating conditions and parameters from the examination of its chracteristics. Finally the possibility of a high Tc superconducting rotor has been investigated.

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Optimal Design and fabrication of Prototype DC Reactor for Inductive Superconducting fault Current Limiter (유도형 고온초전도 한류기용 Prototype 직류 리액터의 설계와 제작)

  • 김태중;강형구;고태국
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.12S
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    • pp.1292-1298
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    • 2003
  • In this paper, dc reactor lot the inductive high-Tc superconducting fault current limiter (SFCL) was optimally designed by finite element method(FEM). The Prototype high-Tc do reactor was manufactured and compared to the results of design. This dc reactor consists of 4∼stacked double pancake coils which are wounded with Bi-2223 wire coated with SUS315L. Kapton tape is used for the insulation of turn to turn and layer to layer. Each pancake is connected in series by soldering Finally, optimal design and manufacture method lot the dc reactor is suggested in this paper. Through the comparison of result of optimal design and experimental result of prototype high-Tc superconducting dc reactor, reliance on the design of the high-Tc dc reactor tot the 1.2 kV/80 A SFCL is proved.

Fabrication of High Tc Superconductor Using Thermal pyrolysis Method (열분해법 의한 초전도선재 합성)

  • Lee, Sang-Heon;Choi, Young
    • Proceedings of the KIEE Conference
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    • 2006.07c
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    • pp.1337-1338
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    • 2006
  • BiSrCaCuO was prepared by the thermal pyrolysis method. The solid precursor produced by the dehydration of the gel at $120^{\circ}C$ for 12h is not in the amorphous state as expected but in a crystalline state. X-ray diffraction peaks of nearly the same angular position as the peaks of high Tc phase were observed in the precursor. After pyrolysis at $90^{\circ}C$ and calcination at $840^{\circ}C-920^{\circ}C$ for 4h, the high Tc phase was cleary observed. In this paper, the establishment of fabrication condition and additive effects of second elements were examined so as to improve the related properties to the practical use of BiSrCaCuO superconductor, and we reported the production of the BiSrCaCuO high Tc superconductor by the pyrolysis method.

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Detection for Residual Thyroid Tissue and Metastatic Lesion after Total Thyroidectomy in Patients with Differentiated Thyroid Cancer: Comparison between Tc-99m Pertechnetate Sean and High Dose I-131 Therapy Sean (분화 갑상선암 환자의 수술후 잔여갑상선조직 및 전이병소의 진단: Tc-99m Pertechnetate 스캔과 고용량 옥소 치료 후 I-131 스캔의 비교)

  • Lee, Joo-Ryung;Ahn, Byeong-Cheol;Jeong, Shin-Young;Lee, Jae-Tae;Lee, Kyu-Bo
    • The Korean Journal of Nuclear Medicine
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    • v.37 no.2
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    • pp.120-127
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    • 2003
  • Purpose: To evaluate diagnostic sensitivity of nuclear imaging in the detection of residual thyroid tissue and metastatic lesion, we have compared neck scintigrams with Tc-99m pertechnetate (Tc-99m scan) and high dose I-131 iodide (I-131 scan) in patients with differentiated thyroid cancer. Subjects and Methods: One hundred thirty-five thyroidectomized patients for differentiated thyroid cancer were enrolled in this study. Twenty-three had a previous history of radioiodine therapy. Planar and pin-hole images of anterior neck with Tc-99m were acquired at 20 minutes after injection, followed by I-131 scan three days after high-dose radioiodine therapy within 7 days interval. Patients were asked to discontinue thyroid hormone replacement more than 4 weeks. Results: All subjects were in hypothyroid state. Seventy out of 135 patients (51.9%) showed concordant findings between Tc-99m and I-131 scans. I-131 scan showed higher number of uptake foci in all of 65 patients showing discordant finding. Tc-99m scan showed no thyroid bed uptake in 34 patients, whereas 23 of them (67.6%) showed bed uptake in I-131 scan. Tc-99m scan did not show any uptake in thyroid bed in 11 of 112 patients without previous history of radioiodine therapy, but 9 of them showed bed uptake in I-131 scan. Tc-99m scan showed no bed uptake in all of the 23 patients with previous history of radioiodine therapy, in contrast 14 of them (60.9%) showed bed uptake in I-131 scan. Conclusion: These results suggest that Tc-99m scan has poor detectability for residual thyroid tissue or metastatic lesion in thyroidectomized differentiated thyroid cancer patients, compared to high dose I-131 therapy scan. Tc-99m scan could not detect any remnant tissue or metastatic lesion in patients with previous history of radioiodine treatment, especially.

Effect of the Bifunctional Chelate on the Biodistribution of 99mTc-labeled Cyclic RGD Peptide

  • Lee, Dong-Eun;Choi, Kang-Hyuk
    • Journal of Radiation Industry
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    • v.12 no.4
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    • pp.355-363
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    • 2018
  • A novel $N_3S_1$ chelate, Pro-Lys-Cys (PKC) to cyclic RGD to radiolabel with $^{99m}Tc$ was conjugated in an effort to decrease the high intestinal accumulation observed for $^{99m}Tc$-labeled PGC-RGD. The target specificity of the resulting PKC-RGD was similar to that of PGC-RGD as determined by a cell binding assay and a competition binding assay. The $^{99m}Tc$ radiolabeling of PKC-RGD resulted in radiochemical yields of 98% under mild conditions at high specific activities. Biodistribution data in normal mice clearly showed a significant decrease in intestinal uptake at 2 h postinjection for the $^{99m}Tc-PKC-c$ (RGDyK) compared to the $^{99m}Tc-GC-c$ (RGDyK) (from $19.65%ID{\cdot}g^{-1}$ to $7.31%ID{\cdot}g^{-1}$ for the GI tract). The $^{99m}Tc-PKC-c$ (RGDyK) biodistribution was also shown by a higher retention of radioactivity in the whole body, but with kidney accumulation over 8-fold higher than observed with $^{99m}Tc-PGC-c$ (RGDyK) at 2 h ($12.62%ID{\cdot}g^{-1}$ for PKC-RGD and $1.54%ID{\cdot}g^{-1}$ for PGC-RGD, respectively). These results show that the biodistribution may be altered especially concerning lipophilicity resulting in renal rather than hepatobiliary excretion. This comparative study made it possible to explore the effects of lipophilicity on the biodistribution of $^{99m}Tc$-labeled c (RGDyK) through the use of different tripeptide $N_3S_1$ chelators. Therefore, $^{99m}Tc-PKC-c$ (RGDyK) may be an attractive alternative for the in vivo imaging of integrin receptors.

Syntheses and Properties of the High-Tc Superconductive Bi_{2-x}Mo_xSr_2Ca_2Cu_3O_y$ System

  • Keu Hong Kim;Jong Tae Lim;Seung Koo Cho;Byoung Chan Kwak;Don Kim;Jae Shi Choi
    • Bulletin of the Korean Chemical Society
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    • v.11 no.1
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    • pp.25-28
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    • 1990
  • The superconducting properties have been studied for high-Tc superconductors of the $Bi_{2-x}Mo_xSr_2Ca_2Cu_3O_y$ system (x = 0.03-0.30). The crystal structure is pseudo tetragonal with the average lattice parameters a = 5.38 ${\AA}$, b = 5.44 ${\AA}$ and c = 30.6 ${\AA}$. All samples exhibit superconductivity with Tc offset at 79 K and Tc onset at 90-115 K. The Tc onset point decreases with increasing x, but the Tc offset points are nearly the same for all samples. Scanning electron micrographs show a special growth behavior of the grains with a plate shape. It is suggested that the decrease in Tc onset points with substitution of Mo for Bi is due to the decrease in lattice parameters and to the p-orbital of Mo. It is concluded that Mo does not play a crucial role in the superconducting transition of the $Bi_2Sr_2Ca_2Cu_3O_y$ system.

Clinical Usefulness of 99mTc-DMSA Renal SPECT Using High Sensitivity-All Purpose Collimator for Pediatric Patients (고감도 범용성 콜리메이터를 이용한 소아 환자 99mTc-DMSA 신장 SPECT의 유용성)

  • Kim, Jin-Eui;Kim, Jung-Soo;Han, Jae-Bok;Choi, Nam-Gil
    • The Journal of the Korea Contents Association
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    • v.16 no.3
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    • pp.219-231
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    • 2016
  • $^{99m}Tc$-DMSA planar scan that can analyze the functions of kidney quantitatively provides less information on a lesion than tomography scanning. Therefore, this study applied a high sensitivity all-purpose collimator that is sensitive to photonic signals to $^{99m}Tc$-DMSA and carried out a clinical scan with single photon emission computed tomography (SPECT). And diagnostic accuracy and time requirement of were analyzed to know the clinical usefulness of the applied scanning method. 10 subjects were intravenously injected with radiopharmaceutical product (1.0-1.2 MBq/kg) and scanned by a gamma camera with planar scanner (high resolution (HR)-mode, $256{\times}256$, 50 kcts/view, 4 image) and SPECT (HR / high sensitive (HS)-mode, $128{\times}128$, step and shoot, $180^{\circ}$, variable sec/angle, total 64 frame, OSEM reconstruction), respectively. The collected data was compared with an analysis program. The results showed that HS-mode SPECT detected total counts 1.8-5.6 times more than planar scan. Relative renal function evaluated based on the counts was not significantly different by two scanning methods (p=0.96) and it turned out that test time was shortened by 39% when HS-mode SPECT was used. Therefore, SPECT using HR, HS-mode collimator could analyze renal function more quantitatively than using planar scan and the former could diagnose the location information of a lesion more accurately than the latter as well as shortened test time requirement, which demonstrated the clinical usefulness of $^{99m}Tc$-DMSA renal SPECT using high sensitivity all purpose collimator.

Electrical Properties of High Tc Superconductors Using the Pyrolysis Method for Renewed Electric Power Energy

  • Lee Sang-Heon
    • KIEE International Transactions on Electrophysics and Applications
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    • v.5C no.5
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    • pp.217-220
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    • 2005
  • We have fabricated a superconducting YBCO system according to the pyrolysis method and low pressure apparatus. In our experiment, the X-ray diffraction pattern of the non doped YBaCuO layer indicated that the superconductor contained only 90K phase crystal. The critical temperature and critical current density for a thick layer at $650^{\circ}C$ were Tc=90 K and $Jc=6{\times}10^{4}A/cm^2$ at 90K. In low pressure apparatus, the 90 K phase YBaCuO was grown at a lower temperature compared with the normal system. Tc and Jc at $650^{\circ}C$ were Tc = 90 K and $Jc=6{\times}10^{4}A/cm^2$ at 90K.

Sintering Period Dependence of Composition and Superconducting Properties of (BiPb)SrCaCuOx System ((BiPb)SrCaCuOx계에서 소결시간에 따른 조성과 초전도 성질의 변화)

  • Prak, S.;Im, H. B.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1988.10a
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    • pp.98-101
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    • 1988
  • The material system (Bi$\sub$0.7/Pb$\sub$0.3/)Sr$_1$Ca$_1$Cu$\sub$1.8/Ox forms, at 845$^{\circ}C$, two major phases having a high Tc(100K) and a low Tc(∼70K) both of which consists of platelets and a non-superconducting minor phase which has rod-like shape and isolated by the major phases. As the sintering period increases, the amount of high Tc phase increases accompanying the decrease in low Tc phase while the amount of the non-superconducting phase is sintering period independent, resulting in a superconductor with Tc of 100K. Changes in compositions of each phase also occur during sintering due to evaporation of bismuth and lead.

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